Dow Americas Technical Manual
Dow Americas Technical Manual
Dow Americas Technical Manual
Dow Americas
Technical Manual
Dow Americas Technical Manual
Table of Contents
Introduction .............................................................................................................................................................. 3
Technical Information Center .............................................................................................................................. 3
Product Offering ....................................................................................................................................................... 4
Structural Glazing Sealants ................................................................................................................................. 4
Weatherproofing Sealants.................................................................................................................................... 4
Primers................................................................................................................................................................. 6
Building Sealant Recommendations and Surface Preparation Guide for Weatherseal Applications .................. 7
Silicone Structural Glazing..................................................................................................................................... 10
Introduction ....................................................................................................................................................... 10
Structural Joint Design ...................................................................................................................................... 10
Structural Bite .................................................................................................................................................... 11
Deadload ............................................................................................................................................................ 12
Glueline Thickness ............................................................................................................................................ 13
Structural Silicone Used in Shear ...................................................................................................................... 15
Structural Silicone Used in Seismic Applications ............................................................................................. 15
Splice Joints in Curtainwalls ............................................................................................................................. 16
Structural Glazing Guidelines ........................................................................................................................... 18
Substrate Suitability........................................................................................................................................... 18
Back-Painted Glass ............................................................................................................................................ 20
Project Review Services .................................................................................................................................... 21
Product Recommendations ................................................................................................................................ 21
Classification of Silicone Structural Glazing .................................................................................................... 23
Application Methods for Structural Glazing Systems ....................................................................................... 24
Surface Preparation and Sealant Application .................................................................................................... 27
Replacement and Remedial Glazing.................................................................................................................. 31
Quality Assurance – Structural Applications .................................................................................................... 32
Alternate Quality Control Tests......................................................................................................................... 44
Documentation – Quality Assurance and Warranty .......................................................................................... 45
Weatherproofing ..................................................................................................................................................... 53
Introduction ....................................................................................................................................................... 53
Joint Movement ................................................................................................................................................. 53
Joint Types......................................................................................................................................................... 55
Joint Design ....................................................................................................................................................... 56
Moving Joint Considerations ............................................................................................................................. 56
Joint Movement in Shear ................................................................................................................................... 57
Movement During Cure ..................................................................................................................................... 58
Backer Materials ................................................................................................................................................ 59
Hydrophobic Effects .......................................................................................................................................... 59
EIFS Considerations for Design and Specification ........................................................................................... 60
Weatherseal Design Examples .......................................................................................................................... 61
Weatherproofing Joints: Surface Preparation and Sealant Application............................................................. 68
Removal and Replacement of Existing Weatherseals ....................................................................................... 72
Sealant Interaction Considerations .................................................................................................................... 75
Quality Assurance – General ............................................................................................................................. 75
Documentation – Quality Assurance and Warranty .......................................................................................... 79
Appendix A: Cure Inhibition of DOWSIL™ 790 Silicone Building Sealant ........................................................ 84
Appendix B: Use of DOWSIL™ Sealants with Weathered Lock-Strip Gasket Systems ...................................... 86
Appendix C: Winter/Summer Considerations ........................................................................................................ 87
2
Dow Americas Technical Manual
Introduction
This manual is intended to give guidance on proper application procedures and assist in the development
of a quality assurance program for the application of DOWSIL™ silicone sealants for structural and
weathersealing systems.
As construction projects vary in many aspects, such as design, customer requirements and environment,
this manual cannot be considered a comprehensive quality assurance program for all situations.
Any review, recommendation or statement made on behalf of Dow relating to an engineering design,
architectural drawing, product formulation, end-use specification or similar document is limited to the
knowledge of product properties as determined by laboratory testing of material produced by Dow. Any
comments or suggestions relating to any subject other than such product properties are offered only to
call to the attention of the engineer, architect, formulator, end-user or other person considerations that
may be relevant in his/her independent evaluation and determination of the appropriateness of such
design, drawing, specifications, document or formula.
Dow assumes no responsibility for the comments or suggestions relative to subjects other than such
product properties and expressly disclaims any warranty or responsibilities for them.
Telephone:
+1 800 346 9882 (press #1 on menu)
E-mail:
construction@dow.com
3
Product Offering
Structural Glazing Sealants
Dow has a full line of high-performance silicone structural sealants. Following is a brief summary of
each DOWSIL™ brand product offered for structural glazing applications. These sealants should be
selected based upon the unique properties that each has for specific applications. Specific product
information, such as physical properties, application and limitations, can be found in data sheets
available at consumer.dow.com/construction.
Weatherproofing Sealants
Dow has a full line of high-performance weatherproofing sealants. Following is a brief summary of each
DOWSIL™ product offered for weatherproofing applications. These sealants should be selected based
upon the unique properties that each has for specific applications. Specific product information, such as
physical properties, application and limitations, can be found in data sheets available at
consumer.dow.com/construction.
4
DOWSIL™ 790 Silicone Building Sealant
DOWSIL™ 790 Silicone Building Sealant is a one-part, low modulus, neutral-curing silicone
sealant for use in high-movement weathersealing applications. DOWSIL™ 790 Silicone Building
Sealant has excellent primerless adhesion to concrete and most porous substrates. Available in a wide
variety of colors.
DOWSIL™ 123 Silicone Seal and DOWSIL™ Silicone Seal Custom Designs H.C.
DOWSIL™ 123 Silicone Seal is a preformed, low modulus silicone extrusion that can be used as a
bridge joint in a variety of applications, including restoration of failed sealant joints.
DOWSIL™ 123 Silicone Seal HC is a custom extrusion or mold made of higher durometer silicone
rubber used in custom applications. Widths from 1" (25 mm) to 12" (300 mm) and custom shapes are
available in a wide variety of colors and textures.
DOWSIL™ 795 Silicone Building Sealant, DOWSIL™ 791 Silicone Weatherproofing Sealant,
DOWSIL™ 756 SMS Building Sealant or DOWSIL™ 758 Silicone Weather Barrier Sealant may be
used as an adhesive.
For more information, see the EIFS Restoration Guide, Form No. 62-510.
5
DOWSIL™ Parking Structure Sealants
DOWSIL™ NS, SL and FC Parking Structure Sealants are low modulus, neutral-curing silicone sealants
for use in vertical and horizontal joints in parking structures and stadiums. DOWSIL™ NS Parking
Structure Sealant is a one-part, non-sag sealant for vertical or horizontal joints. DOWSIL™ SL Parking
Structure Sealant is a one-part, self-leveling sealant for horizontal joints. DOWSIL™ FC Parking
Structure Sealant is a two-part, fast-curing sealant for dynamic moving horizontal expansion joints.
Available in gray.
For more information, see the Parking Structure Sealants Installation Guide, Form No. 62-481.
Primers
Dow has a full line of high-performance primers for sealants. Primers are used to enhance adhesion of
sealants to specific substrates.
DOWSIL™ Primer-C OS
DOWSIL™ Primer-C OS is a one-part, low VOC, film-forming primer for use with DOWSIL™
sealants on painted and plastic surfaces to promote rapid adhesion. The primer features a
unique fluorescent feature using a UV flashlight (365 nm wavelength) to identify areas where primer
was applied.
6
Building Sealant Recommendations and Surface Preparation Guide
for Weatherseal Applications
Weatherseal
Dow has a full line of high-performance primers for sealants. Primers are used to enhance adhesion.
DOWSIL™ 791
DOWSIL™ 790 DOWSIL™ 795
DOWSIL™ 756 SMS Silicone
Silicone Building Silicone Building
Building Sealant Weatherproofing
Sealant1 Sealant
Sealant
Substrate Surface Prep
Concrete and Masonry
Brick Limited Data/Field Test No Primer 1200 OS/Primer P Primer P
Concrete Field Test No Primer 1200 OS/Primer P Primer P
Mortar Primer P No Primer Primer P Primer P
EIFS2
All Manufacturers3 Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test
Stone
Granite No Primer No Primer Limited Data/Field Test 1200 OS/Primer P
Travertine Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test
Marble4 1200 OS/Primer P Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test
Limestone8 1200 OS/Primer P Limited Data/Field Test Limited Data/Field Test Primer P
(Natural Stone)
Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test Primer P
Sandstone8
Paints
Acrylic Latex Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test
Duracron No Primer Limited Data/Field Test No Primer 1200 OS/Primer P
Polyester Powder
Limited Data/Field Test 1200 OS No Primer No Primer
Coating7
Polyurethane Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test
Polyvinyl Chloride
Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test
(PVC)
Fluoropolymer
Kynar No Primer Limited Data/Field Test No Primer Primer-C OS
Duranar No Primer Limited Data/Field Test No Primer Primer-C OS
Duranar Sunstorm Limited Data/Field Test Limited Data/Field Test No Primer Primer-C OS
Fluropon Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test Primer-C OS
7
DOWSIL™ 791
DOWSIL™ 790 DOWSIL™ 795
DOWSIL™ 756 SMS Silicone
Silicone Building Silicone Building
Building Sealant Weatherproofing
Sealant1 Sealant
Sealant
Substrate Surface Prep
Metals
Aluminum – Chromate
No Primer Limited Data/Field Test No Primer No Primer
Conversion, Alodine
Aluminum – Mill Finish No Primer 1200 OS 1200 OS 1200 OS
Aluminum – Anodized No Primer 1200 OS No Primer No Primer
Copper Do Not Use Do Not Use No Primer No Primer
Lead Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test
Glass6
Coated Glass No Primer 1200 OS No Primer No Primer
Clear Glass No Primer No Primer No Primer No Primer
Steel
Red Lead Primer Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test
Weathered Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test
Stainless Limited Data/Field Test Limited Data/Field Test 1200 OS 1200 OS
Galvanized No Primer 1200 OS No Primer 1200 OS/Primer P
Cold Rolled Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test Limited Data/Field Test
Plastics
PVC Limited Data/Field Test Limited Data/Field Test 1200 OS/Primer P No Primer
Acrylic Limited Data/Field Test Do Not Use Limited Data/Field Test Limited Data/Field Test
Polycarbonate Do Not Use Do Not Use Limited Data/Field Test Limited Data/Field Test
Key: 1200 OS: DOWSIL™ 1200 OS Primer; Primer-C OS: DOWSIL™ Primer-C OS; Primer P: DOWSIL™ Construction Primer P.
Dow must test all materials for adhesion in structural applications.
Field adhesion tests must be performed at the jobsite to verify sealant adhesion.
1
When using a primer with DOWSIL™ 790 Silicone Building Sealant, apply the primer before installing backer rod and allow the primer to dry. Cold
weather and porous surfaces require additional drying time.
2
Do not apply sealant to EIFS finish coat unless approved by EIFS manufacturer.
3
Cleaning procedures for EIFS systems should be followed (page 73).
4
The extremely porous nature of some marble, particularly white marble, can contribute to the potential for fluid migration into this substrate. Contact a
Dow Specialist when working with marble.
5
Laminated glass with polyvinyl buyvol (PVB) interlayer may delaminate up to 1/4" at the edges when in contact with a sealant.
6
Do not use DOWSIL™ 790 Silicone Building Sealant on copper sputter coated glass.
7
See Organic Solvent Usage in this Dow Americas Technical Manual (page 69) for comment.
8
Some limestone and other porous stone substrates contain iron and other impurities that can interact with DOWSIL™ 756 SMS Building Sealant, causing
discoloration of the sealant and/or substrate. Prior to use, DOWSIL™ 756 SMS Building Sealant should be tested for compatibility with these substrates
using water immersion.
This surface preparation guide is intended to aid in proper selection of surface preparation techniques and primers, if necessary, to gain adhesion that meets
Dow;s requirements. The suggestions in this guide are not blanket-approval recommendations; Dow requires all surface prep recommendations in this guide
be verified by field or shop adhesion testing and documented prior to starting the project for each substrate/sealant combination. Failure to verify and
document adhesion results may result in adhesion loss that is not covered by the Dow Warranty. Recommendations in this guide have been shown to be the
best overall recommendations but do not cover every substrate for each material type or finish listed in this guide. Additionally, substrate manufacturers
should be contacted to obtain recommendations for proper cleaning solvents for use with their materials. The entire Weatherproofing section of this manual
should be read and understood before proceeding with the evaluations. The following sections must be followed to verify and document adhesion:
8
Structural
All structural applications must be tested by the Dow test lab.
Key: 1200 OS: DOWSIL™ 1200 OS Primer; Primer-C OS: DOWSIL™ Primer-C OS.
Dow must test all materials for adhesion in structural applications.
Field adhesion tests must be performed at the shop or jobsite to verify sealant adhesion.
5
Laminated glass with polyvinyl buyvol (PVB) interlayer may delaminate up to 1/4" at the edges when in contact with a sealant.
7
See Organic Solvent Usage in this Dow Americas Technical Manual (page 29) for comment.
This surface preparation guide is intended to aid in proper selection of surface preparation techniques and primers, if necessary, to gain adhesion that meets
Dow’s requirements. The suggestions in this guide are not blanket-approval recommendations; Dow requires all surface prep recommendations in this guide
be verified by field or shop adhesion testing and documented prior to starting the project for each substrate/sealant combination. Failure to verify and
document adhesion results may result in adhesion loss that is not covered by the Dow Warranty. Recommendations in this guide have been shown to be the
best overall recommendations but do not cover every substrate for each material type or finish listed in this guide. Additionally, substrate manufacturers
should be contacted to obtain recommendations for proper cleaning solvents for use with their materials. The entire Weatherproofing section of this manual
should be read and understood before proceeding with the evaluations. The following sections must be followed to verify and document adhesion:
9
Silicone Structural Glazing
Introduction
Silicone structural glazing utilizes a high-performance silicone sealant to attach glass, metal or other
panel materials to a metal frame in lieu of gaskets and mechanical attachments. The windload stresses
are transferred through the structural silicone sealant to the structure of the building. The structural
silicone sealant must maintain its adhesive and cohesive properties in order to support the panels
under windload.
