SOR-100 Solvent Racks Operating Instructions

SOR-100 Solvent Racks
Operating Instructions
Revision: 1.0
Date: April 2004
© 2004 Dionex
Doc.: Solvent_Rack_OI_E_V1.doc
SOR-100 Operating Instructions
Declaration of Conformity
Product: Solvent Racks
Type: SOR-100, SOR-100A-2,
SOR-100A-4, SOR-100A-6
Dionex GmbH herewith declares conformity of the above products with the respective
requirements of the following regulations:
• Low-Voltage Equipment Directive 73/23/EEC

changed by 93/68/EEC
• EMC Directive 89/336/EEC
changed by 91/263/EEC; 92/31/EEC; 93/68/EEC
The electrical safety of the products was evaluated based on the following standard:
• EN 61010-1: 1993
Safety requirements for electrical equipment for measurement, control and
laboratory use
Part 1: General Requirements
The Electromagnetic Compatibility (EMC) of the products was evaluated based on the
following standards:
• EN 50081-1: 1992:
Electromagnetic Compatibility (EMC) - Generic emissions standard
Part 1: Residential, commercial and light industry
• EN 50082-1: 1992:
Electromagnetic Compatibility (EMC) - Generic immunity standard
Part 1: Residential, commercial and light industry
• EN 61000-3-2: 1998
Electromagnetic Compatibility (EMC)
Part 3 / Section 2: Limits for harmonic current emissions
This declaration is issued for the manufacturer

Dionex GmbH
Dornierstrasse 4
D-82110 Germering
by the President, Dr. Peter Jochum.

