Process Equipment and Plant Design
Process Equipment and Plant Design
Process Equipment and Plant Design
Fresh water carrying pipelines in chemical industries are coloured with __________
1
color.
2 Which of the following material is seldom used for pressure vessel construction ?
3 The ratio of shear stress to shear strain is called
4 25 per cent cut segmental baffle means that the baffle
Liquid/petroleum fuel storage tanks are built underground (as in case of petrol pumps),
5
when the storage capacity is less than __________ kilolitres.
6 (1) for fully open globe value may be around
7 Lug support is
Pick out the wrong statement pertaining to the use of valve tray, seive tray and bubble
8
cap trays in continuous distillation column.
Holes of a sieve tray are arranged in triangular pitch of __________ times the hole
10
diameter.
In case of a shell and tube heat exchanger, the minimum shell thickness for carbon steel
11 (inclusive of corrosion allowance) depends on shell diameter and is in the range of
__________ mm.
12 The stress developed in a material without any permanent set is called the
13 In a shell and tube heat exchanger, the 'tube pitch' is defined as the
Which of the following is not a valid assumption in continuous binary distillation for
14
calculating the number of equilibrium stages by Mc-Cabe-Thiele's method ?
Overall distillation column efficiency for most of the refinery columns can be given by
15 (for μ = 0.07 - 1.4 cp and relative volatility < 4) (where η = overall column efficiency, % μ
= molal average viscosity of feed at average column temperature and pressure, cp Δp =
pressure drop per tray, psi)
16 The value of fouling factor depends upon the
In case of bubble cap distillation column of diameter greater than 1.2 metres, the cap
17
diameter is roughly about __________ cms.
Tube side pressure drop in a 1-2 heat exchanger (for turbulent flow of fluids through the
18 tubes) is about __________ times, that in a 1-1 heat exchanger having the same size &
number of tubes and operated at the same liquid flow rate.
To keep the power input constant for a stirred vessel operating under fully developed
19 turbulent flow conditions (constant power number), if the impeller diameter is
increased by 20%, the impeller speed should be decreased by a factor of
20 In a heat exchanger, shell side fluid velocity can be changed by changing the tube
Where does the maximum tensile strength occur in a thick cylindrical vessel subjected
21
to internal pressure ?
22 It is not desirable to design a heat exchanger for LMTD correction factor, FT, of less than
23 A rivetted joint does not fail by __________ of rivets.
Triangular pitch tube layout as compared to square pitch in a shell and tube heat
24
exchanger
25 Bracket supports are the most suitable for supporting __________ vessels.
In a multipass shell and tube heat exchanger, the shell side cross flow area does not
26
depend upon
Two iron pipes of the same nominal diameter but different schedule numbers will have
27
the same
Steam side heat transfer co-efficient for design consideration under ordinary condition
28
can be assumed to be about __________ kcal/hr.m^2.°C.
Lessing ring is formed by the addition of a partition across the centre of a raschig ring,
30
which results in an area increase of about __________ percent.
In chemical process equipments, the conical bottom heads used, usually has an apex
31
angle of
Smaller sized packings are generally dumped to the packed columns, and the large ones
32 of size greater than __________ mm are stacked individually, which provides better
control over bed porosity and offers lower gas pressure drop.
Shell side heat transfer co-efficient in case of square pitch as compared to the triangular
33
pitch under similar condition of fluid flow and tube size is
Correct use of 'factor of safety' is very important in equipment design. It is defined as
34
the ratio of the
The operating velocity in the absorption tower is usually 40-50% of the flooding
35 velocity. Packed absorption towers are normally designed for a pressure drop of about
__________ mm of water column per metre height of packing.
__________ tray arrangement is recommended for distillation column having diameter
36
upto 4 ft.
37 What is the value of 'q' for saturated liquid feed to a distillation column ?
38 In perforated plate towers, the
The ends of a cylinderical vessel can be closed by a head, which can be one of the four
41 shapes. For the same thickness, choose the one which can withstand the highest
pressure.
For laminar flow (NRe < 2100) in steel pipe, the optimum inside pipe diameter is given
42
by
45 Pick out the wrong statement pertaining to the design of a basket type evaporator.
Pick out the wrong statement pertaining to the design of the bubble cap tray of a
46
distillation column to give stable operation and even vapour distribution.
47 Speed of the drum of the rotary vacuum filter normally ranges from __________ rpm.
Pressure drop (Δp) and the superficial gas mass velocity (G) in case of packed absorption
49
tower operating in the preloading range are related as
10 25
the most suitable for thick vertical vessel. same as bracket support.
Bubble cap trays though most expensive are Murphree efficiency of all the three trays are
the best in situations, where low vapour rates nearly equal, however the peak efficiency is
is to be handled and a positive liquid seal is generally higher for seive and valve trays than
essential at all flow rates. the bubble cap.
increases decreases
1.5 to 2 2.5 to 5
3-5 5-11
η = 17 - 61.1 log μ
10 20
2 1/2
(1.2)^3/2 (1.2)^3/5
layout pitch
At the inner surface. At the mid thickness of the cylindrical wall.
