Astm E1820
Astm E1820
Astm E1820
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
NOTE 1—Construction lines drawn parallel to the elastic loading slope to give vp, the plastic component of total displacement, vg.
NOTE 2—In curves b and d, the behavior after pop-in is a function of machine/specimen compliance, instrument response, etc.
FIG. 1 Types of Force versus Clip Gage Displacement Records
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
formulas presented in this test method are applicable over the a greater working range is needed, an enlarged gage such as the
range of crack size and specimen sizes within the scope of this one shown in Fig. 3 is recommended. Accuracy shall be within
test method. 61 % of the full working range. In calibration, the maximum
deviation of the individual data points from a fit (linear or
5. Significance and Use curve) to the data shall be less than 60.2 % of the working
5.1 Assuming the presence of a preexisting, sharp, fatigue range of the gage when using the elastic compliance method
crack, the material fracture toughness values identified by this and 61 % otherwise. Knife edges are required for seating the
test method characterize its resistance to: (1) fracture of a gage. Parallel alignment of the knife edges shall be maintained
stationary crack, (2) fracture after some stable tearing, (3) to within 1°. Direct methods for load-line displacement are
stable tearing onset, and (4) sustained stable tearing. This test described in Refs (2-5).
FIG. 2 Double-Cantilever Clip-In Displacement Gage Mounted by Means of Integral Knife Edges
NOTE 1—The crack-starter notch shall be centered between the top and bottom specimen edges within 0.005 W.
FIG. 7 Envelope of Fatigue Crack and Crack Starter Notches
sfYS the wide notch or 0.6 mm (0.024 in.) for the narrow notch,
KMAX 5 ~0.063sfYS MPa=m! (6)
sTYS whichever is less, the maximum stress intensity that may be
or applied to the specimen shall be given by:
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
distinguish but should be defined on one side by the fatigue 8.6.3.1 Measure compliance to estimate the original crack
precrack and on the other by the brittle region. Proceed to 9 to size, ao, using unloading/reloading sequences in a force range
evaluate fracture toughness in terms of K, J, or CTOD. from 0.5 to 1.0 times the maximum precracking force. Estimate
8.4.4 If stable tearing occurs, test additional specimens to a provisional initial crack size, aoq, from at least three
evaluate an initiation value of the toughness. Use the procedure unloading/reloading sequences. No individual value shall differ
in 8.5 to evaluate the amount of stable tearing that has occurred from the mean by more than 60.002 W.
and thus determine the displacement levels needed in the 8.6.3.2 Proceed with the test using unload/reload sequences
additional tests. Five or more points favorably positioned are that produce crack extension measurements at intervals pre-
required to generate an R curve for evaluating an initiation scribed by the applicable data analysis section of Annex A8 or
point. See Annex A9 and Annex A11 to see how points shall be Annex A10. Note that at least eight data points are required
positioned for evaluating an initiation toughness value. before specimen achieves maximum force. If fracture instabil-
8.5 Optical Crack Size Measurement: ity is an expected response, then it may be helpful to load the
8.5.1 After unloading the specimen, mark the crack accord- specimen monotonically over the range Pm< P < PQ. (See
ing to one of the following methods. For steels and titanium Annex A5 for a definition of PQ). If crack size values change
alloys, heat tinting at about 300°C (570°F) for 30 min works negatively by more than 0.005 ao(backup), stop the test and
well. For other materials, fatigue cycling can be used. The use check the alignment of the loading train. Crack size values
of liquid penetrants is not recommended. For both recom- determined at forces lower than the maximum precracking
mended methods, the beginning of stable crack extension is force should be ignored.
marked by the end of the flat fatigue precracked area. The end 8.6.3.3 For many materials, load relaxation may occur prior
of crack extension is marked by the end of heat tint or the to conducting compliance measurements, causing a time-
beginning of the second flat fatigue area. dependent nonlinearity in the unloading slope. One method
8.5.2 Break the specimen to expose the crack, with care that may be used to remedy this effect is to hold the specimen
taken to minimize additional deformation. Cooling ferritic steel for a period of time until the force becomes stable at a constant
specimens to ensure brittle behavior may be helpful. Cooling displacement prior to initiating the unloading.
nonferritic materials may help to minimize deformation during
8.6.3.4 The maximum recommended range of unload/reload
final fracture.
for crack extension measurement should not exceed either
8.5.3 Along the front of the fatigue crack and the front of the
50 % of Pm or 50 % of the current force, whichever is smaller.
marked region of stable crack extension, measure the length of
the original crack and the final physical crack length at nine 8.6.3.5 After completing the final unloading cycle, return
equally spaced points centered about the specimen centerline the force to zero without additional crosshead displacement
and extending to 0.005 W from the root of the side groove or beyond the then current maximum displacement.
surface of smooth-sided specimens. Calculate the original 8.6.3.6 After unloading the specimen, use the procedure in
crack size, ao, and the final physical crack size, ap, as follows: 8.5 to optically measure the crack sizes.
average the two near-surface measurements, combine the result 8.7 Alternative Methods:
with the remaining seven crack length measurements and 8.7.1 Alternative methods of measuring crack extension,
determine the average. Calculate the physical crack extension, such as the electric potential drop method, are allowed.
Dap = ap − ao. The measuring instrument shall have an accu- Methods shall meet the qualification criteria given in 9.1.5.2. If
racy of 0.025 mm (0.001 in.). an alternative method is used to obtain JIc, at least one
8.5.4 None of the nine measurements of original crack size additional, confirmatory specimen shall be tested at the same
and final physical crack size may differ by more than 0.05B test rate and under the same test conditions. From the alterna-
from the average physical crack size defined in 8.5.3. tive method the load line displacement corresponding to a
8.6 Resistance Curve Procedure: ductile crack extension of 0.5 mm shall be estimated. The
8.6.1 The resistance curve procedure involves using an additional specimen shall then be loaded to this load line
elastic compliance technique or other technique to obtain the J displacement level, marked, broken open and the ductile crack
or CTOD resistance curve from a single specimen test. The growth measured. The measured crack extension shall be 0.5 6
elastic compliance technique is described here, while the 0.25 mm in order for these results, and hence the JIc value, to
normalization technique is described in Annex A15. be qualified according to this method.
8.6.2 Load the specimens under the displacement gage or 8.7.2 If displacement measurements are made in a plane
machine crosshead or actuator displacement control. Load the other than that containing the load line, the ability to infer
specimens at a rate such that the time taken to reach the force load-line displacement shall be demonstrated using the test
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
9.1.4.1 Original Crack Size—None of the nine physical tions (Section 9),
measurements of initial crack size defined in 8.5.3 shall differ 10.2.7 If the loading rate is other than quasi-static, report the
by more than 0.05B from the average ao. applied dK/dt,
9.1.4.2 Final Crack Size—None of the nine physical mea- 10.2.8 Original measured crack size, ao (8.5), original
surements of final physical crack size, ap, defined in 8.5.3 shall predicted crack size, aoq, final measured crack size, ap, final
differ by more than 0.05B from the average ap. In subsequent predicted crack extension, Dapredicted, physical crack extension
tests, the side-groove configuration may be modified within the during test, Dap, crack front appearance—straightness and
requirements of 7.5 to facilitate meeting this requirement. planarity, and fracture appearance,
9.1.5 The following crack size requirements shall be met in 10.2.9 Qualification of fracture toughness measurement
the tests using the resistance curve procedure of 8.6. (Annex A4-Annex A7 and Annex A8-Annex A11), based on
9.1.5.1 Crack Extension—None of the nine physical mea- size requirements, and based on crack extension, and
surements of crack extension shall be less than 50 % of the 10.2.10 Qualified values of fracture toughness, including
average crack extension. R-curve values.