Only silicone sealants are suitable for use in structural glazing applications. A considerable amount of
time has been spent developing and testing silicone sealants to meet the needs of structural glazing
applications. Whenever a silicone sealant is used to structurally attach panels, a comprehensive
quality control procedure must be established to ensure the smooth, efficient, trouble-free completion
of the project.
Specific quality control procedures must be followed on all structural glazing projects in order to obtain
a Dow Structural Warranty.
10
Structural Glazing Design
Structural Bite
Structural bite is the minimum width or contact surface of the silicone sealant on both the panel and
the frame. The structural bite requirement is directly proportional to the windload on the building and
the size of the glass. The higher the design windload and the larger the size of the glass, the greater the
structural bite requirement. The structural bite must be sized appropriately to allow the windload on
the glass or panel to be transferred to the structure. The structural bite for windload (live load) is
calculated using the specified windload, glass or panel dimension and sealant design strength of
20 psi (14,000 kg/m2 or 138 kPa).
For example, a 4' x 8' lite of glass, exposed to a 60 psf windload, requires a silicone bite of 1/2". Always
round up to the nearest 1/16" and never round down.
For example, a 1219 mm x 2438 mm lite of glass, exposed to a 290 kg/m2 windload, requires a silicone
bite of 13 mm. Always round up to the nearest millimeter and never round down.
For example, a 1219 mm x 2438 mm lite of glass, exposed to a 3.5 kPa windload, requires a silicone bite
of 16 mm. Always round up to the nearest millimeter and never round down.
11
Deadload
In unsupported deadload designs, the weight of the panel places constant load upon the sealant.
DOWSIL™ brand structural sealants can support the weight of the panel or glass when used within
the following guidelines:
• For DOWSIL™ 795 Silicone Building Sealant, DOWSIL™ 983 Structural Glazing Sealant,
DOWSIL™ 995 Silicone Structural Sealant and DOWSIL™ 121 Structural Glazing Sealant,
the allowable deadload design strength is 1 psi or 6.9 kPa.
• The weight of the panel divided by the total silicone contact area must not exceed 1 psi, the
deadload design strength of the sealant. Insulating glass unit manufacturers require deadload
support for their insulating glass units.
weight of glass in lb
Bite =
sealant contact length (inches) * sealant design strength (1 psi)
For example, a 4' by 8' lite of monolithic glass at a weight of 3.3 psf will have a weight of 105.6 lb and a
glass perimeter of 288". Based on a 1 psi deadload design strength, a bite of 3/8" is required.
weight of glass in N
Bite (mm) =
sealant contact length (m) * sealant design strength (6.9 kPa)
Sloped Glazing
Sloped glazing is a form of structural glazing used in skylights and similar non-vertical applications.
Conventional structural glazing guidelines can be followed for sloped glazing with modifications to the
windload accounting for the slope. The structural glazing calculation takes into account the weight of the
glass counteracting the negative design windload on the building. The flatter the slope of the glazing
system, the greater the reduction in the windload effect on the structural joint.
For many slope-glazed systems, the glass sets on a gasket and the structural joint is installed to the edge
of the glass. The sealant in this application acts as both the structural seal and the weatherseal. Dow
permits the use of its sealants in this manner provided that the joint maintains an aspect ratio of 1:1
where the depth of the sealant is equal to or greater than the width of the joint opening. The structural
bite in this design is the depth of the joint along the edge of the glass. The sealant in this design must be
structurally attached to a fin that can support the structural load on the glass. Glass tolerances must be
considered.
Glass that is sloped outward from vertical imposes a deadload upon the glazing that must be added to the
windload, even when there is contact with setting blocks. If the outward slope is greater than 15 degrees
from vertical, it is prudent to perform your calculations as if the entire weight of the glass is supported
by the silicone. If there are no setting blocks, the entire lite is supported by the structural silicone. The
design load on the silicone for live and deadload must be determined and the bite dimension sized
appropriately. For these designs, contact Dow at consumer.dow.com/construction.
Outward Sloping:
0.5 * short span length (ft) * [windload (psf) + sine(β) * lite deadload (psf)]
Bite (in) =
12 in/ft * sealant design strength (20 psi)
Glueline Thickness
A minimum glueline of 1/4" (6.4 mm) is required. Consideration should be given to increase the
glueline based on type of sealant used as well as movement due to thermal effects of the panel or lite.
For application purposes, the glueline should be sufficient to allow proper fill of the structural joint and
demonstrated in deglaze activities. For one part sealants, a bite-to-glueline ratio should be maintained at
3:1 or less to enable reasonable curing to the full depth of joint. One part sealants cure via reaction from
moisture in the air, so deep section joints, 3/4” (19 mm) or greater, may take several months to fully cure
in depth. Use of two part sealants allow for greater ratios of bite-to-glueline ratios (such as projects in
13
high velocity hurricane zones with excessive windloads) as long as the joint can be adequately filled
and that the parts are properly mixed to ensure proper reaction for property formation.
All panels that are structurally glazed undergo repeated expansion and contraction due to variation in
temperature. Glueline thickness must be properly designed to accommodate these movements. The
thermal movement can be calculated for any panel or framing member if the length of the material,
material type (e.g., glass, aluminum) and coefficient of thermal expansion (CTE) are known.
Movement (inches) = panel length (inches) * CTE (inches/inches/ºF) * temperature change (ºF)
For example, for a 4' by 8' high lite of glass fixed at the sill and a temperature change of 180ºF, glass
with a CTE of 5.1 x 10–6 will show movement of 0.088". Aluminum with a CTE of 13.2 x 10–6 will
move 0.228". Differential movement between the glass and aluminum will be 0.228" minus 0.088",
which is 0.14".
Movement (mm) = panel length (mm) * CTE (mm/mm/ºC) * temperature change (ºC)
For example, for a 1219 mm by 2438 mm high lite of glass fixed at the sill and a temperature change
of 82ºC, glass with a CTE of 9.2 x 10-6 will show movement of 1.84 mm. Aluminum with a CTE of
23.8 x 10-6 will move 4.76 mm. Differential movement between the glass and aluminum will be
4.76 mm minus 1.84, which is 2.92 mm.
The dimension of glueline required (a) for the differential movement (b) can be calculated using the
Pythagorean Theorem. Likewise, the allowable movement (b) for a particular glueline dimension (a) can
also be calculated. The new glueline thickness (c) is limited by the movement capability of the sealant in
shear in a structural joint configuration.
14
For the example discussed above where differential movement of 0.14" (b) is expected, and the sealant
has an original glueline thickness of 0.25" (a), the sealant will elongate to a new glueline thickness of
0.287" (c). Extension of the sealant from 0.25" to 0.287" will be 14.8%.
For DOWSIL™ 995 Silicone Structural Sealant, DOWSIL™ 795 Silicone Building Sealant,
DOWSIL™ 983 Structural Glazing Sealant and DOWSIL™ 121 Structural Glazing Sealant,
maximum extension from thermal expansion is 15% in any structural silicone joint. The lower
allowable movement capability in structural joints is due to the joint design, where the joint width,
or glueline, is less than the joint depth, or structural bite.
NOTE: Coefficients of Thermal Expansion Values for common building materials are available in the
Weatherproofing section of this technical manual.
The direction of the panel movement would also need to be considered. Consider whether thermal
movement will take place in one direction due to the setting blocks preventing any downward movement
of the glass panel or in the case of an unsupported system where the thermal movement can be taken by
the glass in both directions. This will need to be taken into consideration when designing the sealant
joint dimensions.
The modulus of the structural silicone in shear is lower than in tension (consider the calculations through
the Pythagorean Theorem from the Glueline Thickness section of this manual). Therefore, combinations
of shear and tension loading cannot be added without understanding the stress-strain relationship of each
joint. Contact Dow Technical Service for more information.
For a case study regarding the use of structural sealants in an earthquake, please refer to DOWSIL™
structural glazing sealants help the tallest building in Chile withstand glass breakage during a magnitude
8.8 earthquake, Form No. 63-1216.
Broker, K. A., Fisher, S., and Memari, A. M., “Seismic Racking Test Evaluation of Silicone Used in
15
a 4-Sided Structural Sealant Glazed Curtain Wall System,” J. ASTM Int., Vol. 9, No. 3, 2012. Paper ID
JAI104144
Memari, A.M., Fisher, S., Krumenacker, C., Broker, K.A., and Modrich, R.U., “Evaluation of the
Structural Sealant Glazing Curtain-Wall System for a Hospital Building,” J. ASTM Int., Vol 9, No. 4,
2012. Paper ID JAI104143
Zarghamee, M. S., Schwartz, T. A., and Gladstone, M., “Seismic Behavior of Structural Silicone
Glazing,” Science and Technology of Building Seals, Sealants, Glazing and Waterproofing, Vol. 6,
ASTM STP 1286, J. C. Myers, ed., American Society for Testing and Materials, Philadelphia, PA,
1996, pp. 46−59.
It is best to avoid splice joints within a structural joint. Placing 13' to 16' (4 m to 5 m) of aluminum
frame thermal movement and live load deflection of the floor into the shearing of a 1/4" (6 mm) wide
structural silicone joint will: 1) exceed the design stress of the silicone, causing fatigue; 2) place
excessive loading onto glass, causing possible failure; or 3) cause premature fogging of the insulating
glass unit.
If splice joints cannot be avoided within a structural silicone joint due to the requirements of field-
applied structural silicone in a stick system, then the splice joint should be applied to within 1" (25 mm)
of the head of a piece of glass. If silicone failure occurs due to excessive joint movement, a minimum of
forces will be placed onto the glass due to the placement.
16
Best Design Better Design Poor Design
17
Structural Glazing Guidelines
Following are general guidelines that should be followed for all structural glazing applications. All
exceptions must be handled on a project-specific basis and documented in writing by the Dow Technical
Service Representative.
NOTE: Closing off the joint opening with a weatherseal immediately after application of an exterior
applied structural joint will drastically slow down the cure of the structural sealant.
All exceptions to these guidelines must be reviewed and approved by a Dow Technical Service
Representative.
Substrate Suitability
Dow project services include adhesion and compatibility testing according to ASTM standards. These
methods do not encompass any substrate approval; therefore, adhesion or compatibility reports from
Dow should not be interpreted as substrate approvals.
Dow does recognize typical substrates for use in silicone structural glazing based on historical and
industry practices, (e.g., anodized aluminum). Dow will reject the use of DOWSIL™ brand structural
sealants in designs with non-typical substrates without further confirmation of substrate suitability and
durability.
Where non-typical substrates are specified, a system design professional should be consulted regarding
material suitability for structural glazing based on feedback from industry guidelines and substrate
manufacturer input. Discussion will need to take place on its durability prior to its acceptance and use in
structural applications. Dow may require the customer provide independent confirmation of a substrate’s
suitability.
18
irregularities is required. Some off-the-shelf extrusions may not be suitable for all structural glazing
applications. The width of the extrusion must be adequate to achieve the calculated minimum structural
bite with a suitable spacer attached.
Extruded mill finish aluminum is not an appropriate surface for structural silicone application due to
poor adhesion. The graphite lubricant used in the extrusion process causes a highly variable surface to
which adhesion is not always predictable. Therefore, aluminum must have a minimum of an alodine
finish for structural glazing applications. Anodizing and thermal set paints such as fluorocarbon and
polyester powder coat are also suitable aluminum finishes. In addition, high-grade stainless steel (316)
can also be specified, as verified by past adhesion tests and actual projects.
Carbon steel, painted steel and galvanized steel are generally not appropriate surfaces for structural
silicone glazing due to substrate durability concerns when exposed to corrosive agents. Exceptions can
be made based on the merit of design and exposures. Examples may include steel components painted
with high-performance industrial-grade coatings or use of structural sealants to adhere galvanized steel
backpans in spandrel conditions to secure an insulated cavity where panels are not exposed to exterior
elements. Acceptable conditions must be approved, in writing, upon testing and review by Dow, the
substrate manufacturer and the coating manufacturer.
Masonry:
Masonry and cementitious substrates are typically not suitable structural members for structural silicone
attachment. The alkalinity of the substrate can be a variable in the durability and longevity of adhesion
necessary for structural silicone. When structural attachment to masonry is required, mechanical anchors
should be installed into the masonry to anchor a metal plate, and the structural silicone should then be
bonded to the metal. The metal must be compatible with masonry and have a high-performance finish.
Insulating Glass
Insulating glass units are widely used in structurally glazed facades to improve the thermal performance
of a facade. By using insulating glass units, architects and specifiers can increase the areas of glass that
can be used on a facade without compromising the thermal performance of the building. This allows
the designer much greater scope when designing a building facade using the latest building materials
and concepts.
When using IG units in any structurally glazed facade, specifically developed DOWSIL™ silicone IG
sealants should be used. These sealants are resistant to attack from ultraviolet light that provides a
structural seal that bonds the outer glass of the IG unit to the inner glass, thereby providing a system that
is structurally bonded from the outer glass of the IG unit through to the building structure. Silicone
sealants are the only products that are specified in national and international standards for this
application. Not only does the silicone IG sealant provide structural integrity for the IG unit, it also
firmly holds the two glass elements together and prevents damage to the primary PIB (polyisobutylene)
seal, which controls the ingress of moisture into the unit. DOWSIL™ products have a proven track
record in this application.