0.99 0.95
tearing shearing
permits the use of less tubes in a given shell facilitates comparatively easier external
diameter. cleaning because of large clearance.
thick walled vertical horizontal
baffle spacing clearance
1250 2500
5 20
20° 40°
25 50
more same
1-5 20-40
more less
0.1 to 2 5 to 7
Δp = G Δp = G0.5
75 300
Maintenance cost for valve and seive trays are Valve trays have the highest turn down ratio
comparatively more than bubble cap tray due (i.e. the ratio of the highest to the lowest
to their relatively complicated construction vapour flow rates) and thus provides the
features. maximum flexible operating range.
5 to 10 10 to 15
8-15 12-18
30 35
4 8
(1.2)^2/3 (1.2)^5/3
0.80 0.55
tearing of the plate across a row none of these
permits the use of more tubes in a given shell
both (b) and (c).
diameter.
thin shperical (e.g. Horton sphere) none of these
pitch none of these
7500 15000
35 55
60° 80°
75 150
less twice
100-150 1000-1500
facilitate handling of large flow rate of liquid. improve the flow condition.
500-1500 1500-2500
Torispherical Ellipsoidal
Di, opt = 7.6 Q^0.36 . Ρ^0.9 Di, opt = 3 Q^0.36 . ρ^1.86 μ^0.08
3 to 8 8 to 15
Δp = G2
Height equivalent to a theoretical plate (HETP) is the height of packing that will give the
same separation as one theoretical plate in gas-liquid mass transfer operations like
2
distillation, absorption/stripping and humidification/dehumidification. HETP which is
experimentally determined, depends upon the
With increase in gas flow rate to fabric surface area ratio (Nm3/hr/m2 fabric surface
4
area), the size & the cost of a bag filter
A head comprises of straight flange section, corner torus, section and central dished
5
section. Crown radius and knuckle radius in a head is related respectively to the
7 Which of the following is used to set the diameter of the distillation column ?
Ponchon Savarit method is based on the use of enthalpy concentration diagram, which
contains the bubble point curve (saturated liquid curve), dew point curve (saturated
8
vapour curve) and equilibrium tie lines. As compared to McCabe-Thiele's method, this
method
The optimum size ratio for two mixed reactors in series depends on the kinetics of the
9
reaction and the conversion level. For reaction orders more than one, the
10 In a shell and tube heat exchanger, tube side __________ of the mass velocity.
Which of the following is not a graphical method (but is an analytical method) for the
11
calculation of theoretical number of stages in case of continuous binary distillation?
In packed towers provided with saddle packing, liquid redistributors are positioned at
14
every __________ times column diameter or 6 metres whichever is less.
The slope of the feed line in distillation opeartion is given by (where, q = fraction of the
20
feed stream that is liquid.)
21 Speed of industrial paddle agitator ranges from __________ rpm.
22 __________ strain is measured using a 'strain rosetter'.
23 Thin spherical shells subjected to internal pressure, develop __________ stresses.
With increase in the reflux ratio for a fixed production from a continuous binary
24
distillation column, the __________ decreases.
The slope of operating line in the rectifying section of a distillation column is unity, if the
25
reflux ratio is
26 Vertical vessels are not supported by
With increase in pressure drop (for a given particle size), the dust collection efficiency of
27
a cyclone separator will
28 Spherical shaped pressure vessel is considered to be the most ideal, because it can
An adequate clearance between the tray and the shell wall of a distillation column is
29
provided to
31 Pick out the wrong statement about the design of a sieve plate column.
34 In a __________ rivetted joint, the rivets in the various rows are opposite to each other.
The circumferential (hoop) stress in a thin walled cylinderical vessel under internal
38
pressure is
39 (1) for fully open gate valves would be
42 The most common standard size of bubble caps used in industrial operation is
Compensation against openings in process vessels for giving inlet and outlet
43 connections, for providing sight glasses and manholes etc. is provided for strength and
rigidity. The most efficient type of compensation is of __________ type.
44 In case of a continuous distillation column, increase in reflux ratio may result in the
In a distillation column, the minimum residence time for liquid in the downspout is
45
about __________ seconds.
46 Thickness of the frame of a plate and frame filter as compared to that of plates is
Which of the following factors affect the pressure drop in a co-current gas-liquid
47
absorption packed tower ?
The thickness of heat transfer plates used in the plate type heat exchanger ranges from
48
__________ mm, pressed in a single piece provided with grooves & corrugations.
Safety valves are provided in heat exchangers Liquid metals and dowtherm are used for very
for removal of non-conden-sables. high temperature heating.
increases decreases
central dished section and corner torus corner torus section and central dished
section. section.
is more accurate in finding the number of accounts for the enthalpy changes in the
equilibrium stages. process.
equal sized reactors are the best. smaller reactor should come first.