9.1.5.2 Crack Extension Prediction—The crack extension,
Dapredicted, predicted from elastic compliance (or other 11. Precision and Bias
method), at the last unloading shall be compared with the 11.1 Bias—There is no accepted “standard” value for any of
measured physical crack extension, Dap. The difference be- the fracture toughness criteria employed in this test method. In
tween these shall not exceed 0.15 Dap for crack extensions less the absence of such a true value no meaningful statement can
than 0.2 bo, and the difference shall not exceed 0.03 bo be made concerning bias of data.
thereafter. 11.2 Precision—The precision of any of the various fracture
9.2 Fracture Instability—When the test terminates with a toughness determinations cited in this test method is a function
fracture instability, evaluate whether the fracture occurred of the precision and bias of the various measurements of linear
before stable tearing or after stable tearing. The beginning of dimensions of the specimen and testing fixtures, the precision
stable tearing is defined in A6.3 and A7.3. For fracture of the displacement measurement, the bias of the force mea-
instability occurring before stable tearing proceed to Annex surement as well as the bias of the recording devices used to
A5, Annex A6, and Annex A7 to evaluate the toughness values produce the force-displacement record, and the precision of the
in terms of K, J, or CTOD. For fracture instability occurring constructions made on this record. It is not possible to make
after stable tearing, proceed to Annex A5, Annex A6, and meaningful statements concerning precision and bias for all
Annex A7 to evaluate toughness values and then go to 9.3 to these measurements. However, it is possible to derive useful
evaluate stable tearing. information concerning the precision of fracture toughness
9.3 Stable Tearing: measurements in a global sense from interlaboratory test
9.3.1 Basic Procedure—When the basic procedure is used, programs. Most of the measures of fracture toughness that can
only an initiation toughness can be evaluated. Proceed to be determined by this procedure have been evaluated by an
Annex A9 and Annex A11 to evaluate initiation toughness interlaboratory test program. The KIc was evaluated in (8), JIc
values. was evaluated in (9), the J-R curve was evaluated in (10), and
K Based Fracture
KIc = [MPa-m1/2]
KJIc = [MPa-m1/2]
J Based Fracture
Jc = [kJ/m2]
JIc = [kJ/m2]
Ju = [kJ/m2]
d Based Results
dc* = [mm]
dIc = [mm]
dc = [mm]
du = [mm]
Final Da/b =
Final Jmax/sYS = [mm]
Specimen Information
Type =
Identification =
Orientation =
Basic dimensions
B = [mm]
BN = [mm]
W = [mm]
aN(Notch Length) = [mm]
Particular dimensions
C(T) H = [mm]
SE(B) S = [mm]
DC(T) D = [mm]
Material
Material designation =
Form =
Tensile Properties
E (Young’s modulus) = [MPa]
n (Poisson’s ratio) =
sYS (Yield Strength) = [MPa]
sTS (Ultimate Strength) = [MPa]
Precracking Information
Final Pmax = [N]
Final Pmin = [N]
Pm = [N]
Final DK/E = [MPa-m1/2]
Fatigue temperature = [°C]
Fatigue crack growth information
4
Supporting data have been filed at ASTM International Headquarters and may
FIG. 8 Suggested Data Reporting Format be obtained by requesting Research Report RR: E24-1013.
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
ANNEXES
(Mandatory Information)
NOTE A1.1—Annex A1-Annex A3 cover specimen information. ing with a support span, S, equal to four times the width, W.
The general proportions of the specimen configuration are
A1.1 Specimen
shown in Fig. A1.1.
A1.1.1 The standard bend specimen is a single edge-
notched and fatigue-cracked beam loaded in three-point bend-
NOTE 1—The two side planes and the two edge planes shall be parallel and perpendicular as applicable to within 0.5°.
NOTE 2—The machined notch shall be perpendicular to specimen length and thickness to within 62°.
FIG. A1.1 Recommended Single Edge Bend [SE(B)] Specimen
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
S ai
2 1 1 2W DS ai
12W D 3/2 All basic test method J integral values shall be corrected for
crack growth using the procedure of Annex A16.
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
where:
A1.4.2.2 J Calculations for the Resistance Curve Test vpl(i) = plastic part of the load-line displacement = n(i)−
Method—At a point corresponding to a(i), v(i), and P(i) on the (P(i)CLL(i)), and
specimen force versus load-line displacement record, calculate CLL(i) = experimental compliance, (Dv/DP)(i), correspond-
the J integral as follows: ing to the current crack size, ai.
~K~i!! 2 ~1 2 v2! For test methods that do not evaluate an experimental
J ~i! 5 E 1 Jpl~i! (A1.7) load-line elastic compliance, the load line displacement CLL(i)
where K(i) is from A1.4.1, and can be determined from the following equation:
Jpl~i! 5 J pl~i21! 1 b
~i21!
F S DS
hpl Apl~i! 2 A pl~i21!
BN DGF G
a~i! 2 a~i21!
1 2 gpl b
~i21!
1
S S
C LL~i! 5 EB W 2 a
e i
D 2
(A1.10)
(A1.8)
F ai
SD ai
1.193 2 1.98 W 1 4.478 W SD 2
SDai
2 4.443 W
3
S DG
ai
1 1.739 W
4
Where:
hpl = 1.9 and where:
gpl = 0.9; Be = B − (B − BN)2/B
In Eq A1.8, the quantity Apl(i) − Apl(i–1) is the increment of The compliance estimated using Eq A1.10 should be verified
plastic area under the force versus load-line displacement by calibrating against the initial experimental load versus load
record between lines of constant displacement at points i−1 and line displacement data to assure the integrity of the load line
i shown in Fig. A1.3. The quantity Jpl(i) represents the total displacement measurement system.
crack growth corrected plastic J at point i and is obtained in A1.4.2.3 J Calculations for the Resistance Curve Test
two steps by first incrementing the existing J pl(i-1) and then by Method—Crack Mouth Opening Displacement—At a point
modifying the total accumulated result to account for the crack corresponding to ai, n(i), and P(i) on the specimen force versus
growth increment. Accurate evaluation of Jpl(i) from the Eq crack mouth opening displacement record calculate the J
A1.8 relationship requires small and uniform crack growth
integral as follows:
increments consistent with the suggested elastic compliance
spacing of Annex A8 and Annex A10. The quantity Apl(i) can be ~K~i!!2 ~1 2 n2!
J ~i! 5 1 Jpl~i! (A1.11)
calculated from the following equation: E
Apl~i! 5 Apl~i21! 1 [P ~i! 1 P ~i21!# [vpl~i! 2 vpl~i21!#/2 (A1.9) where K(i) is from A1.4.1, and
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
2 3
W 5 [0.999748 2 3.9504u 1 2.9821u 2 3.21408u
Calculation of d requires sYS/sTS$ 0.5.
1 51.51564u 4 2 113.031u5# (A1.13) A1.4.5.2 Calculations of CTOD for the Resistance Curve
where: Test Method—For the resistance curve test method, calcula-
1 tions of CTOD for any point on the force-displacement curve
u 5 B WEC (A1.14)
e
F
S/4
i
G 1/2
11
are made from the following expression:
Ji
di 5 m s (A1.17)
i Y
Ci = (Dvm/DP) on an unloading/reloading sequence, where Ji is defined in A1.4.2.2 or A1.4.2.3 with a = ai, the
vm = crack opening displacement at notched edge, current crack size and:
Be = B − (B − BN)2/B.
NOTE A1.3—Crack size on a single edge bend specimen is normally
sYS
m 5 A0–A1* s
TS
S D
sYS 2
1 A2* s
TS
sYS
–A3* s
TS
S D S D 3
(A1.18)
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
FIG. A2.1 Two Compact Specimen Designs That Have Been Used Successfully for Fracture Toughness Testing
A2.4.2 Calculation of J—For the compact specimen calcu- The load line compliance estimated using Eq A1.10 should
late J as follows: be verified by calibrating against the initial experimental
J 5 Jel 1 Jpl (A2.4) compliance to assure the integrity of the load line displacement
measurement system.
where:
Jel = elastic component of J, and
Jpl = plastic component of J.
NOTE 1—A surfaces shall be perpendicular and parallel as applicable to within 0.002 W TIR.
NOTE 2—The intersection of the crack starter notch tips with the two specimen surfaces shall be equally distant from the top and bottom edges of the
specimen within 0.005 W.
