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    CRM PPC Blaines

    Uploaded by

    Vara Prasad Paluri
    This document provides a certificate of analysis for BND 5002, an Indian reference material for calibrating Blaine air permeability apparatus. The certified value for the specific surface area is 393 m2/kg with an expanded uncertainty of ±9.38 m2/kg. BND 5002 consists of Portland pozzolana cement powder in sealed glass vials and is traceable to SI units. Instructions are provided for proper storage, handling, and use of the reference material.

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    © All Rights Reserved
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    CRM PPC Blaines

    Uploaded by

    Vara Prasad Paluri
    46 views2 pages
    This document provides a certificate of analysis for BND 5002, an Indian reference material for calibrating Blaine air permeability apparatus. The certified value for the specific surface area is 393 m2/kg with an expanded uncertainty of ±9.38 m2/kg. BND 5002 consists of Portland pozzolana cement powder in sealed glass vials and is traceable to SI units. Instructions are provided for proper storage, handling, and use of the reference material.

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    Crm Ppc Blaines

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    This document provides a certificate of analysis for BND 5002, an Indian reference material for calibrating Blaine air permeability apparatus. The certified value for the specific surface area is 393 m2/kg with an expanded uncertainty of ±9.38 m2/kg. BND 5002 consists of Portland pozzolana cement powder in sealed glass vials and is traceable to SI units. Instructions are provided for proper storage, handling, and use of the reference material.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    46 views2 pages

    CRM PPC Blaines

    Uploaded by

    Vara Prasad Paluri
    This document provides a certificate of analysis for BND 5002, an Indian reference material for calibrating Blaine air permeability apparatus. The certified value for the specific surface area is 393 m2/kg with an expanded uncertainty of ±9.38 m2/kg. BND 5002 consists of Portland pozzolana cement powder in sealed glass vials and is traceable to SI units. Instructions are provided for proper storage, handling, and use of the reference material.

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    ertified

    Reference nce Materia


    AND
    BHARATNA NIRDESHAK DRAVYA BND
    NCB C A L

    TIONAL PHYSICA
    artilya Nirdeshar
    LABORATORY
    k
    NMIO
    D r a v y a

    (INDIAN REFERENCE MATERIAL)


    OILYN
    5IT Certificate of Analysis
    BND 5002
    FINENESS STANDARD
    PORTLAND POZZOLANA CEMENT
    t 9.38 m°/kg
    NCB Specific surface area (Blaine): 393 m/kg
    Certificate number: BND
    5002/a4

    a Certified Reference Material (CRM),


    This Bharatiya Nirdeshak Dravya (BND 5002),
    Cement and Building Materials (NCB), India
    has been developed by National Council for
    in-house secondary
    for calibrating Blaine Air Permeability Apparatus, developing
    of analysts, according
    reference materials for routine control and evaluating proficiency
    5002 consists of 4 sealed
    to Indian Standard IS 4031 (part 2)-1999. One set of BND
    -

    of powdered Portland Pozzolana


    glass vials and each vial contains approximately 10g
    Cement.

    expanded uncertainty, estimated with known


    Certified Value: The certified value and its
    sources of bias, is given below:
    ESTIMATION METHOD CERTIFIED VALUE AND
    MEASURAND
    EXPANDED UNCERTAINTYY
    Specific surface area (Blaine) IS4031 (Part 2):1999 393 m/kg t 9.38 m/kg
    The certified value has been standardized with a specific gravity of 2.83
    surface area is estimated
    The expanded uncertainty of the certified value for specific
    in Measurement (GUM) at
    according to the Guide to the expression of Uncertainty
    95.45% confidence level. The uncertainty includes the measurement variability among
    the testing laboratories, material inhomogeneity, latter controlled through statistical
    means (ISO 13528:2015). The specific surface (Blaine) is the best estimate of true value
    based on the results of analytical programme carried out in three NCB laboratories.

    Traceability: The BND 5002 is metrologically traceable to SI units through Indian


    national measurement standards at CSIR-National Physical Laboratory (National
    Measurement Institute of India). All measurements have been carried out to establish
    traceability through an unbroken chain of comparisons, having stated uncertainty.

    Nature of Material: Non-hazardous

    Date of Certification: 23rd October 2018

    Page 1 of 2
    Instructions for Storage and Use and Precautions for Handling:
    1. BND 5002 CRM should be used in controlled conditions, using calibrated equipment, by
    trained personnel.
    2. TheBlaine cell calibrated for bed volume, preferably by an accredited laboratory, must be
    used.
    3. Before use, shake the material vigorously for 2 minutes in a suitable jar to break any lump
    or agglomerate. Wait for 2 minutes and then stir with a clean rod in order to distribute the
    fines throughout the material.
    4. The material should be stored under non-humid conditions to avoid any ingress of
    moisture/CO. One vial is sufficient for carrying out one time calibration for apparatus
    constant, taking measurements on three compacted beds, as required in IS 4031 (Part 2)-
    1999. Leftover portion in a vial, if any, should not be used at a later date.
    5. For standardization, prepare the bed of this CRM (standard sample) using 0.50 porosity.
    Alternatively, make a firm bed by trial method.
    6. Porosity of the test sample will have to be determined by trial method using the following
    equation given in IS 4031 (Part 2)-1999, for calculating specific surface oftest sample:
    W pV1-e)
    7. Specific gravity of test sample and CRM being almost same (in Indian cements), the
    application of above CRM simplifies calculation of apparatus constant for PPC and
    provides greater degree of accuracy in results.
    8. Record of usage of CRM and the results must be maintained.

    Expiration of Certification: The certification of BND 5002 is valid, within the measurement
    uncertainty specified, until 30h September 2023, provided the CRM is handled and stored in
    accordance with instructions given in this certificate. The certificate will be treated as
    nullified if the storage and handling instructions are not followed.

    Maintenance of Certification: NCB will monitor this BND over the period of its
    certification. If substantive technical changes occur that affect the certification before the
    expiration of certification, NCB will notify the purchaser.

    Accredited as per
    BND 5002/ASet released from NCB stock on: ISO 17034:2016 vide
    Certificate No. RC-1016
    Authorized by:

    Dr. R. P. Pant Sh. P. N. 0jha


    Head, BND Division Head of Centre
    CSIR-National Physical Laboratory Center for Quality Management,
    Dr. K. S. Krishnan Marg Standards and Calibration Services
    New Delhi-110012

    For further Information, please contact: National Council for Cement and Building Materials
    34 Km. Stone, Delhi-Mathura Road (NH-2), Ballabgarh, Haryana - 121004, India;

    Phone +91-129-4192239/303, +91-129-2242051, +91-129-4192222; Fax +91-129-2242100, +91-129-2246175


    Email: ncb.cqc@gmail.com, nccbm@ncbindia.com, info@ncbindia.com website: www.ncbindia.com

    This certificate shall not be reproduced without written approval from CSIR-NPL, Delhi
    Responsibilities for issue and release of this certificate lie with National Council for Cement and

    Building Materials.

    Page 2 of2

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