March 3, 2004
Table of Contents
1 Introduction ....................................................................................................................... 1
1.1 How to Use This Manual ........................................................................................... 1
1.2 Unpacking .................................................................................................................. 2
1.3 Intended Use............................................................................................................... 2
1.4 Federal Communications Commission (FCC) Note .................................................. 3
2 Overview............................................................................................................................. 5
2.1 Unit Description ......................................................................................................... 5
2.2 Supported Configurations .......................................................................................... 5
2.3 Front Panel Display and Controls .............................................................................. 6
2.4 System Wellness ........................................................................................................ 6
2.5 Safety Precautions ...................................................................................................... 7
3 Installation.......................................................................................................................... 9
3.1 Location...................................................................................................................... 9
3.2 Electrical Connections ............................................................................................. 10
3.3 Rear Panel Connectors ............................................................................................. 10
3.3.1 Interfaces for Device Control............................................................................... 11
3.3.2 DC Input (Power) ................................................................................................. 11
3.3.3 15-Pin D-Sub Port ................................................................................................ 11
3.4 Fluid Connections .................................................................................................... 12
3.4.1 Connecting the Solvent Reservoirs to the Degasser ............................................ 12
3.4.2 Connecting the Degasser to the Pump.................................................................. 14
4 Operation.......................................................................................................................... 15
4.1 Stand-alone Operation.............................................................................................. 15
4.2 Operation with a Dionex P680 HPLC Pump ........................................................... 15
4.2.1 Operating the Degasser with the Pump's Firmware ............................................. 16
4.2.2 Operation with Chromeleon ................................................................................. 16
4.3 Operation after a Power Failure ............................................................................... 16
5 Troubleshooting............................................................................................................... 17
5.1 List of The Most Frequently Observed Error Messages .......................................... 17
5.2 Chromeleon Error Messages .................................................................................... 17
5.3 List of the Most Frequently Observed Problems ..................................................... 18
6 Maintenance ..................................................................................................................... 19
6.1 General Notes........................................................................................................... 19
6.2 Maintenance Intervals .............................................................................................. 20
6.3 Leak Sensor .............................................................................................................. 21
6.4 Shutting Down the Instrument ................................................................................. 22
7 Technical Information..................................................................................................... 23
i
8 Accessories........................................................................................................................ 25
9 Technical Appendix - Pinouts......................................................................................... 27
10 Index ............................................................................................................................ 29
ii
1 Introduction
1.1 How to Use This Manual
The layout of this manual is designed to provide quick reference to the sections of interest to
the user. However, in order to obtain a full understanding of the SOR-100 Solvent Racks, we
recommend that you review the manual thoroughly before beginning operation.
We assume that the person using this manual is sufficiently trained in the use of analytical
instrumentation and is aware of the potential hazards when using chemical solvents.
Almost all descriptions in the manual apply to all SOR-100 Solvent Racks. Therefore, the term
"the Solvent Rack" or "the rack" is used throughout the manual. If some detail applies to only one
rack type, the type is identified by name.
Please note: The device configuration may vary; therefore, not all descriptions
necessarily apply to your particular instrument.
At various points throughout the manual, messages of particular importance are indicated by
certain symbols:
Please note: Indicates general information intended to optimize the performance of the
instrument.
Important: Indicates that failure to take note of the accompanying information may
result in damage to the instrument.
Warning: Indicates that failure to take note of the accompanying information may
result in personal injury.
This manual is provided "as is." Every effort has been made to supply complete and accurate
information and all technical specifications have been developed with the utmost care. However,
Dionex assumes no responsibility and cannot be held liable for any errors, omissions, damage, or
loss that might result from any use of this manual or the information contained therein. We
appreciate your help in eliminating any errors that may appear in this document.
The information contained in this document is subject to change without notice.
Chromeleon® and Summit® HPLC System are registered trademarks of Dionex Corp. All other
trade or company names mentioned are subject to the copyright and the property and trademark
rights of the respective companies.
All rights reserved, including those for photomechanical reproduction and storage on electronic
media. No part of this publication may be copied or distributed, transmitted, transcribed, stored in
a retrieval system, or transmitted into any human or computer language, in any form or by any
means, electronic, mechanical, magnetic, manual, or otherwise, or disclosed to third parties
without the express written permission of Dionex Corp.
1
1.2 Unpacking
All electrical and mechanical components of the Solvent Rack are carefully tested before the
instrument is shipped from the factory. After unpacking, please inspect the rack for any signs
of mechanical damage that may have occurred during transit.
Please note: Immediately report any shipping damage to both, the incoming carrier and
Dionex. Shipping insurance will compensate for the damage only if
reported immediately.
Please note: Keep the original shipping container and the packing material. They will
provide excellent protection for the instrument in case of future transit.
Shipping the unit in any other packaging automatically voids the product
warranty.
To unpack the Solvent Rack:
• Place the shipping container on the floor. Remove the accessories.

• Grasp the Solvent Rack by the sides. Slowly and carefully, pull the rack out of the shipping
container and place it on a stable surface.
Important: To prevent the rack from falling, lift the unit itself from the sides. Do
not lift the unit by the packaging material or the front panel.
• Remove the foam inserts, and then remove the polythene packaging.
• Check off the contents of the accessory pack against the list (→ page 25).
Caution: When lifting or moving the Solvent Rack, lift only from the bottom or
sides of the unit. Lifting the Solvent Rack by the front panel may damage
the hinges.
1.3 Intended Use

The Solvent Racks are designed for use in analytical HPLC systems, especially with the
Dionex P680 HPLC pumps. They can be controlled by either the pump firmware or the
Chromeleon Chromatography Management System. The racks can be operated in stand-alone
mode, also.
Please note that the Solvent Racks may be operated only using the accessories shipped with the
unit (→ page 25) and within their technical specifications (→ page 23).
If there is any question regarding appropriate usage, contact Dionex before proceeding.
Dionex is not liable for any damage, material or otherwise, resulting from inappropriate or
improper use of the instrument.
2
1.4 Federal Communications Commission (FCC) Note