NOTE 3—Integral or attachable knife edges for clip gage attachment to the crack mouth may be used.
NOTE 4—For starter-notch and fatigue-crack configuration see Fig. 7.
FIG. A2.2 Compact Specimen for KIc Testing
A2.4.2.1 J Calculations for the Basic Test Method—For the where K(i) is from A2.4.1, and:
compact specimen at a point corresponding to n, P on the J pl~i! 5 (A2.8)
specimen force versus load-line displacement record calculate
as follows:
K2~1 2 n2!
F S D
h ~i21! Apl~i! 2 Apl~i21!
Jpl~i21! 1 b
~i21! BN GF 1 2 g~i21!
a~i! 2 a~i21!
b~i21! G
J5 1 Jpl (A2.5)
E where:
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
u 5 sin 21
F S dm
2 1D D
~D 1 R 2!1/2
2
G SDD
2 tan21 R , and (A2.15)
are made from the following expression:
Ji
di 5 ms
Y
(A2.18)
S D
sYS
m 5 A0–A1* s
TS
1 A2* s S D
sYS 2
TS
S D
sYS
–A3* s
TS
3
(A2.19)
NOTE 1—All surfaces shall be perpendicular and parallel as applicable within 0.002 W TIR.
NOTE 2—The intersection of the crack starter notch tips on each surface of the specimen shall be equally distant within 0.005W from the centerline
of the loading holes.
NOTE 3—Integral or attached knife edges for clip gage attachment to the crack mouth may be used.
NOTE 4—For starter-notch and fatigue-crack configuration see Fig. 7.
NOTE 5—Required circularity measurements shall be made at eight equally spaced points around the circumference. One of these points shall be the
notch plane. Average the readings to obtain the radius. All values shall be within 5 % of the average.
FIG. A3.1 Disk-Shaped Compact Specimen, DC(T), Standard Proportions and Dimensions
FS ai
21W DS SD ai
SD
ai ai
0.76 1 4.8 W 2 11.58 W 1 11.43 W
2
SD 3 ai
2 4.08 W S D DG
4
where:
12WS D
ai 3/2 npl(i) = plastic part of the load-line displacement,
ni − (PiCLL(i)), and
CLL(i) = experimental compliance, (Dn/DP)i correspond-
A3.5.2 Calculation of J—For the DC(T) specimen, calcu-
ing to the current crack size, ai.
late J as follows:
For test methods that do not evaluate an experimental elastic
J 5 Jel 1 J pl (A3.4)
compliance, CLL(i) can be determined from the following
where: equation:
Jel = elastic component of J, and a~i! 2
1 2
Jpl = plastic component of J. 1 11 W
A3.5.2.1 J Calculation for the Basic Test Method—For the CLL~i! 5 EB a~i! 3 (A3.10)
e
DC(T) specimen at a point corresponding to n(i), P(i) on the 12 W
specimen force versus load-line displacement record calculate
as follows: F a~i!
S D a~i!
2.0462 1 9.6496 W 2 13.7346 W S D 2
S DG
a~i!
1 6.1748 W
3
K2~1 2 n 2!
J5 E 1 Jpl (A3.5) where:
Be = B − (B − B N)2/B.
where K is from A3.5.1 with a = ao, and
The compliance estimated using Eq A1.10 should be verified
hApl
Jpl 5 B b (A3.6) by calibrating against the initial experimental compliance to
N o
assure the integrity of the load line displacement measurement
where: system.
Apl = Area A as shown in Fig. A1.2, In an elastic compliance test, the rotation corrected compli-
BN = net specimen thickness (BN = B if no side grooves ance, Cc(i), described in A3.5.4 shall be used instead of CLL(i)
are present), given above.
bo = uncracked ligament, (W − a o), and
h = 2 + 0.522bo/W. A3.5.3 Calculation of Crack Size—For a single-specimen
All basic test method J integral values shall be corrected for test method using an elastic compliance technique on DC(T)
crack growth using the procedure of Annex A16. specimens with crack opening displacements measured at the
A3.5.2.2 J Calculation for the Resistance Curve Test load-line, the crack size is given as follows:
Method—For the DC(T) specimen at a point corresponding to a~i! 2 3
ai, vi, and Pi on the specimen force versus load-line displace- W 5 0.998193 2 3.88087u 1 0.187106u 1 20.3714u
ment record, calculate as follows: 2 45.2125u 4 1 44.5270u5 (A3.11)
~K~i!!2 ~1 2 v2! where:
J ~i! 5 E 1 J pl~i! (A3.7)
1
where K(i) is from A3.5.1 and: u5 (A3.12)
@~BeECc~i!!1/2 1 1]
J pl~i! 5 (A3.8)
where:
F Jpl~i21! 1 b
~i21! BN S D
h ~i21! Apl~i! 2 Apl~i21!
GF a ~i! 2 a~i21!
1 2 g~i21! b
~i21!
G Cc (i) = specimen crack opening compliance (Dv/DP) on
an unloading/reloading sequence, corrected for
rotation (see A3.5.4),
where:
Be = B − (B − BN) 2/B.
h(i−1) = 2.0 + 0.522 b (i−1)/W, and
g(i−1) = 1.0 + 0.76 b(i−1)/W. A3.5.4 To account for crack opening displacement in DC(T)
In the preceding equation, the quantity Apl(i) − Apl(i−1) is the specimens, the crack size estimation shall be corrected for
increment of plastic area under the force versus load-line rotation. Compliance shall be corrected as follows:
displacement record between lines of constant displacement at Ci
Cc~i! 5 H* (A3.13)
points i−1 and i shown in Fig. A1.3. The quantity Jpl(i)
represents the total crack growth corrected plastic J at Point i F D
GF
R sinui 2 cosu i R sinui 2 cosui G
--`,,,``,`,`,,`````,
D = one half of the initial distance between the displace- with: A0=3.62, A1= 4.21, A=4.33, and A3=2.00. Calculation
ment measurement points, of d requires sYS/sTS$ 0.5.
u = angle of rotation of a rigid body element about the
unbroken midsection line, or A3.5.6.2 Calculation of CTOD for the Resistance Curve
Test Method—For the resistance curve test method, calcula-
u 5 sin 21
F S dm
2 1D
~D2 1 R2!1/2
D G SDD
2 tan21 R , and (A3.14)
tions of CTOD for any point on the force-displacement curve
are made from the following expression:
Ji
d 5 ms (A3.17)
Y
dm = total measured load-line displacement.
where J is defined in A3.5.2.2 with a = ai, the current crack
A3.5.5 Other compliance equations are acceptable if the
resulting accuracy is equal to or greater than those described size and,
and the accuracy has been verified experimentally.
A3.5.6 Calculation of CTOD:
sYS
m 5 A0–A1* s
TS
S D
sYS 2
1 A2* s
TS
sYS
–A3* s
TS
S D S D 3
(A3.18)
A4.1 Assessment of Force/Clip Gage Displacement the significance of small pop-ins (see Fig. A4.1b and Fig.
Records—The applied force-displacement record obtained A4.1d). Referring to Fig. A4.1 and Fig. A4.2, measure the
from a fracture test on a notched specimen will usually be one values of Pc and nc or Pu and nu from the test record at points
of the four types shown in Fig. A4.1. corresponding to: (a) the earliest significant pop-in fracture,
A4.1.1 In the case of a smooth continuous record in which that is, for which F > 0.05 and (b) fracture, when pop-ins prior
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
the applied force rises with increasing displacement up to the to fracture may be ignored, that is, for which F < 0.05 as
onset of unstable brittle crack extension or pop-in, and where follows:
no significant slow stable crack growth has occurred (see 3.2
and Fig. A4.1a and Fig. A4.1b), the critical CTOD, dc shall be 1 n n
S
n 1 Pn 2 y n
F512P · n 1x D (A4.1)
determined from the force and plastic component of clip gage
displacement, np, corresponding to the points Pc and nc. If where:
F = factor representing the accumulated increase in com-
failure occurs close to the linear range, apply the procedure of
pliance and crack size due to all stable crack exten-
Annex A5 to test whether a valid KIc measurement can be
sions, or pop-ins, or both, prior to and including the nth
made.
pop-in, and
A4.1.2 In the event that significant slow stable crack exten-
n = sequential number (see Fig. A4.2) of the last of the
sion precedes either unstable brittle crack extension or pop-in,
particular series of pop-ins being assessed.
or a maximum force plateau occurs, the force-displacement
curves will be of the types shown in Fig. A4.1c, Fig. A4.1d, NOTE A4.2—When only one pop-in occurs, n = 1. When multiple
respectively. These figures illustrate the values of P and n to be pop-ins occur it may be necessary to make successive assessments of F
used in the calculation of du. with n = 1, 2, 3, or more.