Back-Painted Glass
Back-painted glass is not an appropriate substrate for silicone structural glazing because of substrate
durability concerns and adhesion of the coating to the glass. Adhesion testing completed by Dow only
addresses adhesion of the sealant to its direct substrate and does not encompass adhesion of the coating
to the glass.
• Typically, back-painted glass has been used in interior applications that offered additional
mechanical support. Dow can complete adhesion testing in order to help you make your sealant
choice for non-structural applications.
• Additionally, compatibility of the sealant to the coating should be addressed by the coating
manufacturer. Dow is not responsible for the adhesion of the coating to the glass and any effect
the sealant may have on this adhesion.
• Back-painted glass in which the edges have been deleted or not coated along the structural
sealant bondline may be tested for structural sealant adhesion and be considered a clear glass
substrate.
Based on historical testing and success, most silicone setting blocks, composed of 100% silicone, are
found to be compatible for full contact with structural silicones. 100% silicone setting blocks are thereby
our primary recommendation for 4-sided SSG applications.
Other materials such as EPDM, neoprene, SCR (Silicone Compatible Rubber – an EPDM-based
material) and other similar organic materials may cause discoloration of light-colored silicone sealants.
When discoloration is noted, per the criteria in ASTM C1401 Section 34.3, these materials will not be
approved for full contact in structural glazing applications.
When using these materials in structural glazing applications, light-colored or gray sealants
should not be used. When using gray DOWSIL™ 983 Structural Glazing Sealant, gray DOWSIL™ 121
Structural Glazing Sealant, gray DOWSIL™ 982 FS Insulating Glass Sealant and gray DOWSIL™ 982
Silicone Insulating Glass Sealant, 100% silicone accessory materials are recommended.
20
When using EPDM, neoprene, SCR (Silicone Compatible Rubber, an EPDM-based material) and other
similar organic materials for weatherseal applications, only dark-colored (black, charcoal or bronze –
NOT gray) silicone sealants will be recommended for contact with these organic extrusions. Where
discoloration is severe, even dark-colored silicone sealants may not be approved for weatherseal
applications, due to potential long-term adhesion loss.
When using insulating glass, the IG manufacturer should be contacted for specific recommendation of
setting blocks to ensure compatibility with the IG unit components (spacer, PIB, glass coatings, etc.).
NOTE: When applying a weatherseal over the silicone setting block, a 1/8" minimum sealant thickness
is required. See the figure on page 10.
Product Recommendations
After reviewing project drawings and specifications and having performed laboratory testing,
Dow will assist in the selection of the correct DOWSIL™ sealant/primer and/or surface preparation
for the specific application.
Print Review
Guidelines for silicone structural glazing details are provided in this section.
Dow must review all structural details before any approval or acceptance is given. Typical horizontal
and vertical details, plus any non-typical details, should be submitted for review. Also provide
elevations indicating glass dimensions and design windload values for the building. Dow has found that
a few underlying principles are critical to consider in virtually all joint designs using silicone sealants.
Dow will review joints for compliance with these underlying design principles, provide suggestions or
changes, and/or identify limitations of the designs. It will also allow Dow’s technical staff to check that
all components that will need to be tested as part of the project review have been supplied. This will
include bonding substrates, spacers, setting blocks, gaskets, etc.
Adhesion Testing
Dow will evaluate the adhesion of our product to materials representative of those to be used on the job
(i.e., glass, metal, masonry, composites, etc.) using a modified ASTM C794 peel adhesion test. All
samples submitted for testing should be a minimum of 8" (200 mm) in length. For example, for
aluminum extrusions, supply one 8" (200 mm) sample for each sealant to be tested. For glass, one
standard 12" by 12" (300 mm by 300 mm) sample is sufficient. Upon completion of this testing, Dow
will forward in writing product recommendation, surface preparation and primer recommendation (if
needed). Testing takes approximately four weeks from receipt of samples.
21
Compatibility Testing
Chemically incompatible glazing accessories (gaskets, spacers, setting blocks, etc.) can lead to sealant
discoloration and/or loss of sealant adhesion to the substrate. To ensure a product’s suitability, Dow tests
the compatibility of job site representative accessory materials with its silicone sealants using ASTM
C1087. For each sealant to be tested, supply 4" (100 mm) minimum length of the gasket, spacer or
setting block. Results of the compatibility test will be forwarded in writing. Testing takes approximately
four weeks from receipt of samples.
Silicone sealant may yellow when in contact with EPDM, neoprene, bitumen, asphalt and other
organic-based membranes, coatings and gaskets. Dark-colored sealants will typically mask the
yellowing. ASTM C1087 compatibility testing will confirm the degree of yellowing. Testing may be
performed with questionable materials upon request. See the comment below discussing the application
of sealants to membranes.
Upon completion of testing, approvals for full contact or incidental contact will be provided.
Incidental contact is defined as the contact between the structural sealant joint and complementary
material used in the construction of structurally glazed systems where the contact area is no greater
than the cross-sectional area of the gasket or structural joint or the face width of the setting block in
contact with the structural joint. An incidental contact test result for gaskets implies use of the sealant
should be for 1- and 2-sided silicone structurally glazed applications in which the sealant contacts the
gasket at an intersection.
Approval for full contact means the sealant can be in contact with the accessory component for any
contact area greater than the component’s cross-sectional area. Full contact approval implies the use of
the sealant is acceptable for any application of the sealant being in contact with a gasket for the length of
a glazing leg, which is typical of a 4-sided silicone structural glazing design.
Some studies have shown that the addition of DOWSIL™ Construction Primer P will significantly
reduce or eliminate the yellowing or discoloration because it is a film-forming barrier. However, this
must be verified in field testing on a project-specific basis.
Non-Stain Testing
If natural stone is being used on the project, Dow can test and evaluate the performance of its sealants to
determine if fluid in the sealant has the potential to migrate into porous substrates such as granite,
marble, travertine and limestone. Job site representative samples of the stone need to be tested using a
modified ASTM C1248 procedure. For each stone type and sealant to be tested, supply two samples of
the dimension 1" by 3" (25 mm by 75 mm) the thickness of the stone. Larger samples can be cut for
testing. Testing takes approximately six weeks from receipt of samples.
Mock Ups
Mock-up Testing Curing Minimums for Structural Load Testing – The structural sealant must be fully
cured and adhered to the substrates prior to running structural load testing. With one-part structural
sealants (DOWSIL™ 795 Silicone Building Sealant or DOWSIL™ 995 Silicone Structural Sealant), it
22
is best to leave the weatherseal open until complete cure and adhesion occurs for “exterior applied”
designs. Closing off the joint opening with a weatherseal immediately will drastically slow down the
cure of the structural sealant if shot and applied from the exterior.
A one-part sealant can be applied from the interior at the same time the weatherseal is applied. This type
of application is illustrated in the Joint Composition diagram shown previously in the Structural Joint
Design section of this manual. A 12" “mini mock-up” sample can be made and destructively tested for
complete cure and adhesion.
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4-Sided Structural Glazing
Glass is supported on all 4 sides with structural silicone. Structural silicone is used for bonding all 4
edges of the glass to the support frame, and the deadload can either be supported mechanically by a fin
and setting block or by the structural silicone. It is generally recommended that 4-sided structural
glazing be performed in-shop.
NOTE: Special attention to cleaning and sealant application is required under the following conditions:
• Occurrence of severe wind during application may cause undue stress on the curing structural
silicone
• Extremely high or low temperatures – optimum application temperature range is 10-35°C (50-
95°F). For applications below 10°C (50°F), the potential for dew point and frost must be
considered. For applications in higher temperatures, sealant must not be applied when substrate
temperatures are in excess of 50°C (120°F)
• Rain-contaminated joints – remove all moisture from the substrate surface, then solvent clean,
prior to glazing
Insulating glass units can also be installed using bolted glass technology including systems only drilling
through the interior lite of an insulating glass unit. In this system, a high-performance silicone insulating
glass sealant should be used to produce an edge seal of the insulating glass units to secure the exterior
lite to the assembly while maintaining the integrity of the primary PIB seal to protect the interior gas
space of the insulating glass. Silicones are used due to their excellent resistance to ultraviolet light,
which would attack organic-based sealants. In this design, the internal glass is bolted back to the main
structure, while the external glass is structurally bonded to the inner glass around its perimeter.
One of the latest developments in structural glass design is the elimination of the bolted system and
the need to drill the glass by using structurally bonded patch plates as an alternative. Dow’s range of
structural adhesive sealants enables the designer to do away with the cost of drilling holes in glass
and the use of very expensive stainless steel spider systems. This results in a system that has a reduced
cost of manufacture, increased visibility and improved aesthetics. For more information, please refer
to literature regarding Transparent Silicone Structural Adhesive (TSSA) available at
consumer.dow.com/CrystalClearBonding.
Structural glass systems are often referred to as structural glazing, which is often confused with
structural silicone glazing, as both techniques use this generic term. Therefore, architects and specifiers
should be sure which system is being offered.
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Total Vision Systems (Fin Glazing)
Total vision or fin glazing is a system that is used to maximize the area of glass at the front of the
building, reducing the visible mechanical fixings and increasing the unobstructed vision area of the
facade. Total vision glazing is a 2-sided structural glazing system in which the glass is normally
mechanically fixed at head and sill and the vertical edges are structurally attached to glass fins or
mullions. The glass is bonded to the glass fin using DOWSIL™ structural silicone sealants. The
structure is then made watertight using DOWSIL™ weathersealing sealants. This technique is widely
used for lobbies, showrooms and racetracks where the unobstructed visibility is an advantage.
Certain materials, such as plastics, may have high coefficients of thermal expansion that may cause
undue stress on the structural silicone and/or bowing of the panels. Dow must review all designs,
whether glass or non-glass materials, where its sealants are used as structural adhesives.
Panel Stiffeners
For aluminum composite materials that are mechanically attached around the perimeter and the sealant
is used to attach an aluminum stiffener, Dow permits glueline thickness dimensions of less than 1/4"
(6 mm). In this application, there is a negligible amount of differential movement between the two
aluminum components, and shear stress on the sealant is minimal. A best practice is to use a spacer
material to establish a sealant joint, which can be controlled for width and thickness. Ensure use of
suitable sealant for these applications by following the project specification.
For bomb-blast mitigation glazing, the sealant must also anchor the laminated glass through an air blast
explosion. Dow does not approve bomb blast designs because of the intricate interactions between the
sealant, glazing and framing. Potential users should either test their system and have it approved, or
work with a bomb blast consultant who can review the design and determine the sealant requirements.
Dow can provide the consultant with either ASTM D412 Tensile or ASTM C1135 Tensile sealant
strength data for analysis.
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Both DOWSIL™ 983 Structural Glazing Sealant and DOWSIL™ 995 Silicone Structural
Sealant have the high strength and tear propagation properties required to pass either missile impact
or bomb blast test requirements. Numerous glazing systems have successfully passed both tests with
these two products.
Introduction
The Dow application procedures outlined in this manual describe the general requirements for installing
DOWSIL™ Silicone Building Sealants. By following these procedures closely, you will help ensure
good sealant performance. To be eligible to receive a Dow warranty, these procedures must be followed.
Since DOWSIL™ Silicone Building Sealants are applied in many different environments and situations,
these procedures are not intended to be a complete and comprehensive quality assurance program.
Following are the basic steps required for proper structural sealant joint preparation and
sealant installation:
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Substrate Cleaning Procedure
This section provides information on cleaning solvents and general cleaning procedures for porous and
non-porous substrates. One of the key requirements of good sealant adhesion is a clean surface. Proper
cleaning is accomplished through the use of the “two-cloth” cleaning method. Always confirm with the
supplier of each substrate that the cleaning procedures and solvents are compatible with their material.
Please be aware that certain aggressive solvents can adversely affect finishes such as polyester powder-
coated aluminum. Therefore, milder solvents such as IPA (isopropyl alcohol) or high quality white spirit
(greater than 98% pure) can be used without damaging the substrate surface. Check with the substrate
supplier for solvent compatibility with their materials.
Please follow the solvent manufacturer’s safe handling recommendations and local, state and national
regulations regarding solvent usage.
High pressure water blasting is an effective cleaning method, or a bristle brush with running water may
suffice. Porous materials may absorb water or solvents after cleaning or priming. Hence, water or
solvents used for cleaning must be allowed to evaporate completely before sealant is applied.
1. Pour or dispense an acceptable cleaning-grade solvent onto the cloth. A plastic (solvent-resistant)
squeeze bottle works best for organic cleaning solvents. Do not dip the cloth into the container of
solvent, as this will contaminate the cleaning agent.
2. Wipe vigorously to remove contaminants. Check the cloth to see if it has picked up
contaminants. Rotate the cloth to a clean area and re-wipe until no additional dirt is picked up.
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3. Immediately wipe the cleaned area with a separate clean, dry cloth before the solvent has
evaporated. This technique will allow dirt and contaminants suspended in the solvent to be lifted
and removed with the second dry cloth. Multiple cleanings may be required to adequately clean
a substrate.
Organic solvent must be removed with the dry cloth before the solvent evaporates or the cleaning
will be less effective. Some surfaces or weather conditions will allow a small amount of residual organic
solvent to remain. If this is the case, the surface must be allowed to dry before continuing with the
sealant installation.
