Curriculum - Chemical Laboratory Assistant

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CHEMICAL LABORATORY

ASSISTANT
COMPETENCY BASED CURRICULUM
(Duration: 2 Yrs.)

APPRENTICESHIP TRAINING SCHEME (ATS)


NSQF LEVEL- 5

SECTOR – CHEMICAL SECTOR

GOVERNMENT OF INDIA
MINISTRY OF SKILL DEVELOPMENT & ENTREPRENEURSHIP
DIRECTORATE GENERAL OF TRAINING

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CHEMICAL LABORATORY ASSISTANT

CHEMICAL LABORATORY
ASSISTANT
(Revised in 2018)
APPRENTICESHIP TRAINING SCHEME (ATS)

NSQF LEVEL - 5

Developed By

Ministry of Skill Development and Entrepreneurship


Directorate General of Training
CENTRAL STAFF TRAINING AND RESEARCH INSTITUTE
EN-81, Sector-V, Salt Lake City,
Kolkata – 700 091
CHEMICAL LABORATORY ASSISTANT
ACKNOWLEDGEMENT
The DGT sincerely expresses appreciation for the contribution of the Industry, State
Directorate, Trade Experts and all others who contributed in revising the curriculum. Special
acknowledgement to the following industries/organizations who have contributed valuable inputs
in revising the curricula through their expert members:

1. Bharat Petroleum Corporation Limited , Mahul Refinery , Mahul Mumbai


2. Hindustan Petroleum Corporation Limited , Mahul Refinery ,Mahul Mumbai
3. Rashtriya Chemicals and Fertilizers Limited, Chembur ,Mumbai
4. Directorate of Vocational Education and Training, Maharashtra State,Mumbai
5. N.G. Acharya & D. K. Marathe College, Chembur, Mumbai

Special acknowledgement is extended by DGT to the following expert members who had
contributed immensely in this curriculum.

Co-ordinator for the course: Shri Sunil Wakde , ADT, Advanced Training Institute,, Mumbai

Sl. Name & Designation Organization Remarks


No. Sri /Mr./Ms.

1. Dr. Vidyagauri Lele, N. G. Acharya & D. K. Member


Principal &HOD (Chemistry Dept.) Marathe College,
Chembur Mumbai
2. Sri S. A. Salvi , Hindustan Petroleum Member
Sr. Shift Chemist (Quality Control ) Corporation Limited ,
Mahul Refinery , Mahul
3. Sri Hamant K. Ghag Mumbai
Bharat Petroleum Member
Sr. Manager, (Quality Control ) Corporation Limited ,
Mahul Refinery , Mahul
Mumbai
4. Sri Girish Labhane, Rashtriya Chemicals and Member
Sr. Engineer (Mechanical ) Fertilizers Limited,
Chembur ,Mumbai

5. Sri Vimal K. Gulati, Bharat Petroleum Member


Sr. Manager ( Training& Development ) Corporation Limited ,
Mahul Refinery , Mahul
6. Sri Nitin Kumar Mumbai
Hindustan Petroleum Member
Sr. Engineer (Operations ) Corporation Limited
,Mahul Refinery , Mahul
Mumbai
CHEMICAL LABORATORY ASSISTANT
7. Sri R.C. Sonavane ,Trade Instructor Govt. ITI ,Panvel Member
8. Sri P.S.Rane ,Trade Instructor Govt. ITI ,Panvel Member
9. Sri C.P. Jadhav, Trade Instructor Govt. ITI ,Panvel Member
10. Mrs. S.G. Thakur, Govt. ITI ,Mahad Member
Junior Apprenticeship Advisor
11. Mrs. S. S. Barve ,Trade Instructor Govt. ITI ,Mahad Member

12. Sri S.E. Deshmukh, Trade Instructor Govt. ITI ,Mahad Member

13. Sri G.W. Patil, Trade Instructor Govt. ITI ,Mahad Member

14. Sri S.Z. Rajput , Trade Instructor Govt. ITI ,Mahad Member

15. Sri S.G. Raigonde ,Deputy Director (T) ATI, Mumbai Member

16. Sri C.H. Ravi, Deputy Director(T) ATI, Mumbai Member

17. Sri Ujjwal Biswas, Deputy Director(T) ATI, Mumbai Member

18. Mrs. K.K. Phadnis ,Training Officer ATI, Mumbai Member

19. Sri R.S. Wagh, Training Officer ATI, Mumbai Member


CHEMICAL LABORATORY ASSISTANT
CONTENTS

Sl.
Topics Page No.
No.
1. Background 1-2
2. Training System 3-7
3. Job Role 8-9
4. NSQF Level Compliance 10
5. General Information 11
6. Learning Outcome 12-15
7. Learning Outcome with Assessment Criteria 16-18
8. Syllabus 19-22
9. Syllabus - Core Skill 23-29
9.1 Core Skill – Workshop Calculation & Science and
Engineering Drawing
9.2 Core Skill – Employability Skill
10. Details of Competencies (On-Job Training) 30-32
11. List of Trade Tools & Equipment Basic Training - Annexure I 33-41
12. Format for Internal Assessment -Annexure II 42
CHEMICAL LABORATORY ASSISTANT
1. BACKGROUND

1.1 Apprenticeship Training Scheme under Apprentice Act 1961

The Apprentices Act, 1961 was enacted with the objective of regulating the programme of
training of apprentices in the industry by utilizing the facilities available therein for
imparting on-the-job training. The Act makes it obligatory for employers in specified
industries to engage apprentices in designated trades to impart Apprenticeship Training on
the job in industry to school leavers and person having National Trade Certificate(ITI
pass-outs) issued by National Council for Vocational Training (NCVT) to develop skilled
manpower for the industry. There are four categories of apprentices namely; trade
apprentice, graduate, technician and technician (vocational) apprentices.
Qualifications and period of apprenticeship training of trade apprentices vary from trade
to trade. The apprenticeship training for trade apprentices consists of basic training
followed by practical training. At the end of the training, the apprentices are required to
appear in a trade test conducted by NCVT and those successful in the trade tests are
awarded the National Apprenticeship Certificate.

The period of apprenticeship training for graduate (engineers), technician (diploma


holders and technician (vocational) apprentices is one year. Certificates are awarded on
completion of training by the Department of Education, Ministry of Human Resource
Development.

1.2 Changes in Industrial Scenario

Recently we have seen huge changes in the Indian industry. The Indian Industry registered
an impressive growth during the last decade and half. The number of industries in India
have increased manifold in the last fifteen years especially in services and manufacturing
sectors. It has been realized that India would become a prosperous and a modern state by
raising skill levels, including by engaging a larger proportion of apprentices, will be
critical to success; as will stronger collaboration between industry and the trainees to
ensure the supply of skilled workforce and drive development through employment.
Various initiatives to build up an adequate infrastructure for rapid industrialization and
improve the industrial scenario in India have been taken.

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CHEMICAL LABORATORY ASSISTANT
1.3 Reformation
The Apprentices Act, 1961 has been amended and brought into effect from 22 nd
December, 2014 to make it more responsive to industry and youth. Key amendments are
as given below:

 Prescription of number of apprentices to be engaged at establishment level instead of


trade-wise.

 Establishment can also engage apprentices in optional trades which are not designated,
with the discretion of entry level qualification and syllabus.

 Scope has been extended also to non-engineering occupations.

 Establishments have been permitted to outsource basic training in an institute of their


choice.

 The burden of compliance on industry has been reduced significantly.

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CHEMICAL LABORATORY ASSISTANT
2. TRAINING SYSTEM
2.1 GENERAL

Directorate General of Training (DGT) under Ministry of Skill Development &


Entrepreneurship offers range of vocational training courses catering to the need of different sectors
of economy/ Labour market. The vocational training programmes are delivered under aegis of
National Council of Vocational Training (NCVT). Craftsman Training Scheme (CTS) and
Apprenticeship Training Scheme (ATS) are two pioneer programmes of NCVT for propagating
vocational training.

Chemical Laboratory Assistant trade under ATS is one of the most popular courses delivered
nationwide through different industries. The course is of two years (02 Blocks) duration. It mainly
consists of Domain area and Core area. In the Domain area Trade Theory & Practical impart
professional - skills and knowledge, while Core area - Workshop Calculation and science,
Engineering Drawing and Employability Skills imparts requisite core skills & knowledge and life
skills. After passing out the training programme, the trainee is being awarded National
Apprenticeship Certificate (NAC) by NCVT having worldwide recognition.