A4.1.3 If the pop-in is attributed to an arrested unstable
brittle crack extension in the plane of the fatigue precrack, the n1 = elastic displacement at pop-in No. 1 (see Fig. A4.2),
result must be considered as a characteristic of the material Pn = force at the nth pop-in, and
tested. nn = elastic displacement at the nth pop-in.
NOTE A4.1—Splits and delaminations can result in pop-ins with no NOTE A4.3—nn may be determined graphically or analytically (see Fig.
arrested brittle crack extension in the plane of the fatigue precrack. A4.2).
For this test method, pop-in crack extension in the plane of
the fatigue precrack can be assessed by a specific change in
yn = force drop at the nth pop-in, and
compliance. The following procedure may be used to assess
xn = displacement increase at the nth pop-in sampled the weld or base metal region of interest (26).
NOTE A4.4—Although an individual pop-in may be ignored on the A4.1.4 The initial compliance C1 shall be determined by
basis of these criteria, this does not necessarily mean that the lower bound constructing the tangent OA to the initial portion of the
of fracture toughness has been measured. For instance, in an inhomoge- force-clip gage displacement curve as shown in Fig. A4.3. The
neous material such as a weld, a small pop-in may be recorded because of initial compliance C1 is the inverse of the slope of the tangent
fortuitous positioning of the fatigue precrack tip. Thus, a slightly different
line OA:
fatigue precrack position may give a larger pop-in, which could not be
ignored. In such circumstances the specimens should be sectioned after Dng
C1 5 DP (A4.2)
testing, and examined metallographically to ensure that the crack tips have
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
NOTE 1—Construction lines drawn parallel to the elastic loading slope to give np, the plastic component of total displacement, ng.
NOTE 2—In curves b and d, the behavior after pop-in is a function of machine/specimen compliance, instrument response, etc.
FIG. A4.1 Types of Force versus Clip Gage Displacement Records
dure in Section 8, recording a force versus crack mouth A5.3.1 Construct a secant line as shown on Fig. A5.1 with
opening displacement as shown in Fig. A5.1. Digital data is a slope (P/v)5 = 0.95(P/v)o where (P/v)o is the slope of the
A6.1 This annex describes the method for characterizing value may be obtained labeled Jc.
fracture toughness values based on J, Jc, or Ju, for a fracture
A6.2.1 J is calculated at the final point, instability, using the
instability and the associated requirements for qualifying the
J formulas for the basic method including the crack growth
data according to this test method. Data meeting all of the
correction in Annex A16. This point is labeled JQc, a provi-
qualification requirements of 9.1 and those of this annex result
sional Jc value.
in qualified values of Jc or Ju. Data meeting the size require-
ment result in a value of Jc that is insensitive to the in-plane A6.2.2 Qualification of JQc as Jc—JQc = Jc, a measure of
dimensions of the specimen. fracture toughness at instability without significant stable crack
extension that is independent of in-plane dimensions, provided
A6.2 Fracture Instability Before Stable Tearing—When the following two conditions are both met: (1) B, bo $ 100
fracture occurs before stable tearing a single-point toughness JQ/sY, and (2) crack extension Dap < 0.2 mm + JQ/MsY where
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,
A7.1 This annex describes the method for characterizing A7.3 Fracture Instability After Stable Tearing—When
fracture toughness values based on d, dc, or du for a fracture fracture occurs after stable tearing, crack extension D ap $ 0.2
instability and the associated requirements for qualifying the mm (0.008 in.) + dQc/Md, where Md = 1.4 or an alternative
data according to this test method. Data meeting all of the value determined from the test data, see A11.3, a single-point
qualification requirements of 9.1 and those in this annex result fracture toughness value may be obtained, labeled du. In
in qualified values of dc or du. Data meeting the size require- addition, part of an R curve may be developed or the final point
ment result in a value of dc* that is insensitive to in-plane may be used in the evaluation of an initiation toughness value
dimensions of the specimen. (these are described in Annex A8-Annex A11).
A7.3.1 d is calculated at the final point where instability
A7.2 Fracture Instability Before Stable Tearing—When occurs, using the d formulas for the basic method. This point is
fracture occurs before stable tearing a single-point toughness labeled dQu, a provisional du value.
value may be obtained labeled dc, the force Pc and the clip gage A7.3.2 Qualification of dQu as du—dQu = du, if crack exten-
displacement yc, for dc are indicated in Fig. 1. sion, Dap > 0.2 mm (0.008 in.) + dQu/Md where Md = 1.4 or an
alternative value can be determined from the test data, see
A7.2.1 d is calculated at the final point, instability, using the A11.3.
d formulas from Annex A1-Annex A3. This point is labeled d A7.3.3 Significance of dc and du—Values of dQc that meet
Qc, a provisional dc value.
the qualification requirements are labeled dc* and are consid-
A7.2.2 Qualification of dQc as dc*—A fracture toughness ered to be insensitive to the in-plane dimensions of the
value that is insensitive to the in-plane dimensions of the specimen. Values of dQc that do not meet the size requirement
specimen, if the following two conditions are met: (1) dQc = are labeled dc and may be size-dependent. du is not considered
dc* if B, bo $ 300 dQc, and (2) crack extension Dap < 0.2 mm to be a size-insensitive property and, therefore, is not subject to
(0.008 in.) + dQc/Md where Md = 1.4 or an alternative value a size criterion. It is a characteristic of the material and
determined from the test data, see A11.3. Data that fail to meet specimen geometry and size. It signifies that at the test
the size criterion based on B or bo, but still meet the restriction temperature the material is not completely ductile and can
on crack extension, are labeled dc. sustain only limited R-curve behavior.
NOTE A8.1—Annex A8-Annex A11 cover methods for evaluating A8.2.1 J can be calculated at any point on the force versus
toughness for stable tearing. load-line displacement record using the equations suggested in
the calculation section of Annex A1-Annex A3 for the different
A8.1 This method describes a single-specimen technique
for determining the J-R curve of metallic materials. The J-R specimen geometries.
curve consists of a plot of J versus crack extension in the A8.2.2 If the basic method is used, J values must be crack
region of J controlled growth. The J-R curve is qualified growth corrected using the procedure of Annex A16. In this
provided that the criteria of 9.1 and A8.3 are satisfied. case crack size values are obtained from direct optical mea-
surements from the specimen fracture surfaces using the
A8.2 J Calculation: procedure of 8.5.
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
A9.1 Significance—The property JIc determined by this Annex A8. JIc is qualified provided that the criteria of 9.1 and
method characterizes the toughness of a material near the onset A9.8 and A9.9 are satisfied.
of crack extension from a preexisting fatigue crack. The JIc
value marks the beginning stage of material crack growth A9.2 J Calculation—Calculations of the J integral are
resistance development, the full extent of which is covered in made using the equations in Annex A1-Annex A3.
A9.6.5 Using the method of least squares, determine a linear A9.8 Qualification of Data—The data shall satisfy the
regression line of the following form: requirements of 9.1 and all of the following requirements to be
qualified according to this test method. If the data do not pass
lnJ 5 lnC1 1 C 2 ln S D Da
k (A9.5) these requirements no fracture toughness values can be deter-
mined according to this test method.
where k = 1.0 mm or 0.0394 in. Use only the data which
A9.8.1 The power coefficient C 2 of A9.6.5 shall be less than
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
conform to the requirements stated in the previous sections.