5 to 10 15 to 30
2-3 5-8
-q -q/(1-q)
1 to 5 20 to 100
Volumetric Shear
radial circumferential
fixed charges initially running cost of cooling water for condenser
0 ∞
brackets skirts
increase decrease
10 20
zig-zag chain
The tensile strength of a brittle material is less The compressive strength of a ductile
than its compressive strength. materia] is less than its tensile strength.
are manufactured on 2:1 ratio of major to resist half the pressure rating compared to
minor axis and is recommended to be used hemi spherical head provided on the
for pressure vessels operating above a cylindrical shell of the same thickness and
pressure of 1.5 MN/m^2 . diameter.
Plate tower is perferred, if interstage cooling Plate tower is preferred over packed tower, if
is required to remove heats of reaction or the operation involves liquids containing
solution. dispersed solids.
pd/2t pd/4t
much more than that for fully open globe much less (say 2% than that for fully open
valves. globe valves).
double pipe heat exchanger. multipass shell and tube heat exchanger.
1" dia cap with 0.5" dia riser. 6" dia cap with 4" dia riser.
lower fixed charges for the column. greater cost for the reboiler heat supply.
1 8
less same
Size, shape, orientation and surface of the
Density and viscosity of fluids.
packing particles.
In a shell and tube heat exchanger, high A loop seal or U-seal is provided in a vertical
pressure fluid is generally routed through the condenser sub-cooler to prevent quick
tube. draining of the condensate.
central dished section and straight flange straight flange section and corner torus
section. section.
40 to 50 55 to 75
10-15 20-25
1 minimum
columns saddles
increase or decrease depending on the nature
remain unaffected
of the dust.
be designed without wind load
be supported very easily.
considerations.
30 5
In a thick cylindrical shell, the hoop stress is The value of crushing load is more than that
maximum at the inner radius. of buckling load for long colmns.
pd/t pd/3t
8" dia cap with 1" dia riser. 4" dia cap with 8" dia riser.
greater cost for the condenser coolant. all (a), (b) and (c).
80 180
more either (a) or (b)
Fluid flow rates. All (a), (b) and (c).
Tube wall thickness depends on the cor-rosiveness of the fluids and their operating
pressure & temperature and is specified by Birmingham wire gauge (B.W.G)-a number
1 which varies from 8 to 18 with the numbers 14 and 16 being more commonly used.
Outside diameter of tubes varies from about 15 to 50 mm; however a tube of less than
__________ mm outside diameter is generally not recommended for fouling fluids.
Angled baffles are preferred in the agitation tank to control the swirling action; if the
2 viscosity of the liquid to be mixed is about 200 poise. However, the baffle may be
completely eliminated for mixing liquids having viscoisty above __________ poise.
3 Ratio of tube length to shell diameter for a shell and tube heat exchanger is
In a shell and tube heat exchanger, the overall heat transfer co-efficient is proportional
5 to the tube side (volumetric flow rate)^0.8. This is valid, only when the ratio of the tube
side film resistance to the total resistance is almost equal to
6 Which of the following types of reactors is the safest from operation point of view ?
For a cylindrical shell, (subject to the thickness of uppermost course being more than
10
the minimum for diaofthe tank in question), the thickness of the courses of shell
The design stress, which is more than the damaging stress, is the least unit stress that
will render a member unfit for service before the end of its normal life. The design
12
stress factor or factor of safety indicates the margin between design stress and the
__________ stress.
13 Hole diameter of the seive trays in the distillation column ranges from __________ mm.
For annular flow of a fluid, the ratio of the equivalent diameter for pressure drop
15
calculation to the equivalent diameter for heat transfer calculation is
In actual operation of distillation column, the vapour is not distributed uniformly among
16
the bubble caps, primarily because of the
The minimum shell thickness for tank ≤ 15 metres diameter is limited to __________
17
mm, for reasons of elastic stability.
If 'D' is the inside diameter of the shell of a shell and tube heat exchanger, then the
18
baffle spacing is usually in the range of
19 Brass valves are usually made for pipe sizes __________ inches.
At the following point for a given packing and set of fluids, the pressure drop per metre
20
of packed height, with variation in fluid rates and operating pressure
In a shell and tube heat exchanger, triangular pitch arrangement as compared to square
21
pitch arrangement
22 Pick out the wrong statement about routing of fluids in a shell and tube heat exchanger.
23 The necessary wall thickness for a metallic storage vessel is a function of the
In a multiple effect evaporator system having 'n' effects, the amount of water
24 evaporated per unit surface area in approximately equal to __________ times that in a
single effect.
26 Pick out the wrong statement pertaining to the design of a horizontal tube evaporator.
29 __________ shapedroof is the most commonly used roof for cylinderical storage tanks.
Pick out the wrong statement pertaining to 'Horton sphere' used for the storage of
30
liquid ammonia.
A perforated plate has holes of diameter dn arranged in a pitch ph. Each hole has a tube
38
of I.D. dt passing through it. The ligament efficiency is given by
__________ is the determining factor for the number of bubble caps to be used per
39
tray.
Low pressure steam (with saturation temperature between 105 to 120°C) is usually
41 used in the vacuum evaporators, which normally employ a vacuum of about
__________ mm Hg (referred to a 760 mm mercury barometer).
Which of the following is the best tube material from thermal conductivity point of view
42
alone?