Broadly candidates need to demonstrate that they are able to:

 Read & interpret technical parameters/document, plan and organize work processes, identify
necessary materials and tools;
 Perform task with due consideration to safety rules, accident prevention regulations and
environmental protection stipulations;
 Apply professional skill, knowledge, core skills & employability skills while performing jobs
and solve problem during execution.
 Check the job/finishing and assembly as per drawing for functioning, identify and rectify
errors in job/assembly.
 Document the technical parameters related to the task undertaken.

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CHEMICAL LABORATORY ASSISTANT
2.2 CAREER PROGRESSION PATHWAYS:

 Can join Crafts Instructor Training Scheme (CITS) in the trade for becoming instructor in
ITIs.
 Indicative pathways for vertical mobility.

2.3 COURSE STRUCTURE:

Table below depicts the distribution of training hours across various course elements during a
period of two years (Basic Training and On-Job Training): -

Total training duration details: -

Time 1-3 4-12 13-15 16-24


(in months)
Basic Training Block– I ----- Block – II ------
Practical Training ---- Block – I ------ Block – II
(On - job training)

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CHEMICAL LABORATORY ASSISTANT
A. Basic Training
For 02 yrs. course :-(Total 06 months: 03 months in 1styr. + 03 months in 2nd yr.)
For 01 yr. course :- (Total 03 months: 03 months in 1st yr.) \

S No. Course Element Total Notional Training Hours

For 02 Yrs. For 01 Yr.


course course
1. Professional Skill (Trade Practical) 550 275
2. Professional Knowledge (Trade Theory) 240 120
3. Workshop Calculation & Science 40 20
4. Engineering Drawing 60 30
5. Employability Skills 110 55

Total (Including internal assessment) 1000 500

B. On-Job Training:-

For 02 yrs. Course :-( Total 18 months: 09 months in 1st yr. + 09 months in 2nd yr.)

Notional Training Hours for On-Job Training: 3120 Hrs.

For 01 yr. course :-( Total 12 months)

Notional Training Hours for On-Job Training: 2080 Hrs.

C. Total training hours:-


Duration Basic Training On-Job Training Total

For 02 yrs. 1000 hrs. 3120 hrs. 4120 hrs.


Course( Engg.)
For 01 yr. 500 hrs. 2080 hrs. 2580 hrs.
Course ( Engg.)

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CHEMICAL LABORATORY ASSISTANT

2.4 ASSESSMENT & CERTIFICATION:

The trainee will be tested for his skill, knowledge and attitude during the period of course and at
the end of the training programme as notified by Govt of India from time to time. The Employability
skills will be tested in first two semesters only.

a) The Internal assessment during the period of training will be done by Formative assessment
method by testing for assessment criteria listed against learning outcomes. The training institute have
to maintain individual trainee portfolio as detailed in assessment guideline (section-2.4.2). The marks
of internal assessment will be as per the template (Annexure – II).

b) The final assessment will be in the form of summative assessment method. The All India Trade
Test for awarding NAC will be conducted by NCVT on completion of course as per guideline of
Govt of India. The pattern and marking structure is being notified by govt of India from time to time.
The learning outcome and assessment criteria will be basis for setting question papers for final
assessment. The examiner during final examination will also check individual trainee’s profile as
detailed in assessment guideline (section-2.4.2) before giving marks for practical examination.

2.4.1 PASS REGULATION


The minimum pass percent for Practical is 60% & minimum pass percent for Theory subjects
40%. The candidate pass in each subject conducted under all India trade test.

2.4.2 ASSESSMENT GUIDELINE

Appropriate arrangements should be made to ensure that there will be no artificial barriers to
assessment. The nature of special needs should be taken into account while undertaking assessment.
Due consideration should be given while assessing for team work, avoidance/reduction of
scrap/wastage and disposal of scarp/wastage as per procedure, behavioral attitude, sensitivity to
environment and regularity in training. The sensitivity towards OSHE and self-learning attitude are to
be considered while assessing competency.

Assessment will be evidence based comprising the following:

 Job carried out in labs/workshop


 Record book/ daily diary
 Answer sheet of assessment
 Viva-voce
 Progress chart
 Attendance and punctuality
 Assignment
 Project work

Evidences of internal assessments are to be preserved until forthcoming semester examination

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CHEMICAL LABORATORY ASSISTANT
for audit and verification by examination body. The following marking pattern to be adopted while
assessing:

Performance Level Evidence

(a) Weightage in the range of 60 -75% to be allotted during assessment


For performance in this grade, the candidate  Demonstration of good skill in the use of hand
with occasional guidance and showing due tools, machine tools and workshop equipment
regard for safety procedures and practices, has  Below 70% tolerance dimension/accuracy
produced work which demonstrates attainment achieved while undertaking different work with
of an acceptable standard of craftsmanship. those demanded by the component/job/set
standards.
 A fairly good level of neatness and consistency
in the finish
 Occasional support in completing the
project/job.

(b)Weightage in the range of above75% - 90% to be allotted during assessment


For this grade, the candidate, with little  Good skill levels in the use of hand tools,
guidance and showing due regard for safety machine tools and workshop equipment
procedures and practices, has produced work  70-80% tolerance dimension/accuracy achieved
which demonstrates attainment of a reasonable while undertaking different work with those
standard of craftsmanship. demanded by the component/job/set standards.
 A good level of neatness and consistency in the
finish
 Little support in completing the project/job

(c) Weightage in the range of above 90% to be allotted during assessment


For performance in this grade, the candidate,  High skill levels in the use of hand tools,
with minimal or no support in organization and machine tools and workshop equipment
execution and with due regard for safety  Above 80% tolerance dimension/accuracy
procedures and practices, has produced work achieved while undertaking different work with
which demonstrates attainment of a high those demanded by the component/job/set
standard of craftsmanship. standards.
 A high level of neatness and consistency in the
finish.
 Minimal or no support in completing the
project.

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CHEMICAL LABORATORY ASSISTANT
3. JOB ROLE

Brief description of Job roles:

1. Chemical Laboratory Assistant, arranges and sets various chemicals, instruments and
apparatus such as salts, acids, balances, heaters as desired by Chemists for conducting
experiments in chemical laboratory. Sets up required apparatus and equipment as directed by
Chemist. Performs routine tasks, such as preparations of standard solutions and common
reagents, weighing and measuring of salts and chemicals, filtration, precipitation etc.

2. Chemical Laboratory Assistant, Glass and Ceramics conducts routine tests of silica,
clay and other ingredients in laboratories for manufacturing glass and ceramic products. Sets
up apparatus required for performing test to determine properties of clay, silica, etc. Prepares
solution and reagents. Maintains charts and tables for data observed during experimentation.
May undertake tests in laboratory independently.

3. Laboratory Assistant, Chemical Engineering, General conducts chemical and physical


laboratory tests and makes qualitative and quantitative analysis of material for purposes such
as development of new products, materials, and processing methods and for maintenance of
health and safety standards.

4. Biochemists; Chemists, Analytical; Chemists, Inorganic; Chemists, Organic; or


Chemists, Physical. Sets up laboratory equipment and instruments, such as ovens, leaching
drums, gas cylinders, kilns vacuum chambers autoclaves, pyrometers and gas analyzer.
Analyses products, such as drugs, plastics, dyes and paints to determine strength, purity and
other characteristics of chemical contents. Tests ores, minerals, gases and other materials for
presence and percentage of elements and substance, such as Carbon, Tungsten, nitrogen, iron,
gold or nickel. Prepares chemical solutions for use in processing materials, such as textile ,
detergents, paper, felt etc., following standard formulas.

5. Chemical Laboratory Assistant, Petroleum and Lubricants; Crude Tester; Oil Tester;
Gas Analyst (Petroleum refining) tests and analyses samples of crude oil and petroleum
products during processing stages, using laboratory apparatus and testing equipment and
following standard test procedures to determine physical and chemical properties and ensures
prescribed standards of products manufactured. Tests samples of crude and blended oils,
gases, asphalts, and pressure distillates to determine characteristics, such as boiling, vapour,
freeze, condensation, flash and aniline points, viscosity, specific gravity, penetration, doctor
solution, distillation and corrosion, using test and laboratory equipment, such as hydrometers,
fractionators, factional distillation apparatus and analystical scales. Analyses contents of
products to determine presence of gases, such as propane, iso-butane, butane, isopentane, and
ethane using appropriate distillation columns. Determines hydro carbon composition of
gasolines, blending stocks, and gases using fractional distillation equipment and mass
sperctrometer. Operates fractional columns to separate crude oil into oils with different
boiling points to determine their properties. Analyses composition of products to determine
quantitavie presence of gum, sulfar, aromatics olefins, water and sediment. Compares colour
of liquid product with charts to determine processing factors measurable by colour. Compares

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CHEMICAL LABORATORY ASSISTANT
tests results with specifications and recommends processing changes to improve and control
quality of products. May test sub-surface cores during drilling operations.
6. Laboratory Assistant, Metallurgical conducts routine tests of metals and alloys to determine
their physical and chemical properties. Collects metallic wastes, metal samples or ores to be
examined. Sets up scientific equipment required for testing. Assist Metallurgist in testing and
analysing different types of metals, their by-products, waste and alloys. May conduct
examination of metals on his initiative independently.