1. Apply masking tape to the surfaces next to the joint to keep excess primer and sealant off areas
where they are not intended.
2. Ensure that primer is being utilized such that the container is not open to the atmosphere.
Alternatively, pour primer into a small, clean container and replace and tighten the cap on the
primer can to prevent exposure to atmospheric moisture that will contaminate the primer. Use
small amounts of primer in the separate container – for example, enough primer to last for 30–60
working minutes or less.
3. Depending on the substrate and job conditions, two different methods can be used to apply the
primer. The preferred application is to dip a clean, dry, lint-free cloth into the small container of
primer, or apply primer from container onto the cloth. Then gently wipe a thin film onto the
surface. For “hard-to-get-to” areas and rough surfaces, apply the primer in a thin film with a
clean brush. Caution: Over-priming with DOWSIL™ 1200 OS Primer can cause adhesion loss
between the sealant and the primer. If too much primer has been applied, a powdery, chalky,
dusty film will form on the surface. Excess primer should be removed by dusting the joint with a
clean, dry, lint-free cloth or a non-metallic bristle brush.
4. Allow the primer to dry until all the solvent evaporates. This typically takes 5 to 30 minutes,
depending upon the temperature and humidity.
5. Inspect the surface for dryness. If too much primer has been applied, a powdery, chalky, dusty
film will form on the surface. In this case, remove excess primer with a clean, dry, lint-free cloth
or a non-metallic bristle brush before applying sealant.
6. The surface is now ready for application of the sealant. Sealant must be applied the same day the
surfaces are primed. Any surfaces primed but not sealed on the same day must be covered to
prevent contamination or re-cleaned and re-primed before applying sealant.
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Keyway considerations: It is recommended to always use a flat surface for structural glazing. At times,
when additional structural bite is required, it may become necessary to use a keyway as part of the
structural bite. If use of a keyway becomes necessary, please follow these guidelines:
When a keyway is used as part of the glazing surface contributing to the structural sealant bite, the
sealant installation must be carried out as a separate step. The keyway must be cleaned, primed if
necessary, sealant installed and tooled as its own procedure prior to the remainder of the structural
sealant being installed. This is to ensure full joint fill and adhesion to a surface that is contributing to
structural bite.
1. To ensure an aesthetically pleasing job, masking tape should be used to keep excess sealant from
contacting adjacent areas where it is not intended.
2. Apply the sealant in a continuous operation using a caulking gun, pump or glazing table. A
positive pressure, adequate to fill the entire joint width, should be used. This can be
accomplished by “pushing” the sealant ahead of the application nozzle. Care must be taken to
ensure complete fill of the sealant cavity. This is critical, since the effectiveness of the silicone in
structural applications is largely dependent on the sealant bite (contact area).
3. Tool the sealant with firm pressure before a skin begins to form (typically 10 minutes). Tooling
forces the sealant against the spacer and the joint surfaces. Do not use liquid tooling aids such as
water, soap or alcohols. These materials may interfere with sealant cure and adhesion and create
aesthetic issues.
4. Remove the masking tape (if used) before the sealant skins over (within about 15 minutes
of tooling).
Setting Procedure
Many of the specific requirements of glazing are beyond the scope of this guide. For detailed
information, a guide such as the Glazing Association of North America (GANA) Glazing Manual
should be consulted. Some general rules to follow when using silicone sealant in glazing applications
are as follows:
1. Care must be taken to ensure that joint surfaces that have been prepared are not contaminated.
2. In some field glazing applications, the silicone may not be applied the same day the glass is set.
Joint preparation (cleaning and priming) must be accomplished immediately prior to applying the
silicone unless the environment can be proven to not contaminate the cleaned and primed
surface; or steps are taken to prevent contamination so that glazing can occur within 24 hours
after cleaning and priming.
3. Temporary fasteners or clips must be used to retain the structurally glazed lites or panels until the
silicone has fully cured. A two-sided adhesive tape, used as the structural spacer, may be
considered sufficient temporary support provided the tape manufacturer has approved the use of
their product for this application.
30
would also be used to check the adhesion of the sealant to the substrates. Full frame deglazes are also
used to determine time to full cure, plus to test adhesion and joint fill (structural bite).
Another consideration is the effects of temperature over the course of a large project. Full adhesion may
occur in 24 hours when the project starts in mid-summer, but may drift out to 48 hours as the
temperature decreases in winter. The silicone must not be stressed until full adhesion has developed. It is
preferable to allow horizontally glazed units to remain on the fabrication tables until full adhesion
develops, especially when no two-sided adhesive tape is used. (Two-sided adhesive tapes can be used to
prevent stressing of the sealant when moving and transferring units during the cure period.) Adhesion
testing should be carried out to confirm that full adhesion has been achieved. Once full adhesion is
verified, units may be moved in a more rigorous manner.
When multiple substrates are glazed on unitized panels, special attention must be given to the support
requirements of each substrate.
The specifics will vary from project to project. Always contact your Dow Representative for specific
advice. Following are some general guidelines regarding the silicone that should remain common to
most all projects.
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Replacement Glazing Due to Individual Unit Breakage
The following procedure assumes that a DOWSIL™ structural adhesive was originally used on the
project, and that the original recommendations are available to the contractor performing the repairs.
If this information is not available, contact your Dow Representative, who may need to determine
whether DOWSIL™ products have been used on the site.
1. Perform a field adhesion test to confirm the adhesion of the existing silicone to the substrates. If
excellent adhesion is not observed, contact your Dow Representative immediately.
2. Deglaze the area. Depending on the joint design, this may require specially designed tools or
piano wire to cut behind the silicone.
3. Cut away the silicone, leaving a thin film (approximately 0.02–0.04"/0.5-1 mm thick) of
adhesive on the frame. Do not damage the surface finish of the substrate. Or, completely remove
all sealant, but take care not to damage the substrate finish.
4. Clean the residual sealant with solvent using the “two-cloth” cleaning technique described
previously. If fresh sealant will be applied immediately after cutting the cured sealant, then
cleaning of the residual cured sealant may not be necessary.
5. Fresh sealant will adhere to cured sealant without primer. Primer may be necessary if sealant has
been completely removed.
6. The silicone may absorb some solvent. Allow this solvent to evaporate so the existing cured
sealant is completely dry before applying additional sealant.
7. Clean the new glass or panel and set in place. Install temporary fasteners. Mask the joint.
8. Fill the joint with a bead of fresh structural sealant. Refer to the Sealant Application Procedures
section of this manual.
9. After the sealant has fully cured, check that full adhesion has been achieved and then remove the
temporary fasteners.
NOTE: In some instances, the structural joint cannot be accessed once the glass has been set. In such
instances, the sealant can be applied directly to the frame and the glass set in place, compressing the
sealant in the joint. The joint must be filled in excess with sealant, and the glass must be set within 10
minutes or before the sealant begins to skin. Under-filled structural joints are workmanship issues. It is
the responsibility of the sealant applicator to ensure proper joint fill. Dow will review and comment
upon reglazing procedures.
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One-Part Sealants
The following procedure outlines a series of steps to ensure that the quality of the DOWSIL™ 995
Silicone Structural Sealant or DOWSIL™ 795 Silicone Building Sealant is adequate for structural
sealant applications.
DOWSIL™ 795 Silicone Building Sealant must be stored at temperatures below 27°C (80°F). The “use
by” date is clearly displayed on the product package.
Multi-Component Sealants
DOWSIL™ 983 Silicone Structural Glazing Sealant Catalyst, Initial Inspection – When opening a
new pail of catalyst, check for any clear fluid separation on the top. If present, this fluid should be
33
lightly remixed with a long spatula in a motion from bottom to top, similar to how a paint is remixed.
The remixing should take 1 to 2 minutes to complete for a homogeneous catalyst. Place the pail
immediately underneath the follower plate of the pail pump and bleed off any residual air according to
pump instructions. Do not leave opened for extended periods of time, because the catalyst will react
with air and moisture and start to form a cured crust. Pumps that sit idle for greater than 7 days should
have the pail of curing agent inspected for separation and remixed by the above method if separation
has occurred.
DOWSIL™ 983 Structural Glazing Sealant, Initial Inspection – Remove the top plastic disc prior to
placing underneath the follower plate of the drum pump and bleed off any residual air according to
pump instructions. There is no reason to remix the base. An opened drum of base alone will not cure but
may become dirty on the top surface.
Hence, it is recommended that DOWSIL™ 983 Structural Glazing Sealant be applied between
temperatures of 12 to 35°C (50 to 95°F). Variable adhesion properties have resulted when the
product was applied to curtainwall units in an unheated shop during the winter.
Drums of base and pails of catalyst should be stored indoors to maintain the temperature within the
materials. The packaged materials are normally transported in unheated trucks and will be cold in the
winter. Once received, the material should be brought indoors and warmed for a few days before using
to help maintain consistency of cure and adhesion times. Cold base and cold catalyst will cure slower
(even if the shop temperatures are warm), so the material should be allowed to equilibrate for
consistency of these properties. For each drop of 10°C, the reaction rate (cure, snap time, adhesion) is
decreased by approximately ½. It is not uncommon to see these properties drop during the winter from
typical properties seen in the summer. This change in initial properties will not affect the cured
performance of the sealant.
34
The two-part sealant pumps available all require maintenance and trained operators. It is beyond the
scope of Dow as a sealant supplier to provide pump maintenance, spare parts and troubleshooting. The
quality control program recommended by Dow, including snap time, butterfly test, shop adhesion testing
and deglazing, will show pump problems. Sporadic cure rate, non-uniform color, presence of air and
uneven hardness of the finished sealant are issues generally associated with the pump.
A method to evaluate the consistency of mix from the pump is to dispense a winding, snake-like bead of
sealant onto a cardboard sheet. Tool the bead to an approximate 1/4" (6 mm) thickness and monitor the
cure rate of the sealant. Type A durometer hardness can be used to monitor the rate of sealant cure. If
soft spots remain after the bulk of the sealant is cured, there may be a problem with the pump. Please
notify your pump manufacturer for assistance.
DOWSIL™ 983 Structural Glazing Sealant will work only when it is metered and mixed without
incorporation of air. This requires a properly maintained pump with qualified, trained operators. Critical
processing parameters are down pressure on the curing agent and base platens, effective purging during
drum or pail exchange, seal integrity, and proper exchanging of a pail or drum before the system runs
“dry” or cavitates.
If a pump has been idle between projects, it is suggested that a thorough cleaning and refurbishing
of maintenance items be performed. This can be done with the assistance of the pump manufacturer
or its distributor.
Dispensing equipment must be used to airlessly meter and mix DOWSIL™ 983 Structural Glazing
Sealant. The specific operation and maintenance of the pump are beyond the scope of this document.
The applicator must have a start-up, shut-down and maintenance procedure for the pump to properly
apply structural glazing adhesives.
When starting the pump, the curing agent line should be opened and material pumped through the line
until the sealant exiting the dispensing gun ceases to be white or streaked. Instead, it should be a
consistent black color, indicating a mix of the base and curing agent components.
Before shutting down the pump, the static mixer and hoses should be purged with base material and
cleaned with an approved cleaning solvent. The amount of wasted material resulting from the start-up
and shutdown of the pump varies with the type of pumping equipment used.
As the volume of the hose after the static mixer location decreases, so will the amount of wasted
material resulting from start-ups and shutdowns.
Quality control testing to be performed on start-up of the equipment includes the butterfly test and the
snap-time test. Descriptions of each follow. Results of these tests must be recorded in a log similar to the
example in the Documentation section of this manual.
These are guidelines based on Dow’s experience and are not meant to supersede any recommendations
or documentation from the pump manufacturer.
35
Butterfly Test
The butterfly test must be performed every time the pump is started up, including start-ups that
occur after extended breaks. The purpose of this test is to check for an adequate mix of base and
curing agent components.
Snap-Time Test
Once full mix of the two-part sealant (as confirmed by the butterfly test) is achieved, a snap-time test
should be performed. This test must be performed on a daily basis. Snap time is an indicator test that can
vary from technician to technician. The snap-time test relates the base-to-catalyst mix ratio to the cure
rate of the sealant and provides an indication of working time and deep section cure. The snap-time test
is performed as follows:
Regardless of the results of the snap-time tests, ultimately one should be concerned only if the sealant
does not cure. Assuming that the sealant does cure, it is most important that the sealant develops
adhesion to the substrate. Snap-time test is an indicator and should be considered as a part of an overall
quality assurance program.
36
Pump Seal Maintenance Check (Snake Test)
Worn seals on the volumetric (dual-action) catalyst displacement cylinders can cause a variable mix
ratio which can result in an inconsistent cure and should be checked when a pump is started up for the
first time or if soft spots are noticed in the sealant bead. When cylinder seals wear, they can allow an
inconsistent amount of catalyst to be mixed into the sealant. This typically occurs as the catalyst
volumetric cylinder cycles from one direction to the other and allows back pressure to let catalyst escape
from one side. This is a typical maintenance item that should be added to the overall Quality Control
program.
1. Turn on the pump and lay a continuous bead back and forth in a “snake-like” pattern on a piece
of cardboard. Allow the pump to extrude for 3 to 5 minutes so that 2 complete cycles of the
catalyst cylinder are completed.
2. Let the sealant cure for 2 hours.
3. Check the entire bead by pressing your finger into the surface every 2" to 3" and ensuring the
entire sealant bead is fully cured along the entire length.