43 Normal screwed fittings are used for pipes upto a diameter of __________ inches.
44 In a shell and tube heat exchanger, the clearance of the tube is generally
45 Diameter of the seive tray column is determined by the
46 For a given fluid, as the pipe diameter increases, the pumping cost
47 Maximum acceptable total liquid gradient over a tray is about __________ mm.
48 In case of a 'thin' pressure vessel, the ratio of its diameter to wall thickness is
High pressure fluid in a shell and tube heat exchanger should preferably be routed
49
through the
50 Bubble cap tray is the most commonly used tray in large distillation column, because
16 19
300 600
∞ 1
density of the gas, but is independent of the density of the gas and inversely as viscosity of
viscosity of the gas. the gas.
1-1 cocurrent double pipe
expansion joint. changes in its direction.
0.1 0.8
working damaging
lto3 4 to 8
5-10 15-20
liquid gradient on the tray. lower skirt clearance.
2 5
The corrosive and fouling fluid should be The viscous fluid should be routed through
preferably routed through the tubes. the shell side.
ultimate tensile strength (or yield point) of operating pressure and welding/joint
the material and operating temperature. efficiency.
'n'th (1/n)th
In a flanged and standard dished head, the In a flanged and shallow dished head, the
crown radius is ≤ shell outside diameter. crown radius is > shell outside diameter.
It is unsuitable for concentrating those liquids, It is suitable for process, in which the final
which form a scale or deposit salt. product is a liquor instead of solid.
Conical Flat
1.3 to 2 1.6 to 2
250 450
decreases. increases.
5.5 12.5
< 10 > 10
tubes to avoid the expansion of high pressure
shell side for smaller total pressure drop.
shell construction.
of its flexibility and nearly constant efficiency it incurs less pressure drop as compared to
under varying conditions of operation. any other try designed for the same duty.
28 38
1000 1500
20.8 2
0.25 0.5
30-35 35-40
lower static submergence. small downcomer liquid seal.
10 15
Dome Umbrella
Horton sphere is used for the storage of gases Horton sphere is used for the storage of liquid
and volatile liquid at a moderate pressure of 1 at sub-zero temperature at very high pressure
to 10 kg/cm^2 . upto 200 kg/cm^2 .
2.5 1.5 to 3
skirt clearance for bubble caps. all (a), (b) and (c).
650 750
A pressure vessel is said to be made of 'thick' shell, if the ratio of its diameter to wall
6
thickness is
Tube side heat transfer co-efficient for turbulent flow of liquid through tubes is
8
proportional to
Circumferential (hoop) stress in a thin cylindrical vessel under internal pressure is
9
_________ the longitudinal stress.
10 The dust collection efficiency of electrostatic precipitator increases with increase in the
For storing hazardous chemicals in large storage tanks, the minimum safe distance
11
between the two tanks should range between __________ times the tank diameter
In a cylinderical vessel subjected to internal pressure, the longitudinal stress σL and the
17
circumferential stress, σn are related by
18 Nominal size of a pipe is an indication of its __________ diameter.
19 Excessive liquid gradient on a tray may result in the
The ratio of tube length to shell diameter in case of liquid shell and tube heat exchanger
20
ranges from
In a double pipe concentric heat exchanger, the equivalent diameter of annulus for heat
21
transfer would be (where, D1 and D2 are I.D. of inner and outer pipes)
22 What is the slope of the operating line in the stripping section of a distillation column ?
23 __________ shaped roof is most commonly used for cylindrical tanks.
24 In a thin cylindrical shell, the hoop stress is __________ stress.
Commercial packed scrubbers are normally designed for a pressure drop range of
25
__________ mm water coloumn per metre of packed height.
26 The retention time of material in a rotary dryer depends upon its
In actual operation of a bubble cap distillation tower, the __________ at the bottom of
27
the tower is more than that at the top of the tower.
Rotary driers are most economically designed for the number of heat transfer units
28
(HTU) from
The difficulty of liquid distribution in packed towers is accentuated, when the ratio of
29
tower diameter to packing diameter is
A forced circulation long tube vertical evaporator as compared to the natural circulation
30
evaporator
39 In the design of a shell and tube heat exchanger, the corrosion allowance
42 Minimum baffle spacing recommended in a shell and tube heat exchanger is equal to
43 __________ liquor is best handled in a long tube vertical evaporator.
Theoretically calculated diameter of the stripping section of the continuous rectification
44
column is __________ that of the enriching section.
45 Hold up of material in a operating rotary drier is in the range of
A binary liquid azeotropic mixture has boiling point higher than either of the
46
components, when it shows __________ deviation from Raoult's Law.
The testing pressure of storage tanks and pressure vessels designed as per Indian
47
standard codes should be about __________ times.the design pressure.