Draw the regression line as illustrated in Fig. A9.1. 1.0.
A9.6.6 The intersection of the regression line of A9.6.5 with A9.8.2 For the Resistance Curve Procedure the following
the 0.2-mm offset line defines JQ and DaQ. To determine this additional requirements must be satisfied:
intersection the following procedure is recommended. A9.8.2.1 If an elastic compliance method is used, aoq shall
A9.6.6.1 As a starting point estimate an interim JQ(1) = JQ(i) not differ from ao by more than the larger of 0.01W or 0.5 mm.
value from the data plot of Fig. A9.1. A9.8.2.2 The number of data available to calculate aoq shall
A9.6.6.2 Evaluate Da(i) from the following: be $8; the number of data between 0.4JQ and JQ shall be $ 3;
and the correlation coefficient of the least squares fit of
JQ~i! A9.3.4.1 shall be greater than 0.96.
Da ~i! 5 Ms 1 0.2 mm ~0.008 in.! (A9.6)
Y A9.8.2.3 If an experimental value of M is determined, at
A9.6.6.3 Evaluate an interim JQ(i+1) from the following least 6 data points are required in the region 0.2JQ #Ji# 0.6JQ.
power law relationship: Only M $ 2.0 can be used in the method.
JQ~i 1 1! 5 C1 S D
Da~i!
k
C2
(A9.7) A9.9 Qualification of JQ as JIc—JQ = JIc , a size-
independent value of fracture toughness, if:
where k = 1.0 mm or 0.0394 in. A9.9.1 Thickness B > 10 JQ / sY,
A9.6.6.4 Increment i and return to A9.6.6.2 and A9.6.6.3 to A9.9.2 Initial ligament, bo > 10 JQ / sY,
get Da(i) and interim JQ(i+1) until the interim JQ values A9.9.3 Regression Line Slope—The slope of the power law
converge to within 62 %. regression line, dJ/da, evaluated at DaQ is less than sY.
A9.6.6.5 Project the intercepts of the power law curve with
the 0.15-mm (0.006-in.) and the 1.5-mm (0.06-in.) exclusion A9.10 Evaluation of KJIc—Calculate KJIc = =(E8JIc) using
lines vertically down to the abscissa. This indicates Damin and E8 = E/(1−n2) and the qualified JIc of A9.9.
A10.1 This annex describes a single-specimen technique and A10.3 are satisfied.
for determining the d-R curve of metallic materials. The d-R
curve consists of a plot of d versus crack extension. To measure A10.2 d Calculation:
the d-R curve the resistance curve procedure of 8.6 must be A10.2.1 The d calculation can be evaluated at any point
used. The d-R curve is qualified provided that the criteria of 9.1 along the force versus load-line displacement record using the
d 5 Md Da (A11.4)
dQ~1! 5 C1 S D
Dap~1!
k
C2
(A11.8)
requirements, no fracture toughness values can be determined
according to this method.
A11.6.6.4 Return to A11.6.6.2 and A11.6.6.3 to get Da(i) and A11.8.1 The power coefficient C2 of A11.6.5 shall be less
dQ(i + 1) until the dQ values converge to within 2 %. than 1.0.
A11.6.6.5 Project the intercepts of the power law curve with A11.8.2 For the Resistance Curve Procedure the following
the 0.15-mm (0.006-in.) and the 1.5-mm (0.06-in.) exclusion additional requirements must be satisfied:
lines vertically down to the abscissa. This indicates Damin and A11.8.2.1 aoq shall not differ from ao by more than the
Dalimit, respectively. Eliminate all data points that do not fall greater of 0.01W or 0.5 mm.
between Damin and Dalimit as shown in Fig. A11.1. Also A11.8.2.2 The number of data available to calculate aoq
eliminate all data points which lie above the limiting d capacity shall be $ 8; the number of data between 0.4dQ and dQ shall
where dlimit = bo / 7.5m. Where, m is defined in Annex A1 be $ 3; and the correlation coefficient of the least squares fit of
through Annex A3 for the different specimen geometries. A11.6.5 shall be greater than 0.96.
A11.6.6.6 At least five data points must remain between A11.8.2.3 If an experimental value of Md is determined, at
Damin and Dalimit and dlimit. Data point spacing must meet the least 6 data points are required in the region 0.2dQ # di #
requirements of A11.6.3. If these data points are different from 0.6dQ. Only Md # 1.4 can be used by this method.
those used in A11.6.6 to evaluate dQ, obtain a new value of dQ
A11.9 Qualification of dQ as dIc:
based only on qualified data.
d Q = dIc, a size-independent value of fracture toughness, if:
A11.7 An alternative construction line slope, Md, can be A11.9.1 The initial ligament, bo $ 10mdQ.
calculated by fitting the least squares linear regression line to Where m is defined in Annex A1 through Annex A3 for the
the initial J-R curve data for data in the region 0.2dQ # di # different specimen geometries.
0.6dQ as evaluated with Md = 1.4. A minimum of 6 data points A11.9.2 The slope of the power law regression line, dd/da,
are required in the evaluation region to allow an experimental evaluated at DaQ must be less than 1.
NOTE A12.1—Annex A12 and Annex A13 cover miscellaneous infor- A12.2 Compliance from Crack Size:
mation.
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
A13.1 This annex describes the determination of plane- conventional (static) KIc properties applies also to the case of
strain fracture toughness (KIc) properties of metallic materials rapid loading. The plane-strain fracture toughness of certain
under conditions where the loading rates exceed those for materials is sensitive to the loading rate and substantial
conventional (static) testing [2.5 ksi·in.1/2/s (2.75 MPa·m1/2/s)]. decreases in toughness may be noted as the loading rate
increases. Generally, such materials also show a pronounced
A13.2 Summary of Requirements—Special requirements dependence of KIc on test temperature. For example, the
are necessary for plane-strain fracture toughness testing at loading rate sensitivity of structural grade steels has required
loading rates exceeding those of conventional (static) plane- the development of a lower bound KIR curve, given in
strain fracture toughness testing. This description of these Appendix G of Division III of the ASME Boiler and Pressure
requirements does not include impact or quasi-impact testing Vessel Code,5 for the fracture-safe design of heavy-wall
(free-falling or swinging masses). Conventional fracture tough- nuclear pressure vessels. Additionally, KIc values for steels
ness test specimens are prepared as described in this method, tested at various temperatures and loading rates are required for
tested under rapid-load conditions, and a fracture toughness correlation with small-scale production control tests (such as
value is calculated. Load-deflection, load-time, and deflection- the Charpy V-notch test) for setting material specifications and
time curves are recorded for each test. The load-deflection fracture-safe design procedures.
curves resulting from these tests are analyzed to ensure that the
initial linear portion of the force-displacement record is suffi- A13.4 Apparatus:
ciently well-defined that PQ can be determined unambiguously. A13.4.1 Loading—Generally, hydraulic machines with
In addition, a test time (t), restricted to not less than one rapid-acting servo controlled valves are used. Depending on
millisecond is determined. This test time and an optionally the compliance of the loading system and the pump capacity,
calculated average stress intensity factor rate, dK/dt, character- an accumulator may be required.
ize the rapid load test. The yield strength of the material must A13.4.2 Fixtures—The fixtures used for static plane-strain
be determined or estimated for the loading time of the fracture fracture toughness tests are generally suitable for rapid-load
test and is used in the analysis of the fracture test data. All of tests. However, consideration should be given to the possibility
the criteria for static KIc determination apply to the rapid-load that the toughness of the fixture material may be reduced by
plane-strain fracture toughness test. The toughness property is rapid loading.
denoted by KIc( ) where the time to reach the force correspond-
ing to KQ in milliseconds is indicated in the parentheses ( ). 5
Available from American Society of Mechanical Engineers (ASME), ASME
International Headquarters, Three Park Ave., New York, NY 10016-5990, http://
A13.3 Significance and Use—The significance of the www.asme.org.