NCO Code 2015:


3111.0300 _ Laboratory Assistant, Chemical

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CHEMICAL LABORATORY ASSISTANT

4. NSQF LEVEL COMPLIANCE

NSQF level for Chemical Laboratory Assistant trade under ATS: Level 5

As per notification issued by Govt. of India dated- 27.12.2013 on National Skill Qualification
Framework total 10 (Ten) Levels are defined.

Each level of the NSQF is associated with a set of descriptors made up of five outcome
statements, which describe in general terms, the minimum knowledge, skills and attributes that a
learner needs to acquire in order to be certified for that level.

Each level of the NSQF is described by a statement of learning outcomes in five domains,
known as level descriptors. These five domains are:

a. Process
b. professional knowledge,
c. professional skill,
d. core skill and
e. Responsibility.

The Broad Learning outcome of Chemical Laboratory Assistant trade under ATS mostly
matches with the Level descriptor at Level- 5.

The NSQF level-5 descriptor is given below:

LEVEL Process required Professional Professional Core skill Responsibility


knowledge skill
Level 5 Job that requires knowledge a range of Desired Responsibility for
well developed of facts, cognitive and mathematical own work and
skill, with clear principles, practical skills skill, Learning and some
choice of processes and required to understanding of responsibility for
procedures in general accomplish social, political other’s works and
familiar context. concepts, in a tasks and solve and some skill of learning.
field of problem by collecting and
work selecting and organizing
or study applying basic information,
methods, tools, communication.
materials and
information.

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CHEMICAL LABORATORY ASSISTANT
5. GENERAL INFORMATION
Name of the Trade Chemical Laboratory Assistant
NCO-2015 3111.30
NSQF Level Level – 5
Duration of Apprenticeship
Training Two years (02 Blocks each of one year duration).
(Basic Training + On-Job Training)
Duration of Basic Training a) Block –I : 3 months
b) Block – II : 3 months
Total duration of Basic Training: 6 months
Duration of On-Job Training a) Block–I: 9 months
b) Block–II : 9 months
Total duration of Practical Training: 18 months
Entry Qualification Passed 10th class examination under 10+2 system of education
with physics, chemistry and mathematics or its equivalent
Selection of Apprentices The apprentices will be selected as per Apprenticeship Act
amended time to time.
Instructors Qualification for As per ITI instructors qualifications as amended time to time for
Basic Training the specific trade.
Infrastructure for Basic As per related trades of ITI
Training
Examination The internal examination/ assessment will be held on completion
of each block.
Final examination for all subjects will be held at the end of course
and same will be conducted by NCVT.

Rebate to Ex-ITI Trainees 01 year


CTS trades eligible for 1. Chemical Laboratory Assistant
Chemical Laboratory
Assistant Apprenticeship

Note:
 Industry may impart training as per above time schedule for different block, however this is not fixed. The
industry may adjust the duration of training considering the fact that all the components under the syllabus must
be covered. However the flexibility should be given keeping in view that no safety aspects is compromised .
 For imparting Basic Training
 The industry to tie-up with ITIs having such specific trade and affiliated to NCVT.

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CHEMICAL LABORATORY ASSISTANT

6. LEARNING OUTCOME

6.1GENERIC LEARNING OUTCOME

The following are minimum broad Common Occupational Skills/ Generic Learning Outcome
after completion of the Chemical Laboratory Assistant course of 02 years duration under ATS.

Block I & II:-

1. Recognize & comply safe working practices, environment regulation and housekeeping.

2. Understand and explain different mathematical calculation & science in the field of study
including basic electrical. [Different mathematical calculation & science -Work, Power &
Energy, Algebra, Geometry & Mensuration, Trigonometry, Heat & Temperature, Levers &
Simple machine, graph, Statistics, Centre of gravity, Power transmission, Pressure]

3. Interpret specifications, different engineering drawing and apply for different application in
the field of work. [Different engineering drawing-Geometrical construction, Dimensioning,
Layout, Method of representation, Symbol, scales, Different Projections, Machined
components & different thread forms, Sectional views, Estimation of material, Electrical &
electronic symbol]

4. Select and ascertain measuring instrument and measure dimension of components and record
data.

5. Explain the concept in productivity, quality tools, and labour welfare legislation and apply
such in day to day work to improve productivity & quality.

6. Explain energy conservation, global warming and pollution and contribute in day to day work
by optimally using available resources.

7. Explain personnel finance, entrepreneurship and manage/organize related task in day to day
work for personal & societal growth.

8. Plan and organize the work related to the occupation.

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CHEMICAL LABORATORY ASSISTANT
6.2 SPECIFIC LEARNING OUTCOME

Block – I

1. ORIENTATION:-
 Knowledge about the Plant – its raw materials, products, capacity of production etc..
 Knowledge of the process with the help of a simple flow sheet under the guidance of the plant in-
charge / supervisors in the plant.
 Write the report (diary) of day to day work.
 Familiar with various types of testing and analysis equipments etc.
2. SAFTEY :-
 Knowledge about the Cause and prevention of accidents.
 Knowledge about the Personnel safety and use of personnel protective equipments.
 Plan and maintain the House Keeping.
 Operate fire fighting extinguisher and knowledge of the Fire prevention.
 Handle the hazardous chemicals
 Handle the Glassware very carefully.
 Explain the Behaviour Based Safety (BBS)
3. Prepare solution and operate weighing balance for sampling to prepare different types of solution
as per the Equivalent weight, Molecular weight, Atomic weight, Specific gravity, Normality,
Acidity, Basicity, Concentration, Normal Solution and Molar Solutions.
Prepare the acid solutions, basic solutions and oxidizing - reducing agent, solutions.
Prepare solutions of different concentration and determine the concentration and percentage
purity.
4. Prepare the Complexometry solutions, indicators, sampling in solids, liquids and gases.
Standardize the solutions
Prepare the Ethylene diamine tetra acetic acid (EDTA) solution & indicator and titration with
EDTA.
5. Metallurgical analysis
Atomic Absorption Spectrophotometry
Analysis of the different sample (such as Cu, Fe, Mn. etc.) on Atomic Absorption
Spectrophotometer
6. X-ray crystallography:
Determine the different size of crystal samples.
7. Flame Photometry:
Determine the Sodium (Na), Potassium (K), Calcium (Ca) in different industrial samples by
Flame photometer.
8. Check the sample with Electron Microscope.
Perform the Ore analysis, carbon analysis, analysis of Pyrolusite for determining the percentage
of manganese (Mn).
9. Perform the metallurgical analysis in cements industries by using the different volumetric and
gravimetric analytical methods.
10. Perform analysis in Foundry.
11. Perform analysis of Different alloys, brass, solder wire etc.

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CHEMICAL LABORATORY ASSISTANT
12. Gas Chromatography (GC):
Perform the separation of different sample mixture (Industrial products) on gas chromatography.
Identify and determine quantity of the each separated components.
13. High Performance Liquid Chromatography (HPLC):
Perform the separation of different sample mixture (Industrial products) on High Performance
Liquid Chromatography (HPLC).
Identify and determine quantity of the each separated components

Block – II

14. Thin Layer Chromatography (TLC):


Perform the separation of different sample mixture on thin layer chromatography.
15. Gas Chromatography Mass Spectrometry (GC / MS) :
Identify the different sample by using GC/ MS
16. UV – Vis Spectroscopy :
Determine the percentage composition of different sample components.
17. Fourier Transform Infrared Spectrophotometer (IR/FTIR Spectrophotometer):
Perform analysis of different samples (Industrial products)
i) Calibration by polystyrene film
ii) Study of background spectra
iii) Study of different solid samples & analysis of spectrum obtained

18. Explain Water, sources of water and different water treatment processes, de-mineralized (DM)
water ,Industrial water, potable water.
Perform the different sampling techniques used for different water available in industry. Perform
analysis of each water sample for parameters such as PH, alkalinity, Total Dissolved Solids
(TDS), conductivity, total, temporary & permanent hardness of any water sample. Etc.