48 Flanges are connected to pipes by
The ratio of down take area to cross-sectional area of the tube, for calendria type
49
evaporator ranges from
hG = 1.004G^0.37 1.004G^0.8
D^2 D^5
30° 45°
5 and 10 45 and 75
10 10
G^0.2 G^0.5
half equal to
S1/S2 S1 * S2
hold baffle in space. fix the tubes in position.
minimum tube sheet thickness (in which
tubes are fixed) is equal to the O.D. of the
minimum cleaning lane of 6.5 mm is provided,
tube upto 15 mm tube diameter; and for > 15
when tubes are on a square pitch.
mm tube diameter, tube sheet thickness is
smaller than tube diameter.
σh = 2 σL σh = σL
inner outer
maldistribution of gas. back trapping.
2 to 3 3 to 5
D2 - D1
0 ∞
Cone Dome
radial circumferential tensile
4-8 17-34
rpm slope & length
molal flow rate of vapour vapour molecular weight
< 30 <7
It is preferred to use a vertical condenser for Draining of residual liquid on tray during shut
condensation of vapor from a distillation down of distillation column is facilitated by
column without sub-cooling weep holes.
permit release of entrained vapour in the
reduce the discharge fluctuation.
liquid.
strain stress
for carbon steel and cast iron pressure parts is
need not be provided for non-pressure parts
1.5 mm (except for tubes) and for severe
like tie rods, spacers, baffles, supports etc.
conditions it is 3 mm.
hydrostatic head is required for refluxing the only the function of condensation is to be
condensate. carried out.
1.5 to 2 3 to 4
screwing welding
0.5 to 1 1 to 1.5
hG = 0.0176G^0.37 0.0176G^1.37
D D^9
60° 75°
20 20
G^0.8 G^1.5
4 to 5 6 to 8
S2 / S1 1/S1*S2
account for thermal strain. none of these.
O.D. of the tube is 6 to 40 mm while the tube
lengths used are 0.5, 2.5, 3.0, 4.0, 5.0, 6 all (a), (b) & (c).
metres.
none of these
>1 <1
Umbrella Flat
compressive longitudinal
52-68 88-105
flights arrangement all (a), (b) and (c)
pressure and temperature all (a), (b) and (c)
5 to 10 10 to 20
decrease in gas solubility for absorbers. all (a), (b) and (c).
4 to 5 >5
brazing all (a), (b) and (c)
1.5 to 2 2 to 2.5
In a multipass shell and tube heat exchanger, the problem of differential expansion
8
between the shell and tube passes is taken care of by using a
In a shell and tube heat exchanger, the shortest centre to centre distance between the
9
adjacent tubes is
Any shell opening greater than 5 cms for a storage tank must be reinforced for reason
10
of
Minimum tube pitch recommended for shell and tube heat exchangers is about
11
__________ times the outside diameter of the tube.
Liquid redistribution should be done in a packed tower packed with raschig rings every
12
6 metres or __________ times the column diameter, whichever is lower.
In case of saddle packing (e.g., berl and intralox saddles), the maximum size of the
14
packing should not exceed __________ of the column diameter.
16 The thermal stress in a metallic bar does not depend upon the
17 The minimum baffle height should be
For turbulent flow (NRe > 2100) of low viscosity fluid (μ > 20cp) in steel pipes, the
optimum inside pipe diameter is given by(where, Q = fluid flow rate, ft^3/sec.ρ = fluid
18
density, lb/ft^3 μ = fluid viscosity, centipoise Di = optimum inside pipe diameter,
inches)
To avoid the tearing off the plate of an edge, the margin (i.e., the minimum distance
19
from the centre of the rivet hole to the nearest edge of the plate) should be equal to
In a __________ rivetted joint, the number of rivets decreases from the innermost row
23
to the outermost row.
Large process vessels operating under extreme temperature and pressure conditions
are normally clad/ lined with materials like stainless steel, aluminium, nickel & its alloys,
24
copper & its alloys and titanium. The cladding thickness is generally about __________
percent of the total thickness.
Heat transfer co-efficient for a horizontal condenser as compared to a vertical
25
condenser operating under similar conditions is
26 Pick out the wrong statement pertaining to the design of the distillation column.
The longitudinal stress induced in a thin walled cylinderical vessel under internal
27
pressure is
28 In distillation columns, bubble caps are held in place over trays by
29 The buckling tendency of compression members is always in the direction of the
In case of plain carbon steel, butt welded joints are used for shell plate thickness ≤
30
__________ cms.
The average velocity in the tubes of a 1-4 heat exchanger is __________ times that in 1-
31 1 heat exchanger having the same size & number of tubes and operated at same liquid
flow rate.
Hoop (circumferential) stress induced in a thin walled 'Horton Sphere' used for the
32
storage of liquid ammonia under pressure is
33 When one of the fluids is highly corrosive and has fouling tendency, it should
The clearance between two tubes in a shell and tube heat exchanger is known as
38 'ligament', whose minimum value is __________ the outside diameter of the tube, but
in no case it should be less than 4.5 mm.
The ratio for the rate of washing to the final rate of filtration in a washing type of plate
39
and frame filter is
Normally, the length to diameter ratio of rotary dryers varies form 4 to 10 and for its
40
economic operation, the number of transfer units (NTU) for such dryers varies from
Typical static submergence for bubble cap plate column operating at atmospheric
45
pressure may be around
In the allocated cap area, bubble caps are generally arranged on equilateral triangular
46
pitch. Number of caps fixed on a plate is with a
The length of straight rectangular weir used on cross-flow trays is generally __________
47
the column diameter.