If soft spots are present, it is likely the problem needs to be addressed with a pump technician who will
replace the pump seals. The soft spots will typically occur in a consistent fashion (or specified length)
along the extruded bead of sealant.
It is recommended that DOWSIL™ 121 Structural Glazing Sealant be applied between temperatures of
-20 to 37°C (-5 to 100°F).
Cold kits of material will cure slower (even if the shop temperatures are warm). For each drop of 10°C,
the reaction rate (cure, snap time, adhesion) is decreased by approximately ½. It is not uncommon to see
these properties drop during the winter from typical properties seen in the summer. This change in initial
properties will not affect the cured performance of the sealant.
37
If you would prefer to use another manufacturer, please contact your local Dow representative to ensure
you will get proper sealant mix.
Please note that use of dispensing equipment of a model or a manufacturer not listed in this document
will void any DOWSIL™ product and structural adhesion Limited Warranties. The only exception to
this would be if Dow publishes an updated version of this document and/or issues a document indicating
the approval of another manufacturer or dispensing equipment model for use with DOWSIL™ 121
Structural Glazing Sealant.
Twelve 18-element, ½-inch diameter static mixers are included in the packaging with the sealant and are
required to mix the material. A new static mixer must be used for each cartridge to ensure proper mixing
of the material. Neither hand-mixing nor mechanical mixing is satisfactory due to the incorporation of
air, resulting in altered physical properties.
1. Attach air hose to compressor and to end of pneumatic sealant tool. The air pressure should not
exceed 90 psi or the maximum air pressure listed on the gun, whichever is greater.
2. Ensure the dual pistons are to the back of the gun, so the cartridge can be put in. This can be
done using the reverse function on the pneumatic dispensing tool.
3. Remove cap from top of cartridge. Remove the plug on the dispensing end of the cartridge by
inserting a flat screw driver or similar tool into the rectangular slot on the plug. Use the tool to
bend the plug 90 degrees as if to make it perpendicular to the cartridge. This movement will
release the plug. A second option is to invert the cartridge, firmly tap the top plug on the
cartridge on a hard, flat surface, then remove the plug out from the top of the cartridge.
4. Now the cartridge can be inserted. The cartridge should snap into the tool so that the ends of the
cartridge are aligned with the dual pistons.
5. Once the cartridge is inserted, ensure that the pistons are set to move in the forward direction.
Then, press and hold the trigger until material comes out of BOTH the curing agent and
base cartridges.
Once both curing agent and base are being extruded from the cartridge, wipe off the
excess sealant.
38
6. Attach a new static mixer. The end of the static mixer can be cut using a sharp knife or scissors
to make the tip larger or to slant it at an angle. Do not remove any of the mixing elements in
the mixer.
7. With the static mixer screwed on, depress the trigger until the static mixer is completely full and
the DOWSIL™ 121 Structural Glazing Sealant can be seen coming out the end of the mixer.
This is best done over a waste area. Wipe off the initial material that comes out of the static
mixer.
Quality Check: The first inch (25.4 mm) of the static mixer closest to the cartridge should have
a distinct white area and dark (black or grey) area, approximately dividing the static mixer in
half. If you do not see this, you may have skipped step 5.
8. The material is now ready to use. For information on installing the sealant into the joint, refer to
the Sealant Joint Installation Procedure section of this manual.
9. Once the cartridge is emptied, reverse the dual plungers. Remove the cartridge and static mixer
from the dispensing tool and dispose. The static mixer should not be reused. To use another
cartridge of DOWSIL™ 121 Structural Glazing Sealant, repeat steps 3–7.
10. Once you have completed your sealant installation, turn off the air compressor and shut off the
air to the gun. Pull the trigger until the air pressure reads zero and then disconnect the air hose
from the gun.
Quality Control
In lieu of the traditional butterfly test and snap test that is required for the DOWSIL™ 983 Structural
Glazing Sealant, a small amount of material should be extruded into a cup or onto a piece of paper or
cardboard. This material should be checked to ensure that it starts to cure into a rubber in 4–8 hours.
39
sealant performance will be weakened. This is crucial since the effectiveness of the silicone in structural
applications is largely dependent on the sealant bite (contact area).
Keyway considerations: It is recommended to always use a flat surface for structural glazing. When
additional structural bite is required, it may become necessary to use a keyway as part of the structural
bite. If use of a keyway becomes necessary, please follow these guidelines:
When a keyway is used as part of the glazing surface contributing to the structural sealant bite, the
sealant installation must be carried out as a separate step. The keyway must be cleaned, primed if
necessary, sealant installed and tooled as its own procedure prior to the remainder of the structural
sealant being installed. This is to ensure full joint fill and adhesion to a surface that is contributing to
structural bite.
1. To ensure an aesthetically pleasing job, masking tape should be used to keep excess sealant from
contacting adjacent areas where it is not intended.
2. Apply the sealant in a continuous operation using a caulking gun or pump. A positive pressure,
adequate to fill the entire joint width, should be used. This can be accomplished by “pushing” the
sealant ahead of the application nozzle. Care must be taken to ensure complete fill of the sealant
cavity. This is critical, since the effectiveness of the silicone in structural applications is largely
dependent on the sealant bite (contact area).
3. Tool the sealant with firm pressure before a skin begins to form (typically 10 to 20 minutes).
Tooling forces the sealant against the spacer and the joint surfaces. Do not use liquid tooling aids
such as water, soap or alcohols. These materials may interfere with sealant cure and adhesion
and create aesthetic issues.
4. Remove the masking tape before the sealant skins over (within about 15 minutes of tooling).
Some general rules to follow when using silicone sealant in glazing applications are as follows:
1. Care must be taken to ensure that joint surfaces that have been prepared are not contaminated.
2. In some field glazing applications, the silicone may not be applied the same day the glass is set.
Joint preparation (cleaning and priming) must be accomplished immediately prior to applying
the silicone.
3. Temporary fasteners or clips must be used to retain the structurally glazed lites or panels until the
silicone has fully cured. A two-sided adhesive tape, used as the structural spacer, may be
considered sufficient temporary support provided the tape manufacturer has approved the use of
their product for this application.
40
Movement of In Shop Structurally Glazed Units
Once a structurally glazed unit has been sealed, it needs to be stored and left until the sealant has cured
and adhesion has been built up between the sealant and the substrates used. It must be understood at this
stage that the cure of the sealants and the adhesion build-up are not linked. Therefore, if a sealant has
reached full cure, this does not necessarily mean that full adhesion to the substrates has been achieved.
This is particularly true of two-part sealants. Therefore, it is critical that the curtainwall units be allowed
sufficient time for adhesion to develop before units are subjected to stress. Two-sided adhesive tape
helps to prevent failure during the cure by forming a tight bond with the panel and substrate.
There are many ways to handle fabricated curtainwall units after their manufacture. Within the first
four hours after installing DOWSIL™ 983 Structural Glazing Sealant, curtainwall units can be moved
from a glazing table to a bunking area to release floor space in a manufacturing facility. Units moved
within this first 4-hour period must be kept horizontal and be moved carefully to ensure that no stress is
placed on the sealant joint. It is inappropriate to lift the unit via suction cups on the glass during this
initial period.
Units glazed with DOWSIL™ 121 Structural Glazing Sealant that are moved within the first 24-hour
period after installing DOWSIL™ 121 Structural Glazing Sealant must be kept horizontal and be moved
carefully to ensure that no stress is placed on the sealant. It is inappropriate to lift the unit via suction
cups on the glass during this initial period.
While it is general industry practice to wait 24 hours before transporting units to a job site, units glazed
using DOWSIL™ 983 Structural Glazing Sealant may be transported after 4 hours if adhesion testing
has documented sufficient sealant cure and adhesion. When using DOWSIL™ 121 Structural Glazing
Sealant, the units should be allowed to cure for at least 24 hours before being transported. Whatever
time frame for transport is chosen, adhesion testing should be completed and documented at that time to
illustrate the sealant is sufficiently cured and adhering. If units are transported or crated prior to 100%
cure of the sealant (typically 24 hours), banding should be evaluated for proper tension to ensure the
sealant does not take a compression set.
41
Peel-in-Adhesion Test Procedure
Peel-in-adhesion tests are required as a means to verify sealant adhesion on production materials. Peel-
in-adhesion testing should be performed as follows:
The sealant should be applied to each representative substrate. Sealant samples should be peeled back at
the time increment that the units are to be moved. Units may be moved in as little as 4 hours for
DOWSIL™ 983 Structural Glazing Sealant or 24 hours for DOWSIL™ 121 Structural Glazing Sealant,
but typically cure times are from 1 to 7 days. At the time that curtainwall units may be subjected to
stress on the structural silicone, either during transit in the shop or to the jobsite, the sealant must have
achieved 100% cohesive failure to each of the substrates that adhesion is required. Only after the sealant
has achieved 100% cohesive failure can significant stress be applied to the structural joint. Peel-in-
adhesion test results should be correlated with results from deglazing of actual production units.
The tests described above must be performed to verify that adhesion of structural silicone is obtained
before curtainwall units are transported to a jobsite and erected on the building. These are daily tests and
are intended to verify that all surfaces that require structural adhesion have obtained adhesion before
units leave the factory. Adhesion time of two-component structural sealants can vary with conditions of
lower temperature and humidity, and units that do not have full adhesion can lose adhesion during
transportation if adhesion is not verified prior to shipment. Curtainwall units should not be subjected to
stress unless the sealant has developed full adhesion. Dow should be consulted for recommendations in
determining the appropriate handling of structurally glazed curtainwall units.
42
NOTE: Obtaining Adhesion on Painted Aluminum with DOWSIL™ 983 Structural Glazing
Sealant and DOWSIL™ 121 Structural Glazing Sealant – Adhesion development is a key
requirement that must be confirmed at each glazing location before subjecting units to considerable
movements such as tilting, crating or shipping units. However, it may take 1, 2, 7 or more days for
adhesion to develop between DOWSIL™ 983 Structural Glazing Sealant or DOWSIL™ 121 Structural
Glazing Sealant and painted aluminum when either no primer or DOWSIL™ 1200 OS Primer is used.
As an alternative, the use of DOWSIL™ Primer-C OS to may provide quicker adhesion development on
painted substrates compared to no primer or DOWSIL™ 1200 OS Primer.
Deglazing
Deglazing is carried out on glass or panel and frame, which use structural silicone attachment.
Deglazing is a method of quality inspection used to confirm good adhesion and proper fill of the
structural joint. Deglazing on silicone structural glazing projects is an excellent quality control
procedure. Deglazing involves completely detaching the panel from the frame. The structural silicone
sealant should be tested for adhesion to both the panel and the frame. The surface of the panel and/or
frame must not be damaged to obtain the best inspection.
NOTE: When measuring the size of the structural bite during deglazing, if any voids or underfilling
occurs, then the measured bite may not meet the minimum bite requirements outlined in the Dow project
print review letter and DOWSIL™ Structural Glazing Warranty requirements. The minimum measured
bite at any point (on the frame or panel) governs the measured bite reported on the Deglaze Inspection
Form – reporting measured average bites is not acceptable. Always follow proper application techniques
to ensure complete fill is attained to avoid these issues and the need to reapply the sealant.
Deglazing Frequency
Deglazing may not be required as part of a comprehensive quality control program for structural glazing.
Simple processes, such as glazing 1-2 lites in a storefront application make no practical sense to deglaze
unless the design is complicated. For glazing projects with numerous lites, variable geometries or
complex design requirements, deglaze operations should be considered part of a comprehensive quality
control program and should be agreed upon prior to fabrication between contract glazer, designer,
consultant and/or other interested parties. Project documents/specifications should prevail in defining
frequency.
Deglaze operations should be conducted to capture the initial start of fabrication to ensure quality
workmanship with periodic inspection to confirm continued quality. Dow recommends deglazing
according to the following schedule:
44
Documentation – Quality Assurance and Warranty
Suggested logs referred to in this manual are provided on the following pages. In the event of a warranty
claim or inspection, these must be available from the contractor, subcontractor or owner for review by
Dow, the curtainwall consultant and/or the local building official.
Therefore, it is suggested that these quality assurance logs be kept together with the project file. A
hardcover logbook may be preferential to copies of the logs suggested here. A quality assurance
engineer should be responsible for documenting this data on a job-to-job basis. All curtainwall units
must be numbered so the sealant installation dates, sealant lot numbers and quality assurance testing can
be obtained from the project log. The position of each panel on the building should be marked on an
elevation drawing so that it can be easily traced if required.
Dow will be happy to assist you during the implementation of this quality control program. If you have
any questions, contact your local Dow Field Specialist.
At the time of shipment, the DOWSIL™ sealant is warranted that the sealant will meet the Dow sales
specification. For further details on the requirements and limitations of this limited warranty, consult the
DOWSIL™ product data sheet for the sealant in use.
Dow also offers a project-specific 20-year performance warranty for sealants used in structural
applications. Specific requirements must be met to qualify for this performance warranty.
For details on how to obtain the applicable warranty, please consult your local Dow Field Specialist or
authorized building sealant distributor.
45
Quality assurance requirements for a project-specific performance (structural) warranty include, but are
not limited to:
1. Confirmation of Adhesion: Dow Adhesion Letter(s) generated for each substrate that contacts the
approved DOWSIL™ Structural Sealant (DOWSIL™ 795 Silicone Building Sealant,
DOWSIL™ 995 Silicone Structural Sealant, DOWSIL™ 121 Structural Glazing Sealant or
DOWSIL™ 983 Structural Glazing Sealant).