19. Explain chemical Oxygen Demand (COD), Biochemical Oxygen Demand (BOD), and Dissolved
Oxygen (D.O).
Determine the COD, BOD, DO for different water sample /effluent.

20. Determine the mixed liquor suspended solids (MLSS), Total Dissolved Solids (TDS), Total
Suspended Solids (TSS), PH, Turbidity of given water sample.
Perform analysis for Some Minute Minerals like Magnesium (Mg), Potassium (K), Sodium (Na),
Arsenic (As), etc in Hard water and Soft water
21. Detect the acid value, iodine value, saponification value , flash point, pour point, cloud point,
Viscosity, refractive index, optical rotation, specific rotation of oils, fats and petroleum products
etc. of different Industrial samples.
22. Detect the elements, functional group, Melting point, Boiling point, Technique of purification.
Perform preparation of Compound derivatives.
23. Prepare the organic compounds such as Acetanilide, Aspirin, Phenolphthalein, soap,
Glucosazone etc.
24. Perform collection of sample and then analyse the Microbiological Culture analysis.
25. Detect and prepare the inoculate media.
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CHEMICAL LABORATORY ASSISTANT
Explain the Techniques of inoculation & staining.
26. Operate and Handle the equipments used in microbiological lab such as Centrifuge, pH-Meter,
incubator and Shaker.
27. Explain the Sterilization, fermentation and formulation.
Prepare the different Solutions related to the microbiological lab.

NOTE: Learning outcomes are reflection of total competencies of a trainee and assessment will be
carried out as per assessment criteria.

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CHEMICAL LABORATORY ASSISTANT
7. LEARNING OUTCOME WITH ASSESSMENT CRITERIA

GENERIC LEARNING OUTCOME


LEARNING OUTCOMES ASSESSMENT CRITERIA
1. Recognize & comply safe 1. 1. Follow and maintain procedures to achieve a safe
working practices, environment working environment in line with occupational health
regulation and housekeeping. and safety regulations and requirements.
1. 2. Recognize and report all unsafe situations according to
site policy.
1. 3. Identify and take necessary precautions on fire and
safety hazards and report according to site policy and
procedures.
1. 4. Identify, handle and store / dispose off
dangerous/unsalvageable goods and substances
according to site policy and procedures following
safety regulations and requirements.
1. 5. Identify and observe site policies and procedures in
regard to illness or accident.
1. 6. Identify safety alarms accurately.
1. 7. Report supervisor/ Competent of authority in the event of
accident or sickness of any staff and record accident
details correctly according to site accident/injury
procedures.
1. 8. Identify and observe site evacuation procedures
according to site policy.
1. 9. Identify Personal Productive Equipment (PPE) and use
the same as per related working environment.
1. 10. Identify basic first aid and use them under different
circumstances.
1. 11. Identify different fire extinguisher and use the same as
per requirement.
1. 12. Identify environmental pollution & contribute to
avoidance of same.
1. 13. Take opportunities to use energy and materials in an
environmentally friendly manner
1. 14. Avoid waste and dispose waste as per procedure
1. 15. Recognize different components of 5S and apply the
same in the working environment.

2. Understand, explain different 2.1 Explain concept of basic science related to the field such as
mathematical calculation & Material science, Mass, weight, density, speed, velocity,
science in the field of study heat & temperature, force, motion, pressure, heat treatment,
including basic electrical and centre of gravity, friction.
apply in day to day 2.2 Measure dimensions as per drawing
work.[Different mathematical 2.3 Use scale/ tapes to measure for fitting to specification.
calculation & science -Work, 2.4 Comply given tolerance.
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CHEMICAL LABORATORY ASSISTANT
Power & Energy, Algebra, 2.5 Prepare list of appropriate materials by interpreting detail
Geometry & Mensuration, drawings and determine quantities of such materials.
Trigonometry, Heat & 2.6 Ensure dimensional accuracy of assembly by using
Temperature, Levers & Simple different instruments/gauges.
2.7 Explain basic electricity, insulation & earthing.
machine, graph, Statistics,
Centre of gravity, Power
transmission, Pressure]

3. Interpret specifications, 3. 1. Read & interpret the information on drawings and apply in
different engineering drawing executing practical work.
and apply for different 3. 2. Read & analyse the specification to ascertain the material
application in the field of work. requirement, tools and machining /assembly /maintenance
[Different engineering drawing- parameters.
Geometrical construction, 3. 3. Encounter drawings with missing/unspecified key
Dimensioning, Layout, Method information and make own calculations to fill in missing
of representation, Symbol, dimension/parameters to carry out the work.
scales, Different Projections,
Machined components &
different thread forms, Sectional
views, Estimation of material,
Electrical & electronic symbol]

4. Select and ascertain measuring 4.1 Select appropriate measuring instruments such as
instrument and measure micrometers, vernier calipers, dial gauge, bevel protector
dimension of components and and height gauge (as per tool list).
record data. 4.2 Ascertain the functionality & correctness of the instrument.
4.3 Measure dimension of the components & record data to
analyse them with given drawing/measurement.

5. Explain the concept in 5.1 Explain the concept of productivity and quality tools and
productivity, quality tools, and apply during execution of job.
labour welfare legislation and 5.2 Understand the basic concept of labour welfare legislation
apply such in day to day work to and adhere to responsibilities and remain sensitive towards
improve productivity & quality. such laws.
5.3 Knows benefits guaranteed under various acts

6. Explain energy conservation, 6.1 Explain the concept of energy conservation, global
global warming and pollution warming, pollution and utilize the available recourses
and contribute in day to day optimally & remain sensitive to avoid environment
work by optimally using pollution.
available resources. 6.2 Dispose waste following standard procedure.

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CHEMICAL LABORATORY ASSISTANT
7. Explain personnel finance, 7. 1. Explain personnel finance and entrepreneurship.
entrepreneurship and 7. 2. Explain role of Various Schemes and Institutes for self-
manage/organize related task in employment i.e. DIC, SIDA, SISI, NSIC, SIDO, Idea for
day to day work for personal & financing/ non financing support agencies to familiarizes
societal growth. with the Policies /Programmes & procedure & the available
scheme.
7. 3. Prepare Project report to become an entrepreneur for
submission to financial institutions.

8. Plan and organize the work 8. 1. Use documents, drawings and recognize hazards in the
related to the occupation. work site.
8. 2. Plan workplace/ assembly location with due consideration
to operational stipulation
8. 3. Communicate effectively with others and plan project tasks
8. 4. Assign roles and responsibilities of the co-trainees for
execution of the task effectively and monitor the same.
SPECIFIC OUTCOME
Block-I & II (Section:10)
Assessment Criteria i.e. the standard of performance, for each specific learning
outcome mentioned under block – I & block – II(section: 10) must ensure that the
trainee achieves well developed skill with clear choice of procedure in familiar
context. Assessment criteria should broadly cover the aspect of Planning (Identify,
ascertain, estimate etc.); Execution (perform, illustration, demonstration etc. by
applying 1) a range of cognitive and practical skills required to accomplish tasks and
solve problems by selecting and applying basic methods, tools, materials and
information 2) Knowledge of facts, principles, processes, and general concepts, in a
field of work or study 3)Desired Mathematical Skills and some skill of collecting and
organizing information, communication) and Checking/ Testing to ensure
functionality during the assessment of each outcome. The assessments parameters
must also ascertain that the candidate is responsible for own work and learning and
some responsibility for other’s work and learning.

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CHEMICAL LABORATORY ASSISTANT
8. SYLLABUS

BASIC TRAINING (Block – I)


Duration: (03) Three Months
Week
No. Professional Skills (275Hrs ) Professional Knowledge (120 Hrs)
Induction Training. General Safety:
Operation of fire extinguisher. Introduction & importance of safety &.
1. Use of personal protective equipments. General precautions observed in the laboratory.
Introduction to Material Safety Data Sheet Fire prevention and fire control in chemical
(MSDS) and personal protection equipments industries. Study of personal protection
(PPEs) used in chemical plant/laboratory. equipments (PPEs) used in chemical plant.
First aid in chemical plant. Introduction to
occupational health hazard. Environmental
pollution, sources, causes, consequences and
controls.
Induction Training.
Fire & Safety in Chemical Lab/Plant/laboratory
First Aid.
Introduction of pollution control.