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
to unambiguously determine a value for PQ. The presence of such bursts
transducers may be determined by suitably exciting them and observing of crack extension should be recorded for those tests having analyzable
the wave characteristic on an oscilloscope. If ringing (high-frequency force versus displacement records.
oscillation) is observed within the time period required to reach the PQ
NOTE A13.3—The test data may be directly recorded if the recording
force, the stiffness of the transducers should be increased or their mass
devices have sufficient frequency response. Generally, it is advantageous
reduced. Force cells are quite stiff and should provide no problem at the
to use a storage device that will capture the data and permit playing it out
minimum loading time of 1 ms. The displacement transducer might be
at a sufficiently slow speed that a pen recorder can be used in producing
cause for concern depending on its design. The cantilever beam displace-
the required records. Such storage devices are commonly available in the
ment gage described in Section 6 has been used successfully at loading
form of digital storage oscilloscopes having pen recorder outputs. Sepa-
times slightly lower than 1 ms. The resonant frequency of this gage when
rate storage instruments are also available. In general these digital storage
mounted in a specimen in a conventional manner and excited by tapping
devices have performance characteristics that are more than adequate to
is about 3300 Hz. The free-arm resonant frequency is about 750 Hz. Other
capture, store, and replay the transducer signals from a 1-ms test. For
gages of the same type but having different dimensions should operate
example, calculations show that for a typical fracture test, the crack-mouth
satisfactorily if their free-arm resonance is at least 750 Hz. The following
displacement resolution would be about 0.76 mm/sample (0.030 mil/
equation may be used to estimate the free-arm resonant frequency of such
sample) and the force resolution would be about 712 N/sample (160
a gage:
lbf/sample). It should be possible to obtain at least 1000 simultaneous
f 5 RC F G B2Eg
rl4
(A13.1)
samples of force and displacement during such a test. A digital storage
scope capable of at least this performance would have the following
characteristics: maximum digitizing rate of 1 MHz, maximum sensitivity
of 6100 mV, resolution of 0.025 %, and memory of 4096 words by 12
where: bits. It may be necessary to amplify the output of the clip gage moderately
RC = 51.7, and possibly that of the force cell depending on its capacity in terms of the
f = resonant frequency, Hz, range required. These values of resolution are based on a total noise figure
B = arm thickness, m, of about 50 mV.
E = elastic modulus of the arms, MPa,
g = gravitational acceleration, 9.804 m/s2, A13.6 Calculation and Interpretation of Results:
r = density of the arm material, kg/m3, and A13.6.1 Special requirements are placed on the analysis of
l = length of the uniform thickness section of the arms,
the force versus displacement record. These take into account
m.
the fact that experience (18) has shown force versus displace-
The coefficient RC becomes 0.162 if inch-pound units are ment records from rapid-load fracture toughness tests are not
used where B is in inches, E is in pound-force per square inch, always as smooth in the linear range as those obtained from
g is 386 in./s2, r is pounds per cubic inch, and l is in inches. static tests. The special requirements of this annex are designed
A13.4.4 Signal Conditioners—Amplification or filtering of to ensure that an unambiguous value of PQ can be determined.
the transducer signals may be necessary. Such signal condi- The test time must be determined from the force versus time
tioning units should have a frequency response from dc to at record.
least 20/t (kilohertz) where t is the test time in milliseconds as A13.6.2 The additional analysis of the force versus dis-
defined in A13.6.3. As described in A13.4.3, conventional placement record is illustrated in Fig. A13.1. The procedure is
mechanical recording devices may not have sufficient fre- as follows: Construct the straight line OA best representing the
quency response to permit direct plotting of the force versus initial portion of the test record that ideally should be linear but
time and the displacement versus time signals. may not be smooth. Then construct the line OP5 as described
in Annex A5 and determine PQ. Draw a vertical line at vp
A13.5 Procedure: passing through PQ and define Pv at the point of intersection of
A13.5.1 Loading Rate—The rate of loading is optional with this line with the line OA. Determine 5 % of Pv and construct
the investigator, but the time to reach the force corresponding two lines BC and DE parallel to OA with BC passing through
to KQ shall not be less than 1 ms. Use a preload to eliminate Pv + 0.05 P v and DE passing through PQ (Pv − 0.05 Pv). Draw
ringing in the force or displacement transducers associated a horizontal line at P = 0.5 PQ. For the test to be valid that
with clearances in the load train being suddenly taken up by the recorded force versus displacement curve up to PQ must lie
start of rapid loading. within the envelope described by these parallel lines for the
A13.5.2 For each test conducted, a force versus time, a portion of the record with P # 0.5 PQ.
displacement versus time, and a force versus displacement A13.6.3 The test time t in milliseconds is determined from
record shall be obtained. The time scale of these records shall the record of force versus time as indicated in Fig. A13.2.
be accurately determined since the time is used to characterize Construct the best straight line OA through the most linear
the test. Examine the time-dependent records for the presence portion of the record. The value t is then determined from the
of ringing before reaching the PQ force. Such ringing can result point of intersection of this line with the time axis to the time
from inertial effects as described in Note A13.2. The special corresponding to PQ. This time, t is shown in the parentheses
A14.1 Scope tions where the loading rate exceeds that allowed for conven-
A14.1.1 This annex covers the determination of the rate tional (static) testing, see Section 8.4.2.
dependent JIc(t) and the J-integral versus crack growth resis-
A14.2 Summary of Requirements
tance curve (J-R(t) curve) for metallic materials under condi-
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
FIG. A14.1 Strain Gages Mounted on SE(B) Specimen for Measurement of Transmitted Force
FIG. A14.2 Strain Gages Mounted on C(T) Specimen for Measurement of Transmitted Force
Both initial and final crack sizes are required by the A15. The high rate test must be stopped abruptly to obtain a
normalization method of J-R(t) curve development of Annex limited specimen deformation and a crack extension increment
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
FIG. A14.4 Test Fixtures for Drop Tower C(T) Specimens
of the calibrated range of the reference force cell used. The component in frequency response of the displacement mea-
on-specimen, transmitted force measuring system shall be surement system. Capacitive transducers have been designed to
accurate to within 2 % of the final precracking force over the fit in the notch of the C(T) specimen as shown in Fig. A14.5.
calibration range. Fiber-optic transducers have been used to measure load line
A14.5.5 Displacement Transducers—The transducer shall displacement of SE(B) specimens. If the load line displacement
have response characteristics that allow it to follow the motion is measured relative to the test fixture, care must be taken to
of the specimen while not introducing excessive mechanical account for the effects of fixture compliance and brinnelling on
noise into the measured displacement. the measured displacement, as discussed in 8.3.1.1.
A14.5.5.1 Cantilever beam displacement gages such as A14.5.6 Signal Conditioners—The user is referred to Guide
those used in static fracture toughness testing may be suitable E 1942 for a detailed discussion of requirements for data
for rapid-load testing, see A13.4.3. The cantilever beam dis- acquisitions systems. The signal conditioner must have suffi-
placement gage described in Annex A1 of Test Method E 399 cient bandwidth to capture the transducer signal without
has been used successfully at loading times (tQ) slightly less introducing distortion.
than 1 ms. A14.5.6.1 Signal conditioners shall have a frequency band-
A14.5.5.2 Gap measuring transducers that use either capaci- width in excess of 10/tQ for the force signal and 2/tQ for the
tance or optical means to measure displacement have also been displacement signal(s). The more stringent requirement on the
used successfully in rapid-load testing (20). These transducers force signal is necessary to obtain an accurate measurement of
have the advantage that they can be rigidly attached to the the elastic component of the J integral near crack initiation. No
specimen, and the vibration characteristics of the transducer “phase shifting” of transducer signals is allowed by this
generally do not affect the measured displacement. The disad- method. The bandwidth required to accurately capture a signal
vantages are that the output may be non-linear, and the signal of that frequency will depend on the type of low-pass filter in
conditioners used with these transducers are often the limiting the signal conditioner, and the tolerable error. If a low-pass
FIG. A14.5 High Rate Capacitance COD Gage and C(T) Specimen with Attachment Holes
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
FIG. A14.6 Evaluation of tQ and the Test Rates (dJ/dt)I and (dJ/dt)T
filter is present in the measurement system it should not acquisitions systems. The rate at which an analog signal is
introduce more than 0.5 % measurement error, see Guide sampled to create a digital signal shall be high enough to
E 1942. ensure that the peak value is accurately captured. The rate of
A14.5.7 Data Sampling—The user is referred to Guide data acquisition shall result in the time per data set being less
E 1942 for a detailed discussion of requirements for data than tQ/50.