This equipment has been tested and found to comply with the limits for a Class A digital
device, pursuant to part 15 of the U.S. FCC Rules. These limits are designed to provide
reasonable protection against harmful interference when the equipment is operated in a
commercial environment. This equipment generates, uses, and can radiate radio frequency
energy and, if not installed and used in accordance with the instruction manual, may cause
harmful interference to radio communications. Operation of this equipment in a residential
area is likely to cause harmful interference, in which case the user will be required to correct
the interference at his expense.
3
4
2 Overview
2.1 Unit Description
The Solvent Racks are high-quality instruments designed for HPLC analysis as part of a
Dionex Summit HPLC System. They are primarily designed for use with the Dionex P680
HPLC pumps. The racks provide a secure location for installation of the solvent reservoirs
and, when mounted on top of the HPLC system, save valuable bench space. They are
available in various configurations (→ Supported Configurations) and can thus be used in
numerous laboratory environments.
All Solvent Racks include a reservoir tray, solvent reservoirs, and appropriate tubing. The
SOR-100, the only rack that does not contain a vacuum degasser, is intended for use as a solvent
organizer. In the other racks, an integrated analytical vacuum degasser (2-channel, 4-channel, or
6-channel) continuously degasses solvents via special polymer membranes that are permeable to
gas, but not to liquids. Degassing solvents guarantees reproducibility and reduces pulsation in the
connected pump.
All parts in the flow path are made of Teflon® AF, PEEK, or Tefzel® to provide optimum
resistance to the most commonly used solvents and buffer solutions.
2.2 Supported Configurations

For an overview of the currently available models, refer to the list below. If you have any
questions, do not hesitate to contact the Dionex Sales Department or your Dionex distributor.
Model Part No. Description

SOR-100 5030.9200 Solvent Rack without degasser
e.g., for P680A LPG-4 pumps
SOR-100A-2 5030.9210 Solvent Rack with 2-channel degasser (analytical)
e.g., for P680A ISO and P680A HPG-2 pumps
e.g., for P680A HPG-4 pumps
e.g., for P680A DGP-6 pumps
5
2.3 Front Panel Display and Controls
1 2 3
Fig. 1: Solvent Rack front panel
No. Front Panel LEDs Description

1 Power The LED is blue when the Solvent Rack power is on.
2 Vacuum The LED is green if the degasser is working properly.
The LED is red if the degasser vacuum is insufficient for proper degassing. In this
case, the Status LED is red, also.
3 Status The LED is green if the degasser and the leak sensor are working properly.
The LED is red if the leak sensor detected a leak.
The LED is red if the degasser vacuum is insufficient for proper degassing. In this
case, the Vaccum LED is red, also.
2.4 System Wellness

The Solvent Rack supports several System Wellness and reliability features that can help you
detect small problems before they turn into big ones.
If an error is found, an error message is displayed on the front panel of the connected P680 pump.
If the pump is controlled by Chromeleon, the error is logged in the Chromeleon Audit Trail.
Feature Description
Leak detection Reliable operation
(Status LED on the rack's front panel.)
Degasser vacuum level monitoring Reliable operation
(Vacuum and Status LEDs on the rack's front panel.)
6
2.5 Safety Precautions

Please observe the following general safety precautions when operating the instrument or
carrying out any maintenance work:
Warning: Keep in mind that the fluid components of the system may be filled with
toxic solvents. Before starting maintenance, rinse toxic solvents from the
instrument. Avoid inhaling any vapors. Always wear gloves and goggles.
Important: When lifting or moving the Solvent Rack, lift only from the bottom or
sides of the unit. The front panel of the rack tilts upward. Lifting the rack
by the front panel may damage the hinges.
Important: When operating the HPLC system,set the low presure limit for the pump.
This prevents damage resulting from leakage or from running the pump
dry.
Please note: Before interrupting operation for an extended period (i.e, several days),
observe the precautions in Shutting Down the Instrument (→ page 22).
7
8
3 Installation
3.1 Location
After unpacking the Solvent Rack, allow the rack to warm up for approximately 4 hours
before connecting it to the power supply. This delay allows any condensation that might have
occurred during shipping to evaporate. After 4 hours, check the Solvent Rack; if condensation
is still there, allow the instrument to continue to warm up until the condensation is completely
gone.
Install the instrument in the laboratory on a stable surface that is free of vibrations. Make sure that
the surface is resistant to solvents. Avoid locations with extreme changes in temperature (such as
direct sunlight or drafts) and high air humidity. Allow sufficient clearance behind the rack for
electrical connections and ventilation.
If the rack is part of a Summit HPLC system, we recommend that you stack the individual
modules as shown below. This arrangement optimizes the flow path and ensures a low dead
volume.
For all Solvent Racks with the