General & Physical Chemistry


2. Preparation of solutions of solids, liquids, Introduction to chemistry.
volatile, non-volatile, etc. substances. Elements, atoms, molecules and compound.
Preparation of standard & primary standard Chemical & physical changes.
solutions.
Purification & separation of liquid mixture by Methods of purification : distillation
distillation

3. Volumetric Analysis Acid ,base, salt, Atomic Weight, Molecular


(Acidimetric titrations and Alkali metric Weight, Equivalent Weight, Normality,
titration ) Molarity, Molality, ppm, ppb, density, Specific
gravity, Weight - volume relationship
Analysis of acids & bases.

Oxidation-Reduction titration. Structure of Atom.


4. Permanganometry-titration using permanganate To study of Periodic table.
solution. Study IUPAC nomenclature.

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CHEMICAL LABORATORY ASSISTANT
Iodometric and idometric titrations using iodine Electronic Theory of Valence.
5. solution directly or indirectly. Chemical Equilibrium

Precipitation titration. Air and water


6. Complexo metric titrations. Fertilizer

7. Gravimetric Estimation of Aluminum, Copper Metallurgy


& and Sulphate. Metallurgy of:
8. (a) Aluminum.
(b) Copper
9. Inorganic qualitative analysis Extraction of Metal & Non-Metal
&
10. To study Action of pure and salt water on Non-Metals:
metals and alloys Preparation, properties & uses of following:
(a) Hydrogen & its peroxide.
To study action of acids and base on metals (b) Oxygen
alloys

Physics: Simple Machines: Efforts and Load,


(a) Law of parallelogram of forces with the Mechanical Advantage (MA), Velocity Ratio
11. help of mechanical board. (VR), efficiency of machines, the relationship.
(b) Simple pendulum. Simple Harmonic motion.
Electricity:

(a) Electric cell in series connection & Electric current, positive and negative terminal
parallel use of fuses and switches, conductors and
12. connections insulators, simple electrical circuits, Ohms law,
(b) To study ohm’s law Kirchhoff’s law, Parallel and Series circuit
(c) To Study Kirchhoff’s law about current and connections.
voltage

Verification of Faraday’s first law of Electrolysis & Faraday’s laws


13. electrolysis.

Revision
Internal Assessment 03days

NOTE: -

More emphasis to be given on video/real-life pictures during theoretical classes. Some real-life
pictures/videos of related industry operations may be shown to the trainees to give a feel of Industry
and their future assignment.
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CHEMICAL LABORATORY ASSISTANT
BASIC TRAINING (Block – II)
Duration: (03) Three Months
Week
No. Professional Skills (275Hrs ) Professional Knowledge( 120 Hrs )

Preparation of organic compounds Nitration Introduction to organic chemistry


Laboratory preparation of nitro benzene
1. And percentage yield determination. Purification of organic compound.

Oxidation
Laboratory preparation of oxalic acid.

Diazotization: Types of organic reaction


Preparation of methyl orange.
Estimation of Elements
2. Ozazone:
Preparation of gluecosazone. Empirical Formula and Molecular formula.

Saponification:
Preparation of Soap
Preparation of inorganic compounds

Preparation of sodium carbonate and


determination of percentage purity and Classification and nomenclature
3. percentage yield.

Preparation of copper sulphate and determination


of percentage purity and percentage yield.

Organic qualitative analysis. Aliphatic hydro carbons


4.
Halogen derivatives of hydro carbon
& Analysis of organic compounds to determine :
5. a) elements present Aliphatic alcohol
b) functional group
c) melting point Aldehyde and ketones

6. Inorganic estimation
Esters
Estimation of calcium in given tablet
Oil analysis Ether
Determination of acid value of an oil & or fat.
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CHEMICAL LABORATORY ASSISTANT
7. Estimation of formaldehyde by iodometric Amines
method Aliphatic acid
8. Instrumental analysis Principles of potentiometric and conductometric
titrations
Potentiometric titration
Aromatic hydrocarbon & Urea
Conductometric titration

9. Determination of optical rotation of sugar


solution using polarimeter
Aromatic halogen derivatives
Determination percentage of elements by Aromatic acid & Alcohol.
electrolytic analyzer
10. Determine the pH of given solution by using pH pH & buffer solution
meter.

Determination of viscosity of given sample using


viscometer Viscosity

Determination of flash point of given sample


11. Water analysis
1.Hardness
2.Chloride Law of mass action
3.Total dissolved solid (TDS)
4. Alkalinity
12. Study of Micro scope ---
Study Of Staining Technique

Revision
13. Internal Assessment 03 days

NOTE: -

 More emphasis to be given on video/real-life pictures during theoretical classes. Some real-
life pictures/videos of related industry operations may be shown to the trainees to give a feel
of Industry and their future assignment.

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CHEMICAL LABORATORY ASSISTANT
9. SYLLABUS - CORE SKILLS
9.1 WORKSHOP CALCULATION SCIENCE & ENGINEERING DRAWING

Block – I
Sl. Workshop Calculation and Science EngineeringDrawing
No. (Duration: - 20 hrs.) (Duration : - 30 hrs.)
1. Units & Measurements- FPS, CGS, Engineering Drawing: Introduction and its
MKS/SI unit, unit of length, Mass and time. importance
Fundamentals and derived units Conversion Different types of standards used in engineering
of units and applied problems. drawing.
Drawing Instruments: their uses
Drawing board, T-Square, Drafter (Drafting M/c),
Set Squares,
Protractor, Drawing Instrument Box (Compass,
Dividers, Scale, Diagonal
- Scales etc.), Pencils of different Grades,
Drawing pins / Clips.
2. Material Science : properties -Physical & Lines :
Mechanical, Types -Ferrous & Non- types and applications in Drawing as per BIS SP:46-
Ferrous, difference between Ferrous and 2003
Non-Ferrous metals Drawing geometrical object using all types of lines.
Drawing of Geometrical Figures: Angle, Triangle,
Square, Rectangle and Circle.
Letters: - Lettering styles, Single stroke letters and
numbers as per IS standard. Lettering practice.
3. Mass .Weight and Density : Dimensioning- Types of dimension, elements of
Mass, Unit of Mass, Weight, difference dimensions, Methods of indicating Values,
between mass and weight, Density, unit of Arrangement, Alignment and indication of
density, dimensions.
Scales:-Types use and construction. Representative
factor of scale.
4. Speed and Velocity: Rest and motion, Method of presentation of Engineering Drawing
speed, velocity, difference between speed - Pictorial View
and velocity, acceleration, retardation. - Orthogonal View
Average Velocity, Acceleration & - - Isometric viewCircle and its elements.
Retardation. Related problems.
Circular Motion: Relation between circular
motion and Linear motion, Centrifugal
force, Centripetal force
5. Ratio & Proportion : Constructions: - Draw proportionate free
-
Simple calculation on related problems. hand sketches of plane figures. Sketch
Percentage: Introduction, Simple horizontal, vertical and inclined line by free
calculation. hand, Draw circles by free hand using square
and radial line method, Draw arcs and ellipse
by free hand
6. Work, Power and Energy: work, unit of Projections:
work, power, unit of power, Horse power of Concept of axes plane and quadrant.
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CHEMICAL LABORATORY ASSISTANT
engines, mechanical efficiency, energy, use Orthographic projections
of energy, potential and kinetic energy, Method of first angle and third angle projections
examples of potential energy and kinetic (definition and difference)
energy. Symbol of 1st angle and 3rd angle projection as per
Meaning of H.P., I.H.P., B.H.P., and F.H.P. IS specification.
and CC and Torque. - Free hand Drawing of Orthographic projection
from isometric/3D view of geometrical blocks