2. Confirmation of Compatibility: Dow Compatibility Letter(s) generated for each spacer that is
used in direct contact with the DOWSIL™ Structural Sealant (DOWSIL™ 795 Silicone
Building Sealant, DOWSIL™ 995 Silicone Structural Sealant, DOWSIL™ 121 Structural
Glazing Sealant or DOWSIL™ 983 Structural Glazing Sealant).
3. Dow Print Review Approval Letter, which confirms that the documented joints meet Dow
performance standards for structural glazing.
4. Field testing documentation log book(s) that show sufficient testing was done. The minimum
should be one test per elevation per floor. The contractor should determine other job-specific
needs. The contractor should complete and fill out the log to demonstrate that acceptable
adhesion was obtained in actual use. This is in addition to the Adhesion Letter noted in #1.
5. The contractor documents and retains all required quality assurance documentation and, upon
completion of the project, provides a copy to the owner. This documentation must be retained for
this warranty to be valid and will be required should any claims arise in the future. The owner
should retain the quality assurance documentation along with the Dow-issued warranty.
1. Confirmation of Adhesion: Dow Adhesion Letter(s) generated for each substrate that contacts the
approved DOWSIL™ Structural Sealant (DOWSIL™ 795 Silicone Building Sealant,
DOWSIL™ 995 Silicone Structural Sealant, DOWSIL™ 121 Structural Glazing Sealant or
DOWSIL™ 983 Structural Glazing Sealant).
2. Confirmation of Compatibility: Dow Compatibility Letter(s) generated for each spacer that is
used in direct contact with the DOWSIL™ Structural Sealant (DOWSIL™ 795 Silicone
Building Sealant, DOWSIL™ 995 Silicone Structural Sealant, DOWSIL™ 121 Structural
Glazing Sealant or DOWSIL™ 983 Structural Glazing Sealant).
3. Dow Print Review Approval Letter, which confirms that the documented joints meet Dow
performance standards for structural glazing.
4. In-shop logs:
a. Daily adhesion testing and quality control logs must be completed by the contractor to
verify that the units were sufficiently cured and adhered before transported to the site.
b. Deglazing documentation log must be completed and filled out by the contractor to
demonstrate that acceptable adhesion, void-free fill and sealant bite were obtained on
production units per requirements in the log.
5. The contractor documents and retains all required quality assurance documentation and, upon
completion of the project, provides a copy to the owner. This documentation must be retained for
this warranty to be valid and will be required should any claims arise in the future. The owner
must retain the quality assurance documentation along with the Dow-issued warranty.
46
Dow Project Checklist
The following items must be completed for silicone structural glazing projects. Check off and/or date
these items as they are completed. Some items may not apply to all projects. In that case, simply note
“NA” (not applicable).
Design Details
_______ Submit prints to Dow for review
_______ Include windload and maximum glass size
_______ Date(s) of Dow print review
_______ Mock-up drawings/final shop drawings
Quality Assurance
_______ Perform daily product quality testing and document on log sheet(s)
_______ Perform daily field/shop adhesion testing and document on log sheet(s)
_______ Perform deglaze on mock-up and document on log sheet(s)
_______ Perform deglaze on frame according to schedule
47
Product Quality Control Log – One-Part Silicone Sealants
Project:
Location/Elevation/Unit ID:
Sealant Color:
48
Product Quality Control Log – Two-Part Silicone Sealant
49
Product Quality Control Log - DOWSIL™ 121 Structural Glazing Sealant
Date:
Temperature:
Initial
Static Mixer
Location/ Material
Time Lot Number Façade Primer Y/N Check for Mix Initials
Specific Lite Runout Cured
Y/N
Y/N
50
Field/Shop Adhesion Testing Log
Project:
Sealant:
Acceptable
Test Location Acceptable Joint
Applied by Adhesion (Y/N)
Date Applied Test Date (Elevation, Unit Primed (Y/N) Fill (Y/N)
(Initials) and %
Number, etc.) (Measured)
Elongation
51
Dow Deglaze Inspection Form
Project Number: ___________________________________________________________________________________________________
2.
3.
1.
2.
3.
52
Weatherproofing
Introduction
The successful performance of a building exterior is frequently defined by its ability to keep rain
and the elements outside, away from the building’s occupants. One of the critical links to ensuring a
weatherproof building is the joint sealant. Building joints can be sealed effectively by following a
few simple guidelines for designing workable joints, selecting the correct sealant, performing
appropriate surface preparation and performing quality checks to ensure proper performance. This
section of the manual contains design, sealant selection, surface preparation, job site adhesion
testing and remedial procedures.
Joint Movement
Regardless of the size and height of structures, joint movement inevitably occurs by various factors such
as: changes in temperature, seismic movement, elastic frame shortening, creep, live loads, concrete
shrinkage, moisture-induced movements and design errors. Therefore, each joint should be designed to
absorb these movements, using the correct sealant.
When movement is caused by temperature change, the degree of joint movement for each material
should be considered since all materials have their own coefficient of linear thermal expansion (CTE).
Joint movement caused by thermal expansion can be calculated by the following equation:
Material Thermal
Max. Temp. Min. Temp. Movement
Length Material Coefficient
(°F) (°F) (inches)
(inches) inch/inch/°F
160 -20 96 Glass 0.0000051 0.088
53
Average Coefficients of Linear Thermal Expansion for Building Materials -
Reference ASTM C1472-06 (Standard Guide for Calculating Movement and
Other Effects When Establishing Sealant Joint Width)
NOTE: The coefficient of expansion for natural materials (brick, stone, etc.) or fabrications of natural
materials can be highly variable. If a specific material is specified, then the coefficient for that material
should be established and used rather than an average value.
NOTE: Moisture-induced movement of brick masonry will cause the brick to swell and reduce joint
sizes over the life of the project.
54
Joint Types
From a functional point of view, joints for construction can be put into two classes depending on the
degree of movement.
• Control Joint
• Expansion Joint
• Lap Joint
• Butt Joint
• Stack Joint
55
Joint Design
DOWSIL™ sealants have been designed to perform when installed in compliance with accepted
weathersealing procedures. Industry guides documenting in detail the procedures for designing
weatherseal joints are available. Some good examples are found later in this document.
Dow has found that a few underlying principles are critical to consider in virtually all joint designs using
silicone sealants. This section is intended as a review of these underlying design principles. When
considering the design of weatherproof joints, the following basic points must be addressed:
• In all cases, a minimum depth of 1/4" (6 mm) sealant/substrate bond is necessary to ensure
adequate adhesion.
• In most cases, a minimum width of 1/4" (6 mm) opening is necessary to ensure that sealant
applied from a caulking gun will flow into the sealant joints. NOTE: In some cases where the
sealant is used simply as a non-moving bedding compound and is applied to one substrate before
both substrates are pressed together, thinner joint dimensions are acceptable.
• One-part silicone sealants require atmospheric moisture to fully cure. Therefore, the sealant joint
must be designed to ensure that the sealant is not isolated from the air.
• A minimum 1/4" (6 mm) joint width is recommended. Wider joints accommodate more movement
than narrow joints.
• Three-sided adhesion limits the amount of movement that a joint can accept without inducing a
tear. Three-sided adhesion can be eliminated by the addition of a bond breaker tape or backer rod.
With three-sided adhesion, no more than ±15% movement can be accommodated.
• A properly designed moving joint with a 2:1 width to depth ratio will accommodate more
movement than a thick joint (i.e., 1.5:1 or 1:1 ratio). Sealants are designed to deliver optimum
performance when the joints are shaped like an hourglass and use the 2:1 ratio.
• As the sealant joint width becomes larger than 1" (25 mm), the depth should be held at
approximately 3/8" to 1/2" (9 mm to 12 mm). There is no need for greater sealant depth with a
silicone sealant. This may mean that the width to depth ratio will be greater than 2:1 (i.e. 3:1).
• Joint widths up to 4" (100 mm) can be accommodated with silicone sealants. Wide joints may require
additional care and attention to detail to provide an aesthetically pleasing finish. Wider joints may be
better accommodated by DOWSIL™ 123 Silicone Seal. For large joints that will be hidden by
cladding such as the perimeter of curtainwall systems, DOWSIL™ Silicone Transition Strip may be
an option.
• For further information, see Construction Calculators under the Tools and Resources section of the
Dow Construction Website at consumer.dow.com/construction.
100
Minimum Joint Width = * (Mt + M1) + T
X
56
For example:
A horizontal joint between an aluminum curtainwall and a concrete panel with a combined thermal
movement of 5/16" (8 mm), a live load movement of 1/4" (6 mm), a construction tolerance of 1/4"
(6 mm) and 25% movement capacity sealant would be:
Width = 100/25 * (8 + 6) + 6
Width = 62 mm
Weatherseal in Shear
c = 0.375”
(15 mm) a2+b2 = c2 where a = original glueline
b b = joint movement
c = new glueline after joint movement
57
For Example:
a2 + b2 = c2
(0.25”)2 + b2 = (0.375”)2
b2 = 0.078 in2
b = 0.280”
a2 + b2 = c2
(10 mm)2 + b2 = (15 mm)2
b2 = 125 mm2
b = 11.18 mm
These suggestions should help minimize wrinkling but may not eliminate it, as all sealants are prone to
this aesthetic issue. This issue is not known to affect the long term performance of the joint and will not
void any DOWSIL™ weatherseal warranty.
58
Backer Materials
A backer rod is the typical backer material for most weatherseal joints. The role of a backer rod is to
allow a sealant to be installed and tooled to a proper joint profile. Once the sealant cures, the backer
material must not restrict the movement of the sealant or cause 3-sided adhesion. To provide sufficient
backpressure during sealant installation, the backer rod should be sized ~25% larger than the joint
opening. Sizing differs among backer rod types; refer to the manufacturer’s recommendations.
Generally, three common backer rod types can be used with DOWSIL™ sealants :
• Open-cell polyurethane
• Closed-cell polyethylene
• Non-gassing polyolefin
Each backer rod type has demonstrated successful performance with DOWSIL™ sealants.
• Open-cell polyurethane backer rod allows the sealant to cure through the backer rod, which is
beneficial when fast sealant cure is desired. Open-cell polyurethane backer rod can absorb water,
which may have a detrimental effect in certain joint types.
• Closed-cell polyethylene backer rod may outgas if punctured during installation, requiring it to be
left for 20 minutes before application of the sealant.
• Other back-up materials such as expanding foam tapes or glazing gaskets should be reviewed or
tested for compatibility prior to use.
• When a backer rod cannot be positioned in a joint opening, a Teflon or polyethylene tape should
be used to prevent three-sided adhesion.
Dow makes the following exceptions when selecting backer rod types:
• For double weatherseal joints, open-cell polyurethane backer rod must be used unless the interior
seal is allowed 7 days’ cure before installing the exterior seal.
• Open-cell polyurethane backer rod is recommended for use with DOWSIL™ 790 Silicone
Building Sealant against painted or metal surfaces to promote cure from both sides of the joint.
• Because EIFS manufacturers do not permit the use of open-cell polyurethane backer rod with their
systems, use either DOWSIL™ 791 Silicone Weatherproofing Sealant or DOWSIL™ 795
Silicone Building Sealant when EIFS is adjacent to non-porous or metal surfaces. Open-cell
polyurethane backer rod should not be used adjacent to EIFS.
• In some horizontal joints where water can collect, open-cell polyurethane backer rod should
not be used.
Hydrophobic Effects
Silicone sealants cure with moisture in the atmosphere by reacting with a functional silane in the
presence of a catalyst and functional silicone polymers. The silane crosslinkers are of the same chemical
structure as the materials used to waterproof concrete structures such as parking garages and bridge
decks. Silane crosslinkers are used in all silicone sealants and the silicon-modified organic materials
(polyethers and acrylics) that are used as sealants in the construction industry.
As a silicone sealant is applied into a joint, there is the potential for the excess crosslinkers (added to
ensure adequate shelf life) to migrate into the porous material and crosslink into a hydrophobic resin
59
beneath the surface. On occasion, this hydrophobic resin will not allow water to penetrate into the stone
adjacent to the joint and may cause a dry area to appear adjacent to the joint in a rainstorm. While this
phenomenon does not always occur, when it does, it can be attributed to the inherent nature of the
necessary silane crosslinkers. Therefore, it cannot be guaranteed that this phenomenon will never occur
with a specific porous substrate.
However, there are steps that can be taken to minimize the potential for this phenomenon to occur.
Minimizing Hydrophobing
• When priming, use a resin-based primer, such as DOWSIL™ Construction Primer P, as opposed
to a silane primer, such as DOWSIL™ 1200 OS Primer.
• Avoid over-application of any primer, silane or resin, onto the visible surface of the facade.
• Use an open-cell polyurethane backer rod as opposed to a polyethylene or polyolefin backer rod.
This will allow a curing of the excess crosslinker to occur along the backside and minimize a
catalyst/crosslinker mixture from migrating into the stone.
• Make sure there is no more than 1/4" of sealant applied over the midsection of the backer rod.
This will minimize the volume of sealant containing excess crosslinker in the joint.
DOWSIL™ sealants are tested and approved for use by the major EIFS manufacturers.
Refer to the Building Sealant Recommendation and Surface Preparation Guide, Form No. 63-1184,
for current recommendations.
For EIFS restoration, please refer to the EIFS Restoration Guide, Form No. 62-510.
60
Weatherseal Design Examples
Examples of a variety of weatherseal joints follow with a review of joint type for key points
and concerns.