48 (1) for couplings and unions would be
What is the slope of the operating line in the rectifying section of a distillation
49
coloumn ?
50 Stage efficiency for packed tower varies with the
Sieve plate Packed
higher lower
preventing the local overstressing of the shell reduction of discontinuity in shape at the
around the opening. junction.
1.25 1.75
2.5-3.0 5-7.5
0 to 0.08 0 to 0.8
l/5th l/15th
from rolled strips formed into cylinders and by extrusion & casting into static and
seam-welded. centrifugal molds.
0.5 d d
0.1-0.5 1-2
Segmental baffle Flat plate extending across the wall
chain diamond
1 to 5 10 to 20
same less
pd/2t pd/4t
rivets a hold down bar
least radius of gyration. axis of the load.
1.2 0.5
2 1/2
0.15-030 0.5-0.65
elbow union
split cross
ratio of true temperature difference to the ratio of LMTD to the true temperature
LMTD. difference.
equal to half
0.25 0.50
1.5-2.5 3.5-5.5
0.01 0.3
ferrule socket
2.5" 0.5"
clearance of 25-75 mm. cap pitch of 1.3-2 times the cap diameter.
0 ∞
type & size of packing. fluid rates and fluid properties.
Bubble cap plate None of these
same unpredictable
2.5 3.5
10-12.5 15-20
0 to 1.5 0 to 2.2
l/30th l/50th
1.5 d 2.5 d
10-50 15-30
Disk type baffle Helical type baffle
30 to 40 40 to 50
pd/t pd/8t
bolts both (b) and (c)
perpendicular to the axis of the load. none of these.
3.8 6.8
4 1/4
0.75-0.85 0.60-0.90
7.5-10.0 10-15
0.75 0.95
nipple saddle
>1 <1
operating pressure and column diameter. all (a), (b) and (c).
Questions
The minimum plate spacing in most of the pertroleum refinery distillation columns (of
1
dia > 3 ft) is normally __________ inches.
2 Joint efficiency (J) for a seamless pipe is
For a given design of bubble cap, the number of bubble caps to be used per tray is set
3
by the
The shell side pressure drop in a shell and tube heat exchanger is maximum for
4
__________ baffle.
For a cylinderical vessel of moderate height, the weld joint efficiency for joints parallel
to the cylinderical axis is given as 1.0, while for joints along the girth (circumference) it
7
is given as 0.8. In calculating the shell wall thickness using code formula for an internally
pressurised cylinderical vessel, what value of weld joint efficiency should be used ?
19 Column support for the roof of cylindrical storage tank must be provided for
For a cylinderical internally pressurised vessel, which of the following closure types
20 would withstand highest pressure, if each closure is of the same material and
thickness ?
21 In inclined long tube vertical evaporators, the tubes are inclined at an angle of
In a continuous distillation column, the optimum reflux ratio ranges from __________
22
times the minimum reflux ratio.
The wall thickness for a large high pressure pipeline is determined by the consideration
23
of the
In the case of a shell and tube heat exchanger, the logarithmic mean temperature
24
difference
The minimum tray spacing in distillation column of diameter less than 3 ft is normally
31
__________ inches.
32 Oxygen carrying pipelines in chemical industries are coloured with __________ colour.
Normally, the ratio of the total riser area to the tower cross sectional area (for bubble
33
cap towers of diameter more than 3 ft) is around
Pick out the wrong statement about the design of seive plate column and the bubble
34
cap column.
Maximum size of the raschig rings used in a packed tower is about __________ of the
35
coloumn diameter.
39 Pick out the wrong statement pertaining to a shell and tube heat exchanger.
The practical representative values of HETP for a number of commercial operations lies
43
within a range of __________ metre.
Of the pressure vessels, with same thickness but different diameters, which one
44
withstands higher pressure ?
45 Reflux ratio variation in a distillation column is between
Width and depth of grooves in the tube sheet holes normally are __________ inch
46
respectively.
In condenser, the cooling water is passed in the tube side in a pass arrangement,
47
because
In packed towers provided with pall rings liquid redistributors are positioned at heights
48 of every 6 metres or 5-10 times the column diameter, whichever is less. Maximum size
of the pall rings should not exceed __________ of the column diameter.
keep a check on the liquid gradient over the give access to the individual trays for cleaning,
plate by direct visual observation. maintenance and installation.
low gas velocity. high gas velocity.
0.8 0.9
less more
5 15
< 12.5 >3
2.5 7.5
1000 3000
d √d
if its diameter is less than 15-20metres. if its diameter is more than 50 meters.
welded screwed
relative volatility is close to one (e.g.,
feed is not at its bubble point.
separation of close boiling isomers).
hemispherical ellipsoidal (2 : 1)
15° 90°
1.1 to 1.5 1.6 to 2
forces exerted by static and dynamic action at
axial tensile stress in the pipe.
bends.