Block – II
Sl. Workshop Calculation and Science EngineeringDrawing
No. (Duration: - 20 hrs.) (Duration : - 30 hrs.)
1. Algebra: Screw :-
Addition, Subtraction, Multiplication, Division, Its Types and Sizes, Screw thread, their
Algebraic formula, Linear equations (with two standard forms as per BIS, external and internal
variables). thread.
2. Heat & Temperature: Rivets and Joints:-
Heat and temperature, their units, difference Prepare a drawing sheet on rivets nomenclature
between heat and temperature, boiling point, and Joints.
melting point, scale of temperature, relation
between different scale of temperature,
Thermometer, pyrometer, transmission of heat,
conduction, convection, radiation.
3. Mensuration: Area and perimeter of square, Free hand Sketches for simple pipe line with
rectangle, parallelogram, triangle, circle, semi general fittings.
circle, Volume of solids - cube, cuboid,
cylinder and Sphere.
Surface area of solids -cube, cuboid, cylinder
and Sphere.
Volume of cut-out solids: hollow cylinders,
frustum of cone, block section. Volume of
simple solid blocks.
4. Basic Electricity: Introduction, use of Reading of drawing. Simple exercises related
electricity, how electricity is produced, Types to missing lines, dimensions. How to make
of current_ AC, DC, their comparison, voltage, queries.
resistance, their units. Conductor, insulator,
Types of connections - series, parallel, electric
power, Horse power, energy, unit of electrical
energy. Concept of earthling.
5. Simple machines Transmission of power: - Simple exercises related to trade related
Transmission of power by belt, pulleys & gear symbols.
drive. Basic electrical and electronic symbols
Heat treatment process: - Heat treatment and
advantages. Annealing, Normalizing,
Hardening, Tempering.
6. Trigonometry: Free hand sketch of trade related
Trigonometrical ratios, measurement of angles. components / parts /cutting tool indicating
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CHEMICAL LABORATORY ASSISTANT
Trigonometric tables. angles.
Finding the value of unknown sides and angles
of a triangle by Trigonometrical method.
Finding height and distance by trigonometry.
Application of trigonometry in shop problems.
(viz. taper angle calculation).
Calculate the area of triangle by using
trigonometry and application of Pythagoras
theorem.
7. Concept of pressure - Definition:-Force,
Pressure, and their units, atmospheric pressure,
gauges used for measuring pressure, problems.
Introduction to pneumatics & hydraulics
systems
8. Simple exercises related to trade related Test Papers. Solution of NCVT test papers.

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CHEMICAL LABORATORY ASSISTANT
9.2 EMPLOYABILITY SKILLS

(DURATION: - 110 HRS.)

Block – I
(Duration – 55 hrs.)
1. English Literacy
Duration : 20 Hrs. Marks : 09
Pronunciation Accentuation (mode of pronunciation) on simple words, Diction
(use of word and speech)

Functional Grammar Transformation of sentences, Voice change, Change of tense,


Spellings.

Reading Reading and understanding simple sentences about self, work and
environment

Writing Construction of simple sentences Writing


simple English

Speaking / Spoken Speaking with preparation on self, on family, on friends/ classmates,


English on know, picture reading gain confidence through role-playing and
discussions on current happening job description, asking about
someone's job habitual actions. Cardinal (fundamental) numbers
ordinal numbers. Taking messages, passing messages on and filling in
message forms Greeting and introductions office hospitality, Resumes
or curriculum vita essential parts, letters of application reference to
previous communication.

2. I.T. Literacy
Duration : 20 Hrs. Marks : 09
Basics of Computer Introduction, Computer and its applications, Hardware and peripherals,
Switching on-Starting and shutting down of computer.

Computer Operating Basics of Operating System, WINDOWS, The user interface of


System Windows OS, Create, Copy, Move and delete Files and Folders, Use of
External memory like pen drive, CD, DVD etc, Use of Common
applications.

Word processing and Basic operating of Word Processing, Creating, opening and closing
Worksheet Documents, use of shortcuts, Creating and Editing of Text, Formatting
the Text, Insertion &creation of Tables. Printing document.
Basics of Excel worksheet, understanding basic commands, creating
simple worksheets, understanding sample worksheets, use of simple
formulas and functions, Printing of simple excel sheets.

Computer Networking Basic of computer Networks (using real life examples), Definitions of
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CHEMICAL LABORATORY ASSISTANT
and Internet Local Area Network (LAN), Wide Area Network (WAN), Internet,
Concept of Internet (Network of Networks),
Meaning of World Wide Web (WWW), Web Browser, Web Site, Web
page and Search Engines. Accessing the Internet using Web Browser,
Downloading and Printing Web Pages, Opening an email account and
use of email. Social media sites and its implication.
Information Security and antivirus tools, Do's and Don'ts in
Information Security, Awareness of IT - ACT, types of cyber crimes.

3. Communication Skills
Duration : 15 Hrs. Marks : 07
Introduction to Communication and its importance
Communication Skills Principles of Effective communication
Types of communication - verbal, non verbal, written, email, talking on
phone.
Non verbal communication -characteristics, components-Para-language
Body language
Barriers to communication and dealing with barriers.
Handling nervousness/ discomfort.

Listening Skills Listening-hearing and listening, effective listening, barriers to


effective listening guidelines for effective listening.
Triple- A Listening - Attitude, Attention & Adjustment.
Active Listening Skills.

Motivational Training Characteristics Essential to Achieving Success.


The Power of Positive Attitude.
Self awareness
Importance of Commitment
Ethics and Values
Ways to Motivate Oneself
Personal Goal setting and Employability Planning.

Manners, Etiquettes, Dress code for an interview


Do's & Don'ts for an interview.
Facing Interviews
Behavioral Skills Problem Solving
Confidence Building
Attitude

Block – II
Duration – 55 hrs.
4. Entrepreneurship Skills
Duration : 15 Hrs. Marks : 06
Concept of Entrepreneur - Entrepreneurship - Enterprises:-Conceptual issue
Entrepreneurship Entrepreneurship vs. management, Entrepreneurial motivation.
Performance & Record, Role & Function of entrepreneurs in relation to
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CHEMICAL LABORATORY ASSISTANT
the enterprise & relation to the economy, Source of business ideas,
Entrepreneurial opportunities, The process of setting up a business.

Project Preparation & Qualities of a good Entrepreneur, SWOT and Risk Analysis. Concept
Marketing analysis & application of PLC, Sales & distribution Management. Different
Between Small Scale & Large Scale Business, Market Survey,
Method of marketing, Publicity and advertisement, Marketing Mix.
Institutions Support Preparation of Project. Role of Various Schemes and Institutes for self-
employment i.e. DIC, SIDA, SISI, NSIC, SIDO, Idea for financing/
non financing support agencies to familiarizes with the Policies
/Programmes& procedure & the available scheme.

Investment Project formation, Feasibility, Legal formalities i.e., Shop Act,


Procurement Estimation & Costing, Investment procedure - Loan procurement -
Banking Processes.

5. Productivity
Duration : 10 Hrs. Marks : 05
Benefits Personal / Workman - Incentive, Production linked Bonus,
Improvement in living standard.

Affecting Factors Skills, Working Aids, Automation, Environment, Motivation - How


improves or slows down.

Comparison with Comparative productivity in developed countries (viz. Germany,


developed countries Japan and Australia) in selected industries e.g. Manufacturing, Steel,
Mining, Construction etc. Living standards of those countries, wages.

Personal Finance Banking processes, Handling ATM, KYC registration, safe cash
Management handling, Personal risk and Insurance.

6. Occupational Safety, Health and Environment Education


Duration : 15 Hrs. Marks : 06
Safety & Health Introduction to Occupational Safety and Health importance of safety
and health at workplace.

Occupational Hazards Basic Hazards, Chemical Hazards, Vibroacoustic Hazards, Mechanical


Hazards, Electrical Hazards, Thermal Hazards. Occupational health,
Occupational hygienic, Occupational Diseases/ Disorders & its
prevention.

Accident & safety Basic principles for protective equipment.


Accident Prevention techniques - control of accidents and safety
measures.

First Aid Care of injured & Sick at the workplaces, First-Aid & Transportation
of sick person.
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CHEMICAL LABORATORY ASSISTANT
Basic Provisions Idea of basic provision legislation of India.
safety, health, welfare under legislative of India.
Ecosystem Introduction to Environment. Relationship between Society and
Environment, Ecosystem and Factors causing imbalance.
Pollution Pollution and pollutants including liquid, gaseous, solid and hazardous
waste.
Energy Conservation Conservation of Energy, re-use and recycle.
Global warming Global warming, climate change and Ozone layer depletion.
Ground Water Hydrological cycle, ground and surface water, Conservation and
Harvesting of water.
Environment Right attitude towards environment, Maintenance of in -house
environment.
7. Labour Welfare Legislation
Duration : 05 Hrs. Marks : 03
Welfare Acts Benefits guaranteed under various acts- Factories Act, Apprenticeship
Act, Employees State Insurance Act (ESI), Payment Wages Act,
Employees Provident Fund Act, The Workmen's compensation Act.