1. A deep sealant joint will not have the same movement capability as a properly designed joint.
2. Slow cure due to excessive sealant depth.
61
Moving Corner Joints
Good Joint Design Poor Joint Design
62
Remedial Joints
Good Joint Design Poor Joint Design
1. Dimension A less than 1/4" (6 mm) increases difficulty in obtaining adhesion and increases the
likelihood for voids.
2. Dimension B less than 1/8" (3 mm) increases the likelihood of pinholes or voids in tooling; poor
cohesive integrity.
3. No bond breaker material; therefore, the joint will not accept movement.
63
Splice Joints
Good Joint Design Good Joint Design Poor Joint Design
Key Points:
64
Cap Bead Glazing Joints
Good Joint Design Poor Joint Design
65
Dual-Seal Moving Weatherseal
Good Joint Design Poor Joint Design
1. Both weatherseals comply with the requirements for conventional moving weatherseals
(addressed previously).
2. Open-cell backer rod is used to ensure full cure of the back weatherseal.
3. If closed-cell backer rod is used, the back weatherseal must be fully cured prior to the installation
of the exterior seal.
4. Dimension A is at least 3/4" wide to assist application of the rear sealant joint.
1. If both joints are sealed at or near the same time, the closed-cell backer rod will prevent moisture
from reaching the rear sealant joint, and the sealant will not cure.
2. Dimension A is less than 3/4", making application of rear joint difficult.
3. Exterior joint seal to aesthetic snap-on cap.
66
Window Perimeter Joints: Insufficient Aluminum Extrusion
Good Joint Design Poor Joint Design
1. Attempting to apply sealant onto the edge (or behind) thin gauge metal results in inadequate
sealant/substrate contact and water leakage.
67
Weatherproofing Joints: Surface Preparation and Sealant Application
Introduction
This application procedure outlines general requirements for installing DOWSIL™ Silicone Building
Sealants. By following these procedures closely, you will help ensure good sealant performance. To be
eligible to receive a Dow warranty, these procedures must be followed. Since DOWSIL™ Silicone
Building Sealants are applied in many different environments and situations, these procedures are not
intended to be a complete and comprehensive quality assurance program.
Field adhesion tests are required to ensure good sealant performance and to verify any sealant
recommendation (see the Quality Assurance section on page 75).
There are five basic steps for proper joint preparation and sealant application:
The following sections are intended to provide more detailed information in each of these areas.
68
Porous Substrates
Building materials such as cement board panels, concrete, granite, limestone and other stones or
cementitious materials that absorb liquid are considered porous substrates. Dusting alone may be
sufficient cleaning for new porous substrates. Depending on the condition of the surface, porous
substrates may require abrasion cleaning, solvent cleaning or both. Laitance and surface dirt must be
completely removed. Concrete form-release agents, water repellents and other types of surface
treatments, protective coatings and old sealant all affect sealant adhesion. Removal of these treatments,
coatings or sealants by abrasion cleaning may be required to obtain acceptable adhesion.
Abrasion cleaning involves grinding, saw cutting, sand or water blasting, mechanical abrading, or a
combination of these methods. When choosing an abrasion cleaning method, it is important to choose
one that will not leave a residue on the substrate. For example, some metal wire brushes can leave a
varnish on precast panels. Remaining dust and loose particles should be removed by dusting the surface
with a stiff brush, vacuuming, or blowing the joints with water- and oil-free compressed air. Once the
abraded surface is clean and dry, the sealant can be applied. If the surface is dirty, it must be solvent
cleaned with the “two-cloth” method explained later in this section. Some porous materials will trap
solvents after cleaning or priming. Allow this solvent to evaporate before sealant is applied.
Please note that Dow’s recommendations for removal of existing sealants, substrate cleaning, joint
preparation and installation of DOWSIL™ sealants are not intended and may not be appropriate for
remedial work involving existing sealants and/or joints containing PCBs or other potentially hazardous
substances. If you know or suspect that the existing sealants and/or joints contain PCBs or other
hazardous substances, contact a knowledgeable authority on appropriate removal, handling and
disposal procedures.
Organic solvent must be removed with the dry cloth before the solvent evaporates, or the cleaning will
be less effective. Some porous surfaces will allow a small amount of residual organic solvent to remain
in the top surface layer. If this is the case, the surface must be allowed to dry before installing primer (if
needed), backer rod and sealant.
69
Cleaning Procedures for Flashing Substrates
Peel-and-stick and spunbonded polyolefin substrates are unique surfaces to adhere to, but they must be
clean in order to achieve sealant adhesion. However, adhesion to these substrates may be negatively
affected if they are “overcleaned,” burnished or polished. Dow thereby recommends a light two-rag
wipe method using isopropanol alcohol (IPA) for cleaning these surfaces. Utilize clean, soft, absorbent,
lint-free cloths for the cleaning. The “two-cloth” cleaning method consists of a solvent wipe followed by
a dry cloth wipe.
1. If there is significant dirt or debris visible on the membrane surface, lightly brush this off using
a soft brush.
2. Pour or dispense an acceptable cleaning-grade solvent onto the cloth. A plastic (solvent-resistant)
squeeze bottle works best for organic cleaning solvents. Do not dip the cloth into the container of
solvent, as this will contaminate the cleaning agent.
3. Lightly wipe the membrane surface to remove contaminants. Check the cloth to see if it has
picked up contaminants. Rotate the cloth to a clean area and re-wipe until no additional dirt
is picked up.
4. Immediately wipe the cleaned area with a separate clean, dry cloth.
The IPA must be removed with the dry cloth before the solvent evaporates, or the cleaning will be less
effective. If any solvent remains on the substrate after the dry cloth wipe, allow the IPA to completely
“flash” or dry prior to applying primer or sealant. Drying time depends on environmental conditions, but
on a membrane substrate, allowing 5–10 minutes for the IPA to flash off is typically sufficient.
Cure Inhibition
DOWSIL™ 790 Silicone Building Sealant and DOWSIL™ Contractors Concrete Sealant are sensitive
to alcohols. Therefore, when cleaning, Dow recommends using a non-alcohol based solvent and
allowing the solvent to fully dry/flash prior to sealant installation. Primers must also be fully dry prior to
sealant installation. Further, do not use alcohols or solvents as tooling aids with these sealants, as cure
inhibition will result. Any application or contact of DOWSIL™ 790 Silicone Building Sealant and
DOWSIL™ Contractors Concrete Sealant with alcohol, solvents or other uncured sealants may result in
cure inhibition.
1. Joint surfaces should be clean and dry. Apply masking tape to the surfaces next to the joint to
keep excess primer and sealant off areas where they are not intended.
2. Pour some primer into a small, clean container; be sure to replace and tighten the cap on the
primer can. To prevent deterioration of the primer, do not pour more than a 10-minute supply
into the container.
70
3. Depending on the substrate and job conditions, two different methods can be used to apply the
primer. The preferred application is to dip a clean, dry, lint-free cloth into the primer and gently
wipe a thin film onto the surface. For “hard-to-get-to” areas and rough surfaces, apply the primer
in a thin film with a clean brush. Caution: Over-priming can cause adhesion loss between the
sealant and the primer. If too much primer has been applied, a powdery, chalky, dusty film will
form on the surface. Excess primer should be removed by dusting the joint with a clean, dry, lint-
free cloth or a non-metallic bristle brush.
4. Allow the primer to dry until all the solvent evaporates. This typically takes 5 to 30 minutes,
depending upon the temperature and humidity.
5. Inspect the surface for dryness. If too much primer has been applied, a powdery, chalky, dusty
film will form on the surface. In this case, remove excess primer with a clean, dry, lint-free cloth
or a non-metallic bristle brush before applying sealant.
6. The surface is now ready for application of the backer rod and sealant. DO NOT APPLY
PRIMER OVER BACKER ROD.
7. Sealant must be applied the same day the surfaces are primed. Any surfaces primed but not
sealed on the same day must be re-cleaned and re-primed before applying sealant.
Primer Storage
Store primer with cap tightly closed, as DOWSIL™ primers will react quickly when exposed to
moisture, reducing their adhesion-promoting capabilities.
To obtain full adhesion, sealants require a clean, dry, frost-free surface. Although silicone sealants have
excellent wide-temperature gunnability, the practical application temperature can be dictated by frost
formation on the joint edges, which can begin to occur below 4°C (40°F). To assist in the drying of a
frost-containing joint, a water-soluble solvent such as IPA should be used.
1. To ensure an aesthetically pleasing job, masking tape should be used to keep excess sealant from
contacting adjacent areas where it is not intended.
2. Apply the sealant in a continuous operation using a caulking gun or pump. A positive pressure,
adequate to fill the entire joint width, should be used. This can be accomplished by “pushing” the
sealant ahead of the application nozzle. Care must be taken to ensure complete fill of the
sealant cavity.
3. Tool the sealant with light pressure before a skin begins to form (typically 10 to 20 minutes).
Tooling forces the sealant against the back-up material and the joint surfaces. NOTE: Do not use
liquid tooling aids such as water, soap or alcohols. These materials may interfere with sealant
cure and adhesion and create aesthetic issues.
4. Remove the masking tape before the sealant skins over (within about 15 minutes of tooling).
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EIFS Application Procedures
1. Allow the EIFS coating to dry a minimum of 24 hours prior to application of the DOWSIL™
sealant. The sealant joint should be applied to the base coat of the EIFS system. Do not apply
sealant to EIFS finish coat unless approved by the EIFS manufacturer. Drying time may be
greater, depending on temperature and humidity. Consult the EIFS manufacturer for
recommended drying time.
2. The joints must be clean and dry prior to installation of the DOWSIL™ sealant. If sealant is to be
applied immediately following the drying time of the EIFS coating, simply brush or wipe the
joint surfaces to ensure that there is no dust or debris in the joint. If the fully dried coating is
exposed for greater than one day, joint surfaces must either be wire brushed or blown with oil-
free compressed air or cleaned with a suitable solvent such as Isopropyl Alcohol (IPA) using the
“two cloth” cleaning method. Consult the EIFS manufacturer to determine if a specific solvent is
compatible with its system. Allow sufficient time for the solvent to evaporate prior to priming or
installing sealant.
3. Lightly apply DOWSIL™ 1200 OS Primer or other recommended primer with a soft bristle
brush to the inside of the joint. One brush wipe of the substrate should be sufficient. Allow the
primer to dry a minimum of one hour prior to backer rod installation.
4. Install either closed-cell polyethylene or non-gassing polyolefin backer rod with EIFS. Open-cell
polyurethane backer rod should not be used adjacent to EIFS surfaces.
Introduction
In some cases when an existing building is to be repaired or resealed, the existing weatherseal must be
removed before a new weatherseal can be installed. When a failed organic sealant is to be cut out and
replaced, the old sealant must be completely removed as described in the following paragraphs. When a
silicone weatherseal is to be replaced with a new silicone sealant, complete removal of the existing
functional joint may not be necessary. Follow the directions for removal and replacement of cured
silicone sealant.
Before starting a project to replace or repair failed organic sealant, it is recommended to complete a
mock-up demonstrating the procedures for removing the existing sealant and cleaning the substrates. In
addition, adhesion testing should be completed to determine whether or not a primer is required.
Follow this procedure to repair failed organic sealant with DOWSIL™ Silicone Building Sealant in
remedial applications:
1. Cut away the old sealant as close to the joint edges as possible.
2. Clean all joints of contaminants and impurities to the depth at which the new DOWSIL™ Silicone
Building Sealant and backer rod are to be installed. This may be accomplished by several
methods: abrading with a wire brush (power or hand), grinding, saw cutting or solvent cleaning.
3. Blow out dust, loose particles and other debris with moisture-free and oil-free compressed air;
6.0-kg/cm2 air pressure recommended; no moisture or oil allowed in air. (Occasionally, a second
pass with a wire brush and air blast is needed to ensure the joint is clean.) Loose pieces of caulk or
backer rod that have become lodged in the joint should also be removed.
4. After cleaning, the joints must be thoroughly dry, dust-free and frost-free before resealing.
5. Mask joint edges if possible to facilitate application and clean-up.
6. If priming is recommended, follow directions for applying the desired DOWSIL™ primer to the
cleaned surfaces before installing the DOWSIL™ Silicone Building Sealant.
7. Install back-up material in joints to proper design depth.
8. Apply the appropriate DOWSIL™ Silicone Building Sealant in a continuous operation to properly
fill and seal the joint width.
9. Using a blunt instrument, dry tool the joint so it is slightly concave. Tooling should be done as
soon as possible after sealant application. Remove masking as necessary.
10. Seal a test joint and check adhesion after curing 7 to 21 days.
1. If sealant is cured properly and performing in its application but its appearance is poor (e.g., due
to improper tooling), then cleaning the sealant surface with a solvent and recapping the joint should
be sufficient.
a. Clean sealant with a solvent (e.g., xylene, toluene) to remove dirt. Allow solvent
to evaporate.
b. Remask the joint.
c. Apply a thin bead of fresh sealant over the cured sealant.
73
d. Dry tool the sealant.
e. Remove the masking material.
2. If the sealant is mechanically damaged and a recapping will not improve the joint appearance, then
remove the section of old sealant and replace.
a. Cut away the old sealant. If excellent adhesion to the substrate is still maintained, then leave
some sealant at the edges of the joint (up to 0.08"/2 mm thick).
b. If adhesion to the substrate is poor, then remove sealant down to the substrate and
clean the substrate and recondition if necessary (i.e., clean with xylene and prime with
appropriate primer).
c. Mask the joint.
d. Reapply the sealant. (If resealing does not occur on the same day, the joint will have to be
recleaned using a solvent such as xylene or toluene before applying the fresh sealant.)
e. Dry tool the joint.
f. Remove the masking material.
g. Check adhesion after sealant has cured for 7–21 days.
