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    Isc Practical-Questions

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    Anubhab Dutta Gupta
    This document provides questions and answers related to volumetric analysis techniques and concepts covered in an ISC Practical exam. It includes questions about standard solutions, redox reactions of KMnO4, titration principles and calculations, acid-base reactions, qualitative analysis of cations and anions using group reagents, tests for functional groups like carbonyls and carbohydrates. The document tests the examinee's understanding of concepts and procedures from titrimetry, qualitative analysis, and organic qualitative analysis.

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    Isc Practical-Questions

    Uploaded by

    Anubhab Dutta Gupta
    92 views4 pages
    This document provides questions and answers related to volumetric analysis techniques and concepts covered in an ISC Practical exam. It includes questions about standard solutions, redox reactions of KMnO4, titration principles and calculations, acid-base reactions, qualitative analysis of cations and anions using group reagents, tests for functional groups like carbonyls and carbohydrates. The document tests the examinee's understanding of concepts and procedures from titrimetry, qualitative analysis, and organic qualitative analysis.

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    ISC PRACTICAL-QUESTIONS

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    This document provides questions and answers related to volumetric analysis techniques and concepts covered in an ISC Practical exam. It includes questions about standard solutions, redox reactions of KMnO4, titration principles and calculations, acid-base reactions, qualitative analysis of cations and anions using group reagents, tests for functional groups like carbonyls and carbohydrates. The document tests the examinee's understanding of concepts and procedures from titrimetry, qualitative analysis, and organic qualitative analysis.

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    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    92 views4 pages

    Isc Practical-Questions

    Uploaded by

    Anubhab Dutta Gupta
    This document provides questions and answers related to volumetric analysis techniques and concepts covered in an ISC Practical exam. It includes questions about standard solutions, redox reactions of KMnO4, titration principles and calculations, acid-base reactions, qualitative analysis of cations and anions using group reagents, tests for functional groups like carbonyls and carbohydrates. The document tests the examinee's understanding of concepts and procedures from titrimetry, qualitative analysis, and organic qualitative analysis.

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    © All Rights Reserved
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    Download as docx, pdf, or txt
    of 4

    ISC PRACTICAL

    1. What is a standard solution?

    2. What is the equivalent mass of KMnO4 when it acts as oxidizing agent in


    acidic medium?
    (A) 158/5 (B) 158 (C)158/2 (D)158/7

    3. What volume of 10M HCl must be diluted with water to get 1L of 1M HCl?
    (A) 0.1L (B)1L (C)10L (D)100l
    4. What is the principle of volumetric analysis?

    5. It is customary to read lower meniscus in case of colourless and


    transparent solutions and upper meniscus in case of highly coloured
    solutions, why?

    6. What is a molar solution?

    7. Why the last drop of solution must not be blown out of a pipette?

    8. Which is an oxidizing agent and a reducing agent in the reaction between


    KMnO4 and FeSO4?

    9. What is the indicator used in KMnO4 titration?


    10.Why does KMnO4 act itself as an indicator?

    11. What is the end point in KMnO4 titrations?


    12.

    Why are a few drops of dilute sulphuric acid added while preparing a
    standard solution of Mohr’s salt?

    13.Why should you heat the oxalic acid solution to about 60-70°C before
    titrating with KMnO4 solution?

    14.Name the acid radicals detected with dil. H2SO4.


    Carbonate, Sulphite
    15.Name the acid radicals detected by cone. H2SO4.
    Chloride, Nitrate
    16.How is sodium carbonate extract prepared?
    Refer to practical notes
    17.NO2 and Br2 both are brown in colour. How will you distinguish between
    them?
    By acidified ferrous sulphate solution
    18.What is Tollen’s reagent?
    Refer to text book
    19.Why a dark brown ring is formed at the junction of two layers in ring test
    for nitrates?
    Sulphuric acid is heavier than salt sol + ferrous sulphate
    So two layers are formed
    Refer to text book for equations
    20.Why acetic acid is added before adding lead acetate solution?

    21.What is the formula of Sodium nitroprusside?


    22.Name group reagents for different groups.

    23.. Why is it essential to add dil. HCl before proceeding to the test for the
    basic radicals of group II?
    Refer to application of Solubility product from ionic equilibrium Chapter
    (class XI)
    24.Why is the O.S. boiled with cone. HNO3, in III group?

    25.Why is NH4Cl added along with NH4OH in III group?


    Refer to application of Solubility product from ionic equilibrium Chapter
    (class XI)
    26.What is blue lake?

    27.The presence of NH4Cl is quite essential before the addition of (NH4)2CO3 in


    group V. Explain why?
    Refer to application of Solubility product from ionic equilibrium Chapter
    (class XI)
    28.Can we use ammonium sulphate in place of ammonium chloride in group
    III precipitation?

    29.Can we add ammonium hydroxide before ammonium chloride first for


    group III analysis?
    Refer to application of Solubility product from ionic equilibrium Chapter
    (class XI)
    30. Why is it necessary to boil off hydrogen sulphide gas before group III
    analysis? Refer to application of Solubility product from ionic equilibrium
    Chapter (class XI)
    31. Black ppt in group IV indicates which cations?
    Nickel
    32.Why do we get a red ppt. in Fehling’s test?
    Refer to text (carbonyl compounds)

    33.Why do we get a shining mirror in Tollen’s test?


    Refer to text (carbonyl compounds)
    34.Name some reducing and non-reducing sugars
    Refer to text (carbohydrates)
    35.How will you distinguish between sucrose and glucose?
    Refer to text (carbohydrates)
    36.What is the role of tartarate ions in Fehling’s reagent?
    . It acts as complexing agent and prevents the precipitation of copper (II)
    hydroxide.
    37.What is the role of citrate ions in Benedict’s solution?
    . It acts as complexing agent and prevents the precipitation of copper (II)
    hydroxide.
    38.Explain why does fructose reduce Fehling’s solution and Tollen’s reagent
    inspite of the presence of ketonic group?
    In alkaline medium fructose rearranges to glucose and the two are
    equilibrium with each other
    39.What are Fehling A and Fehling B solutions?
    Refer to text (carbonyl compounds).
    40. Name a reagent used to detect carbonyl group in a compound.

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