8. Quality Tools
Duration : 10 Hrs. Marks : 05
Quality Consciousness Meaning of quality, Quality characteristic.

Quality Circles Definition, Advantage of small group activity, objectives of quality


Circle, Roles and function of Quality Circles in Organization,
Operation of Quality circle. Approaches to starting Quality Circles,
Steps for continuation Quality Circles.

Quality Management Idea of ISO 9000 and BIS systems and its importance in maintaining
System qualities.

House Keeping Purpose of House-keeping, Practice of good Housekeeping.

Quality Tools Basic quality tools with a few examples.

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CHEMICAL LABORATORY ASSISTANT

10. DETAILS OF COMPETENCIES (ON-JOBTRAINING)

BROAD LEARNING TO BE COVERED IN INDUSTRY FOR CHEMICAL LABORATORY


ASSISTANT TRADE:

1. ORIENTATION:-
 Knowledge about Plant – its raw materials, products, capacity of production etc.
 Study of the process with the help of a simple flow sheet under the guidance of the plant
in-charge / supervisors found of the plant.
 Writing report (diary) of day to day work.
 Familiarization with various types of testing and analysis etc.
2. SAFTEY:-
 Cause and prevention of accidents.
 Personnel safety and use of personnel protective equipments.
 House Keeping.
 Fire prevention and fire fighting.
 Carefully handling of hazardous chemicals.
 Carefully Handling of Glassware
 Behaviour based safety (BBS)

3. Record keeping and documentation

Note: The following analysis be carried for raw materials, intermediate products and finished
products etc. according to the facilities available in the industries. (Theory portion / topic,
SOP is to be covered before operating each of the laboratory equipments)

The competencies/ specific outcomes on completion of On-Job Training are detailed below: -

Block – I

1. Solution preparation and sampling balance, Equivalent weight , Molecular weight , Atomic
weight, Specific gravity , Normality, Acidity, Basicity, Concentration, Normal Solution,
Molar Solutions, Preparations of acid solutions, basic solutions, oxidizing - reducing agent,
solutions.
Preparation of solutions of different concentration and determination of its concentration and
percentage purity.

2. Complexometry solutions , preparations of indicators, sampling in solids, liquids and gases,


Standardizations of solutions

Preparation of Ethylene diamine tetra acetic acid (EDTA) solution & indicator and titration
with EDTA.

3. Metallurgical analysis
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CHEMICAL LABORATORY ASSISTANT
Atomic Absorption Spectrophotometry
Analysis of different sample (such as Cu, Fe, Mn. etc. ) on Atomic Absorption
Spectrophotometer
4. X-ray crystallography: determination of different size of crystal samples.
5. Flame Photometry:
Determination of Sodium (Na), Potassium (K), Calcium (Ca) in different industrial samples
by Flame photometer.
6. Sample testing on Electron Microscope. Ore analysis, carbon analysis, analysis of Pyrolusite
for determination of percentage manganese (Mn).
7. Different volumetric and gravimetric analytical methods used in metallurgical analysis in
cements
8. Analysis in Foundry
9. Analysis of Different alloys, brass, solder wire etc.
10. Gas Chromatography (GC):

o High Performance Separation of different sample mixture (Industrial products) on


gas chromatography.

o Identification of separated components and determination of quantity of each


separated components.
Liquid Chromatography (HPLC):

 Separation of different sample mixture (Industrial products).on High Performance


Liquid Chromatography (HPLC).
 Identification of separated components and determination of quantity of each
separated components.

Block – II

11. Thin Layer Chromatography (TLC):


Separation of different sample mixture on thin layer chromatography.

12. Gas Chromatography Mass Spectrometry (GC / MS) :


Identification of different sample by using GC/ MS
13. UV – Vis Spectroscopy :
Determination of percentage composition of different sample components
14. Fourier Transform Infrared Spectrophotometer (IR/FTIR Spectrophotometer):

Analysis of different samples (Industrial products )


Calibration by polystyrene film
Study of background spectra
Study of different solid samples &analysis of spectrum obtained

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CHEMICAL LABORATORY ASSISTANT
15. Water, sources of water, Different water treatment processes, demineralised (DM) water
,Industrial water ,potable water.
Perform the Different water samples available in industry and their sampling techniques.
H
Perform Analysis of each water sample for parameters such as P , alkalinity, Total Dissolved

Solids (TDS), conductivity, total, temporary & permanent hardness of any water sample. etc.

16. Explain Chemical Oxygen Demand (COD), Biochemical Oxygen Demand (BOD), Dissolved
Oxygen( D.O). Determination of COD, BOD, DO for different water sample /effluent.
17. Determine the mixed liquor suspended solids (MLSS), Total Dissolved Solids (TDS), Total
Suspended Solids (TSS), PH, Turbidity of given water sample.
Perform analysis for Some Minute Minerals like Magnesium (Mg), Potassium (K), Sodium
(Na), Arsenic (As), etc. Hard water , Soft water
18. Detect the acid value, iodine value, saponification value , flash point, pour point, cloud point,
Viscosity, refractive index, optical rotation, specific rotation of oils, fats and petroleum
products, etc. of different Industrial samples.
19. Detect the elements, functional group, Melting point, Boiling point , Technique of
purification, preparation of Compound derivatives
20. Prepare the organic compounds such as Acetanilide, Aspirin, Phenolphthalein, soap,
Glucosazone etc.
21. Microbiological analysis Culture, Collection, Sampling,
22. Detection, preparation of innocula, Media, Techniques of inoculation & staining
23. Operate and Handle the Handling equipments in microbiological lab. Centrifuge, pH-Meter,
incubator, Shaker
24. Explain the Sterilization, fermentation, formulation. Preparation of Solutions related with
microbiological lab.

Note:

1. Industry must ensure that above mentioned competencies are achieved by the trainees during their on
job training.

2. In addition to above competencies/ outcomes industry may impart additional training relevant to the
specific industry.

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(CHEMICAL LABORATORY ASSISTANT)
ANNEXURE – I

INFRASTRUCTURE FOR PROFESSIONAL SKILL & PROFESSIONAL


KNOWLEDGE

CHEMICAL LABORATORY ASSISTANT

LIST OF TOOLS AND EQUIPMENT for Basic Training (For 20 Apprentices)


A. TRAINEES TOOL KIT ( For each additional unit trainees tool kit Sl. 1-18 is required
additionally)

Sl. no. Name of the Tool &Equipments


Quantity
1. Erlenmeyer flasks 250 ml. Borosilicate 36 nos.
Glass

2. Erlenmeyer flasks 100 ml. Borosilicate 24 nos.


Glass

3. Burettes with Teflon stop cock -25 ml. 16 nos.


Borosilicate Glass

4. Burettes with Teflon stop cock -50 ml. 16 nos.


Borosilicate Glass

5. Pipettes 10 ml. Borosilicate Glass 36 nos.


(Volumetric Type)

6. Pipettes 25 ml. Borosilicate Glass 36 nos.


(Volumetric Type)

7. Pipettes measuring 0 to 5 ml. Borosilicate 24 nos.


Glass

8. Pipettes measuring 0 to 10 ml. Borosilicate 24 nos.


Glass

9. Pipettes measuring 0 to 1 ml. Borosilicate 6 nos.


Glass

10. Pipettes 1ml. (graduated) Borosilicate 12 nos.


Glass

11. Measuring cylinders 25 ml. Borosilicate 10 nos.

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(CHEMICAL LABORATORY ASSISTANT)
Glass

12. Measuring cylinders 50 ml. Borosilicate 24 nos.


Glass

13. Volumetric flask 100 ml. Borosilicate 24 nos.


Glass

14. Volumetric flask 250 ml. Borosilicate 24 nos.


Glass

15. Volumetric flask 500 ml. Borosilicate 24 nos.


Glass

16. Volumetric flask 1000 ml. Borosilicate 12 nos.


Glass

17. Weighing bottles polyethylene or glass 50 24 nos.


ml.

18. Weighing bottles polyethylene or glass 100 12 nos.


ml.

19. Funnels with regular & long stem 7 cm. 24 nos.


dia.

20. Funnels 4 cm. dia. Borosilicate Glass 24 nos.

21. Funnels Buchner different sizes 10 to 25 6 nos.


cm. dia.

22. Funnels separatory 250 ml. Borosilicate 12 nos.


Glass

23. Beakers 100 ml. Borosilicate Glass 48 nos.

24. Beakers 250 ml. Borosilicate Glass 48 nos.

25. Beakers 400 ml. Corning 48 nos.

26. Beakers 600 ml. Borosilicate Glass 24 nos.

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(CHEMICAL LABORATORY ASSISTANT)
27. Watch glasses 5 cm.dia. 24 nos.