25-50 50-75
1/D 1/D^2
6 18
yellow black
0.4-0.6 0.35-0.75
1/10th 1/20th
shear tensile
1 5
The minimum value of baffle spacing is 50 The maximum value of baffle spacing is equal
mm. to the I.D. of the shell.
0.1-0.2 0.2-0.5
1/10-1/15th 1/5-1/10th
1.0 (0.8)^0.5
7.5 50
>5 5-10
15 20
5000 10000
45° 60°
2.2 to 2.6 2.7 to 3
circumferential pipewall tension. temperature stresses.
200-250 750-1000
1/D^5 D^2
24 34
blue red
0.1-0.2 0.55-0.85
1/30th 1/50th
compressive thermal
15 25
0.4-0.9 1.2-1.5
In a shell and tube heat exchanger having triangular pitch, the shell side equivalent
13
diameter is given by
If a single tube pass heat exchanger is converted to two passes; for the same flow rate,
14
the pressure drop per unit length in tube side will __________ times.
Pick out the wrong statement pertaining to the design of a long tube vertical
16
evaporator.
Which of the following is the most common type of baffle used in industrial shell and
17
tube heat exchanger ?
What is the minimum recommended ligament for square pitch arrangement in case of
18
heat exchangers ?
The centre to centre distance between two consecutive baffles in a shell and tube heat
25 exchanger is called the baffle pitch or baffle spacing, which is more than 1/5th the I.D.
of the shell. Which of the following is not a function of the baffles ?
A high vapour velocity is required for high plate efficiency in a seive plate coloumn. The
26 satisfactory value of operating vapor velocity for design purpose in seive plate column is
about __________ percent of the flooding velocity.
27 The approximate liquid depth in an agitation tank is equal to (where, d = tank diameter)
28 Baffle width is normally taken as __________ times the tank diameter.
A cylinderical pressure vessel of volume 6 πm3 has to be designed to withstand a
maximum internal pressure of 10 atm. The allowable design stress of the material is
29
125N/mm2 and corrosion allowance is 2 mm. The thickness of the vessel for a
length/diameter ratio of 3 will be close to
30 Which of the following packing materials provides for maximum mass transfer ?
31 __________ of water makes it a widely used coolant in heat exchangers.
The equivalent diameter for fluid flow through a channel of constant non-circular cross
32 section of area 'A' is given by (where, P = perimeter of the channel in contact with the
fluid)
Fouling factor must be included in the calculation of over all design heat transfer
33
coefficient, when the liquid
34 Lug support is meant for supporting __________ vessels.
Overall mass transfer co-efficient in case of absorption of __________ in water is based
35 on the gas film co-efficient only, as the mass transfer process is gas film (phase)
controlling.
Which tube arrangement in a heat exchanger would facilitate highest heat transfer
36
rate ?
In case of 1.5" heat exchanger tubes, the inside flow area __________ with decrease in
37
BWG.
Cylindrical pressure vessels in horizontal condition is generally supported on a
38
__________ support.
39 Pressure drop per tray in the atmospheric distillation column is about __________ psi.
40 Welded joint efficiency in the design of chemical process equipment is taken as
The thickness of segmental baffles (25 -35% cut truncated plates usually) is generally
41
__________ the tube wall thickness.
The safe height (h) to diameter (d) ratio (i.e., h/d) for liquid/petro fuel storage tank of
42
capacity more than 45 kilolitres is less than
For given number of passes, pitch & tube diameter, the maximum number of tubes that
43
can be accommodated in a shell of tripled inside diameter will be __________ times.
In seive plate column, holes are drilled or punched in sizes ranging from 2.5 to 12 mm (5
47 mm being widely used). The hole pitch is normally __________ times the hole diameter
to give the required hole area.
49 The force due to wind load acting on a tall vessel depends upon its
Bubble cap diameter used for the distillation column having diameter ranging from 1.5
50
to 4.5 metres is about __________ mm.
conical flat
leads to high tray efficiency. results in higher pressure drop per tray.
Plate efficiency increases with increase in Increase in depth of the liquid about the slots
superficial vapour velocity till entrainment increases the plate efficiency, particularly if
limit. the liquid depth is < 1".
2.5 5
half twice
d = 1.1 t d = 1.6 √ t
positive negative
2 2^0.8
Tube dia is 3-6 cms, while tube length in 3-6 Steam is fed to the shell, whereas the liquor is
metres. filled inside the tube.
Centre to centre distance between two A rivetted joint made in overlapping plates is
consecutives rivets in a row is called the pitch. called butt joint.
45 60
0.5 d 0.75 d
0.1-0.12 0.4-0.5
5 mm 6 mm
4 A/P A/P
containing suspended solids flows at low containing suspended solids flows at high
velocity. velocity.
large horizontal cylindrical tall but empty
CO2 SO2
increases decreases
lug skirt
0.01 - 0.5 0.07 - 0.12
0.55 0.75
equal to twice
1 2
a finite stage contactor. used only for distillation, not for absorption.
12.5 17.5
d = 1.5 t 3√ t
no none of these
turbulence noise
equal to not related with
both (a) and (b). neither (a) nor (b).