8.5.4.
A14.6.5 If the specimen is characterized by ductile upper grips or impact absorbers must be added or modified or the test
shelf behavior, the normalization method of Annex A15 can be rate reduced to obtain a smoother data set that can be qualified
used to develop the J-R(t) curve for the test specimen. A according to this method.
multi-specimen method can also be used with J evaluated using A14.7.5 If tQ< tw, the test data are not qualified according to
the basic method relationships corrected for crack extension this method. A slower loading rate must be used, or the
using Annex A16. Using Section 9, calculate JQ (the tentative specimen geometry changed to decrease tw for the test to be
JIc) and the corresponding force PQ and time tQ. If a ductile qualified according to this method.
instability occurs so that the final stable crack size af cannot be A14.7.6 If the normalization method of Annex A15 is used
determined, the normalization method cannot be used to to obtain JIc, the J resistance curve, or both, at least one
develop the J-R(t) curve or the corresponding JQ for this test confirmatory specimen must be tested at the same test rate and
specimen. under the same test conditions. From the normalization method
A14.6.5.1 If a pop-in is present, refer to Annex A4 to assess the load line displacement corresponding to a ductile crack
its significance. If the pop-in is significant, Jc(t) or Ju(t) values extension of 0.5 mm shall be estimated. The additional
corresponding to the point of onset can be calculated using specimen shall then be loaded to this load line displacement
Annex A6. If fracture instability occurs without significant level, marked, broken open and the ductile crack growth
ductile crack extension, Jc(t) or Ju(t) values corresponding to measured. The measured crack extension shall be 0.5 6 0.25
the point of onset can be calculated as defined in Annex A6. If mm in order for these results to be qualified according to this
fracture instability follows significant ductile crack extension, method.
the J-R(t) and JIc(t) can be determined providing that af is
distinguishable. The validity of the J-R(t) curve and JIc(t) are A14.8 Qualifying the High Rate Results
subject to the requirements of Annex A8, Annex A9, and A14.8.1 All qualification requirements of 9.1, Annex A6,
Section 9. Annex A8, Annex A9, and A14.7 must be met to qualify the
J-R(t) curve, JQ(t) as JIc(t), or JQc(t) as Jc(t) according to this
A14.7 Qualification of the Data method. If the normalization method of Annex A15 is used, the
additional requirements of this annex shall also be met.
A14.7.1 Test equipment, specimen geometries, specimen
A14.8.2 The maximum crack extension capacity for a
fixture alignment, and measured data must meet all require-
specimen to qualify the J-R(t) curve is given by the following:
ments of Sections 6, 7, 8, and 9, except as specifically replaced
in A14.5. Additional requirements specified here are necessary Damax 5 0.15bo (A14.2)
for high rate testing.
A14.7.2 All of the test equipment requirements of A14.5 A14.9 Report
shall be met. A14.9.1 The report shall include all the items of Section 10
A14.7.3 Plot the J integral versus the time as shown in Fig. as well as the following:
A14.6. If fracture instability occurs, calculate J based on ao A14.9.1.1 The minimum test time, tw, according to A14.6.2.
using the basic analysis procedure and plot the data up to and A14.9.1.2 The PQ and tQ, corresponding to the calculated
including JQc(t) or JQu(t). Use a linear regression analysis to JQ(t) or JQc(t).
evaluate (dJ/dt)I as shown in the example of Fig. A14.5 using A14.9.1.3 The (dJ/dt)I, (dJ/dt)T values, or both.
the data from 0.5JQ(t) to JQ(t), from 0.5JQc(t) to JQc(t), or from A14.9.1.4 If JIc(t) is being reported, the final crack exten-
0.5 JQu(t) to JQu(t), as the case may be. Extrapolate this line to sion obtained on the confirmatory specimen of A14.7.6 shall be
the abscissa to evaluate the quantity tQ, as shown in Fig. A14.6. reported.
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
A14.10 Precision and Bias tion function method of Annex A15 is used, the crack size and
A14.10.1 Precision—The precision of J versus crack crack extension information must be inferred from initial and
growth is a function of material variability, the precision of the final crack size measurements. The requirement for the addi-
various measurements of linear dimensions of the specimen tional specimen to be tested near to the point of crack initiation
and testing fixtures, precision of the displacement measure- has been added to validate the JIc(t) measurement. A round
ment, precision of the force measurement, as well as the robin used to evaluate the overall test procedures of this
precision of the recording devices used to produce the force method is reported in (21).
displacement record used to calculate J and crack size. For the A14.10.2 Bias—There is no accepted “standard” value for
test rates allowed by this annex, if the procedures outlined in measures of elastic-plastic fracture toughness of any material.
this annex are followed, the force and load-line displacement In absence of such a true value, any statement concerning bias
can be measured with an precision comparable with that of the is not meaningful.
static loading as described in the main body. If the normaliza-
A15.1 Scope are met. The normalization method is not applicable for low
A15.1.1 The normalization technique can be used in some toughness materials tested in large specimen sizes where large
cases to obtain a J-R curve directly from a force displacement amounts of crack extension can occur without measurable
record taken together with initial and final crack size measure- plastic force line displacement.
ments taken from the specimen fracture surface. Additional
restrictions are applied (see A14.1.3) which limit the applica- A15.2 Analysis
bility of this method. The normalization technique is described A15.2.1 The starting point for this analysis is a force versus
more fully in Herrera and Landes (22) and Landes, et al. (23), load point displacement record like that shown in Fig. A15.1.
Lee (24), and Joyce (21). The normalization technique is most Also required are initial and final physical crack sizes optically
valuable for cases where high loading rates are used, or where measured from the fracture surface. This procedure is appli-
high temperatures or aggressive environments are being used. cable only to Test Method E 1820 standard specimen geom-
In these, and other situations, unloading compliance methods etries with 0.45 # ao/W # 0.70 and cannot be used if the final
are impractical. The normalization method can be used for physical crack extension exceeds the lesser of 4 mm or 15 % of
statically loaded specimens if the requirements of this section the initial uncracked ligament.
A15.2.2 Each force value Pi up to, but not including the A15.2.5 The final force displacement pair shall be normal-
maximum force Pmax, is normalized using: ized using the same equations as above except that the final
Pi measured crack size, af, is used. Typical normalized data are
PNi 5 (A15.1) shown in Fig. A15.2.
WB F
W 2 abi
W G
hpl
E a 1 b v8pl 1 c v8pl2
PN 5 (A15.5)
where Ki, hpl, and Jpli are calculated as in Annex A1 and d 1 v8pl
Annex A2 for each specimen type using the crack size ao. where a, b, c, and d are fitting coefficients. This function can
A15.2.3 Each corresponding load line displacement is nor- be fitted to the data of Fig. A15.1 using standard curve fitting
malized to give a normalized plastic displacement: packages available as part of computer spreadsheet programs
vpli ~vi 2 Pi Ci! or separately. An example fit for the data of Fig. A15.2 is
v8pli 5 W 5 W (A15.4)
shown in Fig. A15.3. The normalization function shall fit all
where Ci is the specimen elastic load line compliance based the data pairs described above (including the final pair) with a
on the crack size abi, which can be calculated for each maximum deviation less than 1 % of the PN at the final point.
specimen type using the equations of Annex A1 and Annex A2. Data should be evenly spaced between vpli/W = 0.001 and the
A15.2.4 The final measured crack size shall correspond to a tangency point. If less than ten data pairs are available for this
crack extension of not more than 4 mm or 15 % of the initial fit, including the final measured data pair, this method cannot
uncracked ligament, whichever is less. If this crack extension be used.
is exceeded, this specimen can not be analyzed according to A15.2.8 An iterative procedure is now used to force PNi,
this annex. vpli/W, ai data to lie on Equation A15.5. This involves
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
FIG. A15.2 Normalized Force versus Displacement Curve Showing Points up to Maximum Force and the Final Data Point
FIG. A15.3 The Normalization Function Shown Fitted to the Normalization Data
FIG. A15.4 Data is Adjusted, Defining the Crack Size Necessary to Place All Points on the Analytical Normalization Function
(Only a portion of the data is shown for clarity)
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
A15.4.2 If the normalization function is used the coeffi- presented in (21). A requirement for the testing of a confirma-
cients of the fit shall be reported as well as the maximum tory specimen tested near the point of stable crack initiation is
deviation of the fit and the number of data used. present to validate the JIc measurement.