integrated degasser: You may
SOR-100 Solvent Rack connect drainage tubing here,
underneath the instrument.
P680 Pump
ASI-100 Autosampler
TCC-100 Column Compartment
PDA-100 Detector*
Fig. 2: Summit HPLC system with Solvent Rack

(* As an alternative, the Summit HPLC system may include a UVD 170U or UVD 340U Detector.)
9
Please note: If the Solvent Rack contains an integrated degasser, drainage tubing can
be connected at the bottom right to direct liquid leaks to the waste
(→ Fig. 2). To prevent damage to the rack, make sure that no part of the
tubing is placed higher than the connection port.
3.2 Electrical Connections

Connect the Solvent Rack to the mains, using either a Dionex P680 HPLC pump or an
external power supply unit (part no. 1510.0004) (→ page 25). Please note: The P680 HPLC
pump must have a Solvent Rack port on its rear panel. If the pump does not have this port, the
Solvent Rack cannot be connected to the pump.
The external power supply unit is a primary clocked standard power unit providing a "wide
range" input (auto-sensing). Thus, no adjustment is required to adapt the line voltage to the local
voltage requirements.
For more information about how to connect the Solvent Rack, refer to Operation (→ page 15).
3.3 Rear Panel Connectors
1 2 3
Fig. 3: Solvent Rack rear panel
No. Description
1 Exhaust air outlet
Optional: Connect tubing here to vent vapors leaving the degassing chambers to waste
(→Fig. 4, page 11).
2 DC Input (Power): If the Solvent Rack is not controlled by a P680 pump, connect an external power
supply unit (part no. 1510.0004) from here to the mains (→ section 3.3.2, page 11).
3 15-pin D-Sub port
Connects the Solvent Rack to the pump (→ section 3.3.3, page 11).
10
Fig. 4: Connect tubing here to vent any vapors leaving the degassing chambers to waste
3.3.1 Interfaces for Device Control
Important: To ensure trouble-free operation, only use the cables provided in the
accessories kit.
3.3.2 DC Input (Power)
To connect the Solvent Rack directly to the mains, connect the external power supply unit
(part no. 1510.0004). The external power unit is an optional part.
9 to 18 Volt DC
Fig. 5: DC Input
Please note: The external power unit is required only if you do not want the P680 pump
to control the Solvent Rack. Please note: It is only possible for a P680
pump to control the Solvent Rack if a Solvent Rack port is provided on the
pump's rear panel.
3.3.3 15-Pin D-Sub Port
Connect the Solvent Rack to the pump, using the appropriate cable from the accessories kit.
For more information about how to connect the rack to the pump, refer to Operation, page 15.
For information about the pinout for this 15-pin D-Sub connector, refer to the Technical
Appendix (→ page 27).
11
3.4 Fluid Connections