Many flashings and fluid-applied membranes will discolor light sealants. Dow is available to test
compatibility of flashing and sealant upon request. For any asphaltic or bitumen-based flashing material,
Dow recommends a dark-colored sealant be used or the sealant be installed in a final nonvisible
location. Typically, sealant performance is not affected by the discoloration on the sealant.
High-performance coatings that act as corrosion inhibitors and primers may be used in these
applications. Dow recommends that coating manufacturers be contacted for recommendations.
Dow can complete adhesion testing on cured samples of specified coatings. DOWSIL™ 791
Silicone Weatherproofing Sealant or DOWSIL™ 795 Silicone Building Sealant have been
successfully used in these applications.
74
Sealant Interaction Considerations
Dow Silicone Sealants are specifically formulated to provide durable performance in weatherproofing
applications. Based on the highly developed reactive chemistries of our sealants, used in a vastly diverse
selection of substrates and potential variability in practices in the construction environment, Dow has
found unique situations that should be avoided to prevent interactions of our sealants during the cure
cycle. The following are important considerations specific to these unique instances.
DOWSIL™ 756 SMS Building Sealant may also display an aesthetic discoloration when NOT exposed
to sunlight or when cured in confinement. This discoloration generally dissipates upon exposure to
sunlight.
Product Quality
Dow performs extensive quality assurance testing in our manufacturing facilities in accordance with
rigid ISO 9000 standards. This section is intended to provide the end-user with simple screening tests
to verify that the material, as received and used at the job site on actual substrates, will perform
as intended.
75
This test is performed as follows:
76
Standard Field Adhesion Test
The field adhesion test is a simple screening procedure that may help detect application problems such
as improper cleaning, use of improper primer, poor primer application or improper joint configuration.
As a check for adhesion, a simple hand pull test is required at the job site after the sealant is fully cured
(usually within 7 to 21 days.) Field adhesion testing should be documented using the Field Adhesion
Testing Log. It is suggested that 5 tests for the first 1000' (300 meters) and 1 test per 1000' (300 meters)
thereafter be submitted or 1 test per floor per elevation. The hand pull test procedure is as follows:
NOTE for DOWSIL™ 758 Silicone Weather Barrier Sealant: When field adhesion testing with
DOWSIL™ 758 Silicone Weather Barrier Sealant, please be aware of the unique behavior of this
sealant. No sealant should be pulled on at high speed, but in particular, DOWSIL™ 758 Silicone
Weather Barrier Sealant should be pulled slowly at 90 degrees in order to avoid a false negative result.
77
Field Adhesion Hand Pull Test Criteria
78
Peel-in-Adhesion Test Procedure
Another simple screening test can be done on a flat test surface. A test piece like that shown
is recommended.
Therefore, it is suggested that these quality assurance logs be kept together with the project files. A
hardcover logbook may be preferential to copies of the logs suggested here. A quality assurance
engineer should be responsible for documenting this data on a job-to-job basis. All curtainwall units
must be numbered so the sealant installation dates, sealant lot numbers and quality assurance testing
can be obtained from the project log.
Dow will be happy to assist you during the implementation of this quality control program.
If you have any questions, contact your local Dow Field Specialist or authorized building sealant
distributor.
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Warranty – Weatherproofing Applications
All warranties are dependent on the successful completion of Dow requirements. These requirements
include, but are not limited to:
At time of shipment, the DOWSIL™ sealant product(s) are warranted that the sealant product(s) will
meet the Dow sales specification. For further details on requirements and limitations of this limited
warranty, consult the DOWSIL™ product data sheet for the sealant product(s) in use.
Dow also offers project-specific performance warranties for sealant products used in weatherproofing
applications. These project-specific performance warranties carry various warranty terms (up to 20
years) and remedies. Specific requirements must be met to qualify for a performance warranty. Dow
does not offer project-specific warranties on projects where wood is a primary substrate.
For details on how to obtain the applicable project-specific performance warranty, please consult your
local Dow Field Specialist or authorized building sealant distributor.
Quality assurance requirements for a performance (weatherproofing) warranty include, but are
not limited to:
1. Confirmation of adhesion is required for each substrate that contacts the approved DOWSIL™
weatherproofing sealant. Reference the Surface Preparation Guide within this manual (page 7).
2. Field Testing documentation log book(s) show that a sufficient amount of testing was done. The
minimum testing is per ASTM C1521-02, section 7.3.3, which states, “For each area to be
inspected, perform procedure every 100 linear ft in the first 1,000 linear ft of joint. If no test
failure is observed in the first 1,000 ft of joint, perform procedure every 1,000 linear ft thereafter
or approximately once per floor per elevation.” The contractor should determine other job-
specific needs. The contractor should complete and fill out the log to demonstrate that acceptable
adhesion and joint design were obtained in actual use. This is in addition to the adhesion
documentation noted in #1.
3. The contractor documents and retains all required quality assurance documentation and, upon
completion of the project, provides a copy to the owner. This documentation must be retained for
this warranty to be valid and will be required should any claims arise in the future. The owner
must retain the quality assurance documentation along with the Dow-issued warranty.
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Field/Shop Adhesion Testing Log
Project:
Sealant:
Test
Acceptable
Location Primed
Sealant Acceptable Adhesion Comments/
Date Applied by (Elevation, (Y/N)
Test Date Color and Joint Fill (Y/N) and Tester
Applied (Initials) Unit Primer Lot
Lot # (Y/N) % Initials
Number, #
Elongation
etc.)
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Product Quality Control Log – One-Part Silicone Sealants
Project:
Location/Elevation/Unit ID:
Sealant Color:
Sealant Lot
Tack-Free Time Cured After 24 Elastomeric
Date Time Tester Initials Number/
(Minutes) Hours (Y/N) (Y/N)
Color
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Product Quality Control Log – Two-Part Silicone Sealants
Project:
Location:
Sealant Color:
Sealant Lot
Temperature/ Tester Number (Base)/ Snap Time
Date Time Butterfly Test Comments
Humidity Initials Lot Number (Minutes)
(Catalyst)/Color
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Appendix A: Cure Inhibition of DOWSIL™ 790 Silicone Building
Sealant
This appendix covers the subject of the potential for DOWSIL™ 790 Silicone Building Sealant to be
cure inhibited. More than any other DOWSIL™ sealant, cure inhibition can be a real cause for concern
with DOWSIL™ 790 Silicone Building Sealant. We’ll talk about why, but first let’s take a few moments
to talk about this unique sealant.
DOWSIL™ 790 Silicone Building Sealant’s unique chemistry also causes this sealant to cure slower
than some other sealants, and this contributes to why we strongly suggest using an open-cell backer
rod with this product when being installed against non-porous substrates. With the exception of EIFS,
open-cell backer rod is preferable for DOWSIL™ 790 Silicone Building Sealant use on porous
substrates as well.
Cure Inhibition
It is also this unique chemistry that makes DOWSIL™ 790 Silicone Building Sealant especially
susceptible to cure inhibition. A partial list of inhibiting items includes:
• Any alcohol – isopropyl alcohol (IPA), ethyl alcohol, butyl alcohol, etc. Alcohols may be used
for cleaning but should be allowed to fully flash or dry prior to sealant installation. Use of
alcohols as a cleaner on porous substrates is typically not recommended because it can be
difficult to judge when the alcohol is fully flashed or dry.
• Many other solvents – acetone, methyl ethyl ketone (MEK), methyl isobutyl ketone (MIBK), etc.
• Solvent-containing materials – incompletely cured primers, incompletely dried paints, etc.
• Some kinds of release agents – solvent-containing products, materials containing glycols
of any kind, etc.
• Many types of substrates – some Synergy EIFS products, some EPOXY substrates (any EPOXY
material should be tested), any porous substrate cleaned with a solvent that has not had sufficient
“flash-off” time, etc.
Conditions that should be avoided when working with DOWSIL™ 790 Silicone
Building Sealant:
• DO NOT “wet tool” with solvents or soaps, as this can inhibit the surface of this sealant. The
rest of the sealant bulk may cure normally, but the surface will remain tacky and gummy
indefinitely.
• DO NOT apply this sealant to a backer rod that is contaminated with solvent or primer.
• DO NOT apply this sealant to a surface that has been cleaned with a solvent that has not been
allowed to completely dry.
• DO NOT apply this sealant to EPOXY-containing surfaces (unless they have been tested by the
Dow Americas Construction Test Lab), since they can inhibit the cure.
84
• DO NOT apply this sealant wet to wet with any of the other Dow branded sealants as they can
inhibit the cure. Care should be taken to ensure a minium of 3-5 days of curing of the sealant
installed first prior to installing the second sealant.
85
Appendix B: Use of DOWSIL™ Sealants with Weathered
Lock-Strip Gasket Systems
Lock-Strip Wet Seal Joint
Good Joint Design Poor Joint Design
Dow has evaluated sealants for use as a perimeter weatherseal for weathered and leaking
lock-strip or zipper gasket systems. For our evaluation, various weathered gaskets aged 10 years and
older were collected. DOWSIL™ sealants were tested for adhesion in simulated fillet bead wet seal
joints for several thousand hours of UV exposure and accelerated QUV weatherometer exposure. After
this exposure, both DOWSIL™ 791 Silicone Weatherproofing Sealant and DOWSIL™ 795 Silicone
Building Sealant have demonstrated excellent adhesion characteristics to the weathered gasket and glass.
As a result of this evaluation, Dow recommends the following steps to properly repair and seal leaking
lock-strip or zipper gaskets systems using our silicone sealants:
• Use either DOWSIL™ 791 Silicone Weatherproofing Sealant or DOWSIL™ 795 Silicone
Building Sealant. To minimize sealant discoloration from the gasket, use a dark-colored sealant.
• Solvent clean the glass and metal using the two-cloth wipe method described on page 70.
• Prime both the glass and gasket surface to receive sealant with DOWSIL™ 1200 OS Primer.
• Perform a field adhesion test prior to job start-up and/or after application to verify proper sealant
adhesion in job-site conditions.
• Install the sealant in a fillet bead with a minimum of 1/4" contact on both the glass and
lock-strip gasket.
86
Appendix C: Winter/Summer Considerations
Silicone sealants can be applied in subfreezing temperatures, provided the substrate is frost- and
moisture-free. Although cure will be slower in colder temperatures, adhesion will be acceptable.
DOWSIL™ 795 Silicone Building Sealant, DOWSIL™ 995 Silicone Structural Sealant, DOWSIL™
756 SMS Building Sealant, DOWSIL™ 791 Silicone Weatherproofing Sealant, DOWSIL™ 790
Silicone Building Sealant and DOWSIL™ 758 Silicone Weather Barrier Sealant have wider installation
temperature ranges and are more suitable for use in cold temperatures than organic sealant technologies.
All of these DOWSIL™ sealants can be applied to substrates within a temperature range of -29 to 49°C
(-20 to 120°F) 1. If lower or higher application temperatures are needed, please contact Dow to discuss
appropriate sealants. IPA and MEK are soluble in water and may be more appropriate for winter
cleaning because they help in removing condensation and frost. Xylene and toluene are not soluble in
water and may be better suited for warm-weather cleaning. All surfaces must be free of moisture,
condensation, morning dew and frost conditions prior to installation. (USE CAUTION WITH
ALCOHOL-TYPE CLEANERS WITH DOWSIL™ 790 Silicone Building Sealant.)
At colder temperatures (below 4°C/40°F), substrates should be inspected for frost, which must be
removed. Daily inspections are strongly recommended to review these cold-weather conditions and
correct with proper cleaning. Maintain a log, reviewing and recording low-temperature start-up
conditions. Please allow longer curing time prior to performing field adhesion testing. Contact your
Dow Application Sales Engineer for assistance.
At warmer temperatures (above 32°C/90°F), the solvent may flash prematurely and result in
poor cleaning. Xylene and toluene are slower-drying solvents and may be preferred for cleaning
warmer substrates.
1DOWSIL™ 995 Silicone Structural Sealant can be applied at temperatures up to 140°F. Refer to the product data sheet
for more information.
87
Learn More
Please visit consumer.dow.com/construction
for additional information.
Your exclusive remedy for breach of such warranty is limited to refund of purchase price or
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TO THE FULLEST EXTENT PERMITTED BY APPLICABLE LAW, DOW
LIMITED WARRANTY INFORMATION – PLEASE READ CAREFULLY SPECIFICALLY DISCLAIMS ANY OTHER EXPRESS OR IMPLIED WARRANTY OF
FITNESS FOR A PARTICULAR PURPOSE OR MERCHANTABILITY.
The information contained herein is offered in good faith and is believed to be accurate. However,
because conditions and methods of use of our products are beyond our control, this information DOW DISCLAIMS LIABILITY FOR ANY INCIDENTAL OR CONSEQUENTIAL
should not be used in substitution for customer’s tests to ensure that our products are safe, effective DAMAGES.
and fully satisfactory for the intended end use. Suggestions of use shall not be taken as inducements ®
™ Trademark of The Dow Chemical Company ("Dow") or an affiliated company of Dow
to infringe any patent.
© 2018 The Dow Chemical Company. All rights reserved.
Dow’s sole warranty is that our products will meet the sales specifications in effect at the time of
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shipment.