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
A15.4.3 If JIc is reported, the accuracy of the confirmatory A15.5.2 Bias—Crack sizes generally vary through the
specimen of A15.3.2 shall be reported. thickness of fracture toughness specimens. A nine point aver-
A15.5 Precision and Bias age procedure based on optical measurements obtained from
the post-test fracture surface is generally used to give a
A15.5.1 Precision—The precision of the J resistance curve
reportable crack size. Different measurements would be ob-
is a function of material variability, the precision of the various
measurements of linear dimensions of the specimen and testing tained using more or less measurement points. Alternative
fixtures, precision of the displacement measurement, precision crack sizes can be estimated using compliance methods, which
of the force measurement, as well as the precision of the obtain different average crack size estimates for irregular crack
recording devices used to produce the force displacement front shapes. Stringent crack front straightness requirements
record used to calculate J and crack size. For the test rates are present in this standard to minimize differences caused by
allowed by this annex, if the procedures outlined in this annex these effects. The normalization method acts to interpolate
are followed, the crack size throughout the fracture toughness between optically measured crack average lengths measured at
test can be measured with a precision comparable with that of the start and end of the stable resistance curve fracture
the unloading compliance procedure described in the main toughness test. This method has been demonstrated in (21) to
body. A round robin describing the use of the normalization give results consistent with those obtained by unloading
procedure on rapidly loaded SE(B) and C(T) specimens is compliance procedures.
the specimen type. with a = 1 for SE(B) specimens and a = 0.9 for C(T) and
A16.1.2 Obtain initial crack growth correct J values using DC(T) specimens.
the following relationship (27):
APPENDIX
(Nonmandatory Information)
X1. EXAMPLE
X1.1 To fit Eq A9.1 to the Ji, ai data using the method of X1.2 This equation can be set up and solved using a
least squares, the following equation must be set up and solved standard spreadsheet or using a mathematical analysis program
for aoq, B, and C: like MathCad, Maple, or Mathematica.
REFERENCES
(1) Joyce, J. A., and Tregoning, R. L., “Development of Consistent Size Journal of Testing and Evaluation, Vol 8, No. 5, September 1980.
Criteria for ASTM Combined Fracture Mechanics Standards,” Fatigue (10) Gudas, J. P., and Davis, D. A., “Evaluation of the Tentative JI-R
and Fracture Mechanics, Vol 30, ASTM STP 1360, P. C. Paris, et al, Curve Testing Procedure by Round Robin Tests of HY-130 Steel,”
eds., ASTM, West Conshohocken, PA, 1999. Journal of Testing and Evaluation, Vol 10, No. 6, November 1982,
(2) Joyce, J. A., “Manual on Elastic-Plastic Fracture: Laboratory Test pp. 252–262.
Procedures,” ASTM Manual Series MNL 27, 1996. (11) Zhu, X. K., Leis, B.N., and Joyce, J.A., “Experimental Estimation of
(3) Dawes, M. G.,“ Elastic-Plastic Fracture Toughness Based on the COD J-R Curves for Load-CMOD Records for SE(B) Specimens,” Journal
and J-Integral Concepts,” Elastic-Plastic Fracture, ASTM STP 668, J. of ASTM International, Vol. 5 No. 5 March 2008, http://
D. Landes, J. A. Begley, and G. A. Clarke, eds., ASTM, 1979, pp. www.astm.org/DIGITAL_LIBRARY/JOURNALS/JAI/PAGES/
307–333. 1135.htm
(4) Willoughby, A. A., and Garwood, S. J., “On the Loading Compliance (12) Srawley, J. E., “Wide Range Stress Intensity Factor Expressions for
Method of Deriving Single Specimen RCurves in Three Point Bend- ASTM E 399 Standard Fracture Toughness Specimens,” Interna-
ing,” Elastic-Plastic Fracture: Second Symposium, Volume II— tional Journal of Fracture, Vol 12, June 1976, pp. 475–476.
Fracture Resistance Curves and Engineering Applications, ASTM STP
(13) Newman, J. C., Jr., “Stress Analysis of the Compact Specimen
803, C. F. Shih and J. P. Gudas, eds., ASTM, 1983, pp. II-372–II-397.
Including the Effects of Pin Loading,” ASTM STP 560, 1974, pp.
(5) Hackett, E. M., and Joyce, J. A., “Dynamic J-R Curve Testing of a
105–121.
High Strength Steel Using Key Curve and Multi-Specimen Tech-
(14) Newman, J. C., Jr., “Stress Intensity Factors and Crack Opening
niques,” Fracture Mechanics, Seventeenth Volume, ASTM STP 905,
Displacements for Round Compact Specimens,” International Jour-
ASTM, 1986, pp. 741–774.
nal of Fracture, 17(6), December 1981, pp. 567–578.
(6) Hellman, D., Rohwerder, G., and Schwalbe, K. H.,“ Development of
a Test Setup for Measuring Deflections of Single Edge Notched Bend (15) Underwood, J. H., Kapp, J. A., and Baratta, F. I., “More on
(SENB) Specimens,” Journal of Testing and Evaluation, Vol 12, No. 1, Compliance of the Three-Point Bend Specimen,” International Jour-
January 1984, pp. 62–64. nal of Fracture, Vol 28, 1985, pp. R41–R45.
(7) KarisAllen, K. J. and Mathews, J. R., “The Determination of Single (16) Saxena, A., and Hudak, S. J., “Review and Extension of Compliance
Edge-Notched Bend Specimen Load-Line Displacement from Re- Information for Common Crack Growth Specimens,” International
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---
motely Located Sensors in Elastic-Plastic Fracture Testing,” Journal of Journal of Fracture, Vol 14, October 1978, pp. 453–468.
Testing and Evaluation, JTEVA, Vol 22, No. 6, Nov. 1994, pp. (17) Yoon, K. K., Gross, L. B., Wade, C. S., and VanDerSluys, W. A.,
581-583. “Evaluation of Disk-Shaped Specimen for Determining J-R Curves,”
(8) McCabe, D. E., “Evaluation of the Compact Specimen for Plane Strain Fracture Mechanics: 26th Volume, ASTM STP 1256, W. G. Reuter, J.
Fracture Toughness of High Strength Materials,” Journal of Materials, H. Underwood, and J. C. Newman, eds., American Society for
Vol 7, No. 4, December 1972, p. 449. Testing and Materials, Philadelphia, 1995.
(9) Begley, J. A., Clarke, G. A., and Landes, J. D., “Results of an ASTM (18) Shoemaker, A. K., and Seeley, R. R., “Summary Report of Round
Cooperative Test Program on the JIc Determination of HY-130 Steel,” Robin Testing By ASTM Task Group E24.01.06 on Rapid Loading
ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentioned
in this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk
of infringement of such rights, are entirely their own responsibility.
This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and
if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of the
responsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you should
make your views known to the ASTM Committee on Standards, at the address shown below.
This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,
United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the above
address or at 610-832-9585 (phone), 610-832-9555 (fax), or service@astm.org (e-mail); or through the ASTM website
(www.astm.org).
--`,,,``,`,`,,`````,,,,,,,,``,-`-`,,`,,`,`,,`---