To access to the fluid connections in the Solvent Rack, tilt the front panel upward and pull the
tray with the degassing chambers forward. It is not necessary to lock the open panel in place.
Important: When lifting or moving the Solvent Rack, lift only from the bottom or
sides of the unit. The front panel tilts upward. Lifting the unit by the front
panel may damage the hinges.
Please note: Do not connect a Solvent Rack with analytical degasser to a semi-
preparative P680P HPG-2 pump.
3.4.1 Connecting the Solvent Reservoirs to the Degasser
All Solvent Racks are shipped with solvent reservoirs and appropriate tubing. The bottle caps
have file holes. Four of the holes are capped (white caps) and one is open. The solvent line is
installed in the open hole. A retaining guide holds the tubing in place.
How to connect the solvent lines to the solvent reservoir (→ Fig. 6):
• First, feed the solvent line through the retaining guide and then into the open hole in the
reservoir cap.
• Slide the filter frit (from the accessories kit of your P680 pump) onto the end of the line.
• Fill the solvent reservoir and then, place the complete assembly in the reservoir.
• Tighten the reservoir cap hand-tight, by holding the cap and turning the bottle.
Retaining guide
Filter frit
Fig. 6: Connecting the solvent lines to the reservoir
12
Important: Always install filter frits on the solvent lines. This prevents contaminants
from reaching the HPLC system.
Please note: When replacing a solvent line, remove the frit frist, then the solvent line
and then, the retaining guide.
Please note: Regularly check the suction frits for permeability. Especially when
working with aqueous solvents, algae and other microorganisms can grow
and be deposited on the filter frits. Therefore, replace the solvents at
regular intervals. Rinse the reservoirs thoroughly before refilling them.
Replace the suction frits as necessary.
• Connect the lines to the appropriate connection ports on the degassing module. Route the
solvent lines through the associated openings in the rack's cover. Remove the dummy fitting
from the degasser inlet and connect the solvent lines with the corresponding label (→ Fig. 7).
Route the solvent lines through these openings. A B C A B C

(left pump) (right pump)
Fig. 7: Connecting the solvent reservoir (here: SOR-100A-6)
Please note: Before connecting the solvent lines, make sure that the connectors are free
of contaminants. Even minute particles can allow air to enter the degasser,
and thus reduce the unit's effectiveness.
Please note: When replacing solvents, make sure that the solvents are miscible. Mix
immiscible solvents with an intermediate solvent to replace them step-by-
step.
13
3.4.2 Connecting the Degasser to the Pump
In the P680A ISO, P680A HPG-2, P680A HPG-4, and P680A DGP-6 pumps, the appropriate
solvent lines are connected at the factory and routed through an opening in the pump's top
cover (→ Fig. 8).
The pumps are shipped with

the appropriate tubing
connected and routed
through this opening.
Fig. 8: Opening in the pump's top cover
Remove the corresponding dummy fitting from the degaser outlet (→ Fig. 7) and connect the
solvent line with the corresponding label.
Please note: • On a P680A ISO or P680A HPG-2 pump, connect the solvent lines
directly to the working pump head.
• On a P680A DPG-6 pump, connect the solvent lines to the 3-channel
proportioning valve.
• On a P680A HPG-4 pump, connect the solvent lines to the 2/3-way
valves of the solvent selector.
For more information about tubing connections to these pumps, refer to
the Operating Instructions for the P680 HPLC Pumps.
14
4 Operation
4.1 Stand-alone Operation
Make sure that the installation site meets the facility requirements (→ page 9). Connect the
Solvent Rack to the mains, using the optional external power supply unit (part no.
1510.0004). Connect the external power supply to the DC Input port on the rack's rear panel
(→ Fig. 3, page 10) and to the power source. The degasser reaches the appropriate operating
vacuum after a short time. When the Vacuum and Status LEDs are green, the degasser is
ready for operation.
4.2 Operation with a Dionex P680 HPLC Pump
Please note: If you plan to have a P680 pump control the Solvent Rack degassser,
verify that the Degaser option on the pump's Hardware menu (a submenu
of the Configuration menu) is set to External (→ Operating Instructions
for the P680 HPLC Pumps). If the setting is not External, contact Dionex
Service before proceeding.
Make sure that the installation site meets the facility requirements (→ page 9) and then, follow
the steps below to connect the Solvent Rack to a Dionex P680 pump:
• For pumps