80 95
d 2d
0.45-0.6 0.2-0.45
8 mm 10 mm
4 P/A √A
3 3.5
5 to 10 10 to 15
Shank diameter of the rivets should be less The efficiency of a rivetted joint is the ratio of
than the size of the hole drilled in the plate the strength of the rivetted joint to the
for rivetting. strength of the solid plate.
For a 25 mm hole drilled in plates to be rivetted, the shank diameter of the rivet should
4
be __________ mm.
In a shell and tube heat exchanger having square pitch, the shell side equivalent
5
diameter is given by (where, P = pitch, d = outside diameter of the tube)
Pressure differential maintained across a continuous rotary vacuum filter is in the range
7
of __________ mm Hg column.
8 Vertical storage vessels are never supported by __________ support.
In a double pipe (concentric) heat exchanger, the hydraulic radius for heat transfer (for
9
a fluid flowing through the annulus) would be
Elastic failure of a material occurs, when the tensile stress equals yield strength, yield
point or the elastic limit. Also, the elastic failure occurs according to maximum strain
10
theory, when the maximum tensile strain equals (where, σ = yield strength and E =
modulus of elasticity)
What is the slope of the feed line, if the feed to a distillation column is a saturated liquid
12
?
In a shell and tube heat exchanger for a given heat transfer surface area, smaller
15 diameter tubes are favoured as compared to larger diameter ones ; because the smaller
diameter tubes
16 (1) for 90° elbow (medium radius) and 90°square elbow would be respectively around
17 __________ heat exchanger is also known as 'hair pin type' exchanger,
What is the value of 'q' for saturated vapor feed to a distillation column ?(where q =
18
fraction of the feed stream that is liquid.)
In hydrostatic testing of welded pipe (for leakage, strength etc.) the ratio of minimum
19
hydrostatic test pressure to internal design pressure is around
Frame thickness in the plate and frame filter press is normally in the range of
20
__________ inches.
21 Cylinderical shell thickness of rotary drier is generally __________ mm.
22 The ratio of lateral strain to linear strain is termed as the
23 The distance between the centre of a rivet hole to the nearest edge of the plate is called
Mc Cable Thiele method used for finding theoretical stages in a distillation column
24
assumes that the
27 Pick out the wrong statement pertaining to shell and tube heat exchanger.
28 Wind load consideration in the design of a support can be neglected, when the vessel is
Souders Brown equation given by, , is used for the calculation of the __________ in a
29
continuous distillation column.
The ratio of volumes of the mixed reactor to the plug flow reactor (for identical feed
30
composition, flow rate, conversion, and for all positive reaction orders) is always
Steam economy is defined as the amount of evaporation per unit amount of steam
31 used, while the capacity is the total evaporation obtained per hour. Use of multiple
effect in evaporation
32 (1) for a Tee (used as elbow, entering run) would be around
Log mean temperature difference in case of multi-pass shell and tube heat exchanger is
33
always
Practical dividing line between a ductile and brittle materials is suggested, when the
ultimate elongation is about 5%. Generally, larger the knuckle radius, stronger is the
34
corner torus section of a head. The knuckle radius provided should be less than
__________ of the head.
Tubes are fixed to the tube sheet (a thick circular metallic plate) by the method of tube
rolling and brazing (non-removable) or ferrule connection (removable). Thickness of the
35
tube, sheet is normally __________ the outside diameter of the tube but in no case it
should be less than 22 mm (7/8").
A shell may by termed as thin if its thickness to diameter ratio is less than 0.1. The
36
factor which can be neglected in the calculation of membrane stresses is
Scale up problem in design based on the similarity concept takes into account
37
__________ similarity.
38 __________ closure is the weakest enclosure for cylindrical vessels.
39 Which of the following efficiencies can be greater than 100% ?
height & properties of the liquid. agitator type & speed of agitation.
1 2
25 23
E σ
two five
0 ∞
0.5 1.5
0.25 to 4 0.25 to 8
2-3 18-22
Poisson's ratio bulk modulus
pitch margin
19 38
If sufficient residence time (around 8 seconds) The liquid head in the downcomer should not
is not proivided to the downcoming liquid in be greater than one half the plate spacing to
the downcomer, it may entrain some vapour. avoid flooding.
diameter of the bubble cap column diameter of the seive plate column
1 <1
less than arithmetic mean value. more than arithmetic mean value.
bending deformation
geometrical kinematic
Hemispherical Torispherical
Overall plate efficiency. Murphree plate efficiency.
size of agitator & the tank. all (a), (b) and (c).
3.5 5.5
A reducer is used to change the direction of a The method of fixing tubes to a tube sheet by
pipe in a straight run. expanding is called 'tube rolling'.
26 27
πd/4P^2
σ/E E/σ
ten twenty
> 1 <1
2.5 3.5
1 to 5 1 to 12
6-8 12-15
modulus of elasticity shear modulus
back pitch none of these
76 95
either (a) or (b), whichever is larger either (a) or (b), whichever is smaller
shear elongation