28. Watch glasses 7.5 cm.dia. 48 nos.

29. Dishes evaporating 7.5 cm. dia. 24 nos.

30. Thermometers 0 to 110°C 24 nos.

31. Thermometers 0 to 250°C 12 nos.

32. Thermometers 0 to 350°C 12 nos.

33. Thermometers for drying oven 3 nos.

34. Boiling flasks with round bottom 250ml. 16 nos.

35. Boiling flasks with round bottom 500ml. 16 nos.


for each distilling flasks 50 ml., 100 ml.,
250 ml.

36. Filtering flasks 250 ml. 24 nos.

37. Filtering flasks 500 ml. 24 nos.

38. Condensers Liebig 30 mm. long 24 nos.


Borosilicate Glass

39. Gas generator (Kips) 500 ml. 5 nos.

40. Gas washing bottles (Dressler) 24 nos.

41. Crucibles porcelain 5 cm, dia, height 4 cm 60 nos.


indigenous

42. Test tube ( 160 mm x 15 mm.) 500 nos.

43. Tubes for centrifuge 500 nos.

35
(CHEMICAL LABORATORY ASSISTANT)
44. Bottles with droppers for indicator 16 nos.
solutions & semi-micro qualitative analysis
30 ml.

45. Bottles for solids 50 ml. Borosilicate Glass 24 nos.

46. Bottles for solids 100 ml. Borosilicate 24 nos.


Glass

47. Bottles for solutions 100 ml. Borosilicate 24 nos.


Glass

48. Bottles for solutions 250 ml. Borosilicate 24 nos.


Glass

49. Bottles for solutions 1000 ml. Borosilicate 12 nos.


Glass

50. Bottles for solutions 2000 ml. Borosilicate 12 nos.


Glass

51. LCD Multimedia projector 1 no.

52. Computer/Laptop (latest configuration) 1 no.


with licentiate operating software.

53. Printer (Printer, Scanner & Copier) with 1 no.


one extra cartridge

54 Desiccators vacuum 150mm Diameter 4 no


Borosilicate Glass

55. Tongs (forceps) nickel for crucibles & 16 no


weights size 8 inches

56. Tongs long for crucibles (muffle furnace) 4 no


size 15 inches

57 Spatulas nickel 8” 16 no

58 Test tube support for 10-12 test tubes 16 no

36
(CHEMICAL LABORATORY ASSISTANT)
59 Tripods 16 no

60 Asbestos wire gauage 36 no

61 Test tube holders 16 no

62 Burette stand with clamp & clamp holders 20 no

63 Triangles clay 36 no

64 Glass rods 5 kg

65 Petri Disc 6 no.

66 Slide for Microscope 20 no.

B : INSTRUMENTS & GENERAL SHOP OUTFIT

Digital balances of different makes 200 1 No


67
gram 0.001 mg
Digital Balance capacity 1Kg, accuracy 1 No
68
1gram
Various types of Viscometer ( Redwood, Any Two
69
Ostwald, Brooks field )
70 Shaker (Bottle, Flask etc.) 1 No
Mechanical board for testing triangle and 2 Set
71 parallelogram of forces including all
accessories.
Instrument for determining ‘g’ (simple 2 Set
72
pendulum).with stand
Thermometers
(a) 0 to 110 0C 12 no
73
(b) 0 to 250 0C 12 no
(c) 0 to 360 0C 12 no
74 Polarimeter Digital 1 set
75 Digital refractometer 1 no
76 Equipment to study Kirchoff’s Law 1 set
77 Resistance Box (50 ohms, 100 ohms) 2 no each

37
(CHEMICAL LABORATORY ASSISTANT)
(a) Rheostat 25 Ohms 1 no each
78 (b) Rheostat 100 Ohms

Ammeters with stands:


(a) 0 to 1 Amp (DC) 2 sets
79
(b) 0 to 3 Amp (DC) 2 sets

Voltmeter with stands:


(a) 0 to 1 Volt (DC) 2 sets
80
(b) 0 to 5 Volt (DC) 2 sets
(c) 0 to 10 Volt (DC) 2 sets
Mill voltmeter :
(a) 0 to 5 mV 2 sets
81
(b) 0 to 500 mV 2 sets

82 Digital Multi meter 1 no


83 DC Power supply 12 V, 2 A 2 no
84 Water baths (6 places)(Electrically heated) 1 no
85 Sand bath 1 no
86 pH meter Digital 1 no
87 Auto titrator 1 no
88 Conductivity meter 1 no
Magnetic stirrers (with heating plate) 2 2 no
89
liters capacity
90 Mortar, 100mm, porcelain with pestle 2 no
91 Heating plates (Electrical) 1000 watt 2 no
92 Melting point apparatus 1 no
93 Apparatus for determination of flash point 1 no
94 Bunsen’s burners 16 no
Steam generator (copper) for steam 4 no
95
distillation 2 liter capacity
96 Distilled water plant 4 liter /Hr 1 no
97 TDS Meter digital 1
98 Heating Mental 1,2 & 5 liter 1 set
99 COD Apparatus 1
100 BOD Apparatus 1
101 Incubator 1
Microscope 1
102

38
(CHEMICAL LABORATORY ASSISTANT)
103 Electro chemical equivalent 1
Note: All electrical equipment should be provided with extra 20 meter wire switches,
terminals for connection.
C : GENERAL MACHINERY INSTALLATIONS
104 Vacuum Pump With Trolley 1 no
o
105 Electric Drying oven (200 C) 1 no
o
106 Furnaces (Muffle oven)(1100 C) 1 no
107 Fire Extinguisher 1 no
108 Laboratory Centrifuge (Analytical) 1 no
Note: In case of basic training setup by the industry the tools, equipment and machinery
available in the industry may also be used for imparting basic training.

39
(CHEMICAL LABORATORY ASSISTANT)
INFRASTRUCTURE FOR WORKSHOP CALCULATION & SCIENCE AND
ENGINEERING DRAWING

TRADE: CHEMICAL LABORATORY ASSISTANT

LIST OF TOOLS& EQUIPMENTS FOR -20APPRENTICES

1) Space Norms : 45 Sq. m.(For Engineering Drawing)

2) Infrastructure:

A : TRAINEES TOOL KIT:-


Sl.
Name of the items Specification Quantity
No.
1. Draughtsman drawing instrument box 20+1 set
2. Set square celluloid 45⁰ (250 X 1.5 mm) 20+1 set
3. Set square celluloid 30⁰-60⁰ (250 X 1.5 mm) 20+1 set
4. Mini drafter 20+1 set
5. Drawing board (700mm x500 mm) IS: 1444 20+1 set

B : Furniture Required
Sl.
Name of the items Specification Quantity
No.
1 Drawing Board 20
2 Models : Solid & cut section as required
3 Drawing Table for trainees as required
4 Stool for trainees as required
5 Cupboard (big) 01
6 White Board (size: 8ft. x 4ft.) 01
7 Trainer’s Table 01
8 Trainer’s Chair 01

40
(CHEMICAL LABORATORY ASSISTANT)

TOOLS & EQUIPMENTS FOR EMPLOYABILITY SKILLS

Sl. No. Name of the Equipment Quantity


1. Computer (PC) with latest configurations and Internet connection with 10 Nos.
standard operating system and standard word processor and worksheet
software
2. UPS - 500VA 10 Nos.
3. Scanner cum Printer 1 No.
4. Computer Tables 10 Nos.
5. Computer Chairs 20 Nos.
6. LCD Projector 1 No.
7. White Board 1200mm x 900mm 1 No.
Note: - Above Tools & Equipments not required, if Computer LAB is available in the institute.

41
ANNEXURE-II
FORMAT FOR INTERNAL ASSESSMENT

Name & Address of the Assessor : Year of Enrollment :

Name & Address of ITI (Govt./Pvt.) : Date of Assessment :

Name & Address of the Industry : Assessment location: Industry / ITI

Trade Name : Semester: Duration of the Trade/course:

Learning Outcome:

Maximum Marks (Total 100 Marks) 15 5 10 5 10 10 5 10 15 15

assessment Marks
Quality in workmanship
Attendance/ Punctuality

Skills to handle tools &


Safety consciousness

Speed in doing work

Total internal
Workplace hygiene

Result (Y/N)
Economical use of
Manuals/ Written
Ability to follow

Application of
instructions

Knowledge
Sl. No

equipment

materials

VIVA
Father's/Mother’s
Candidate Name
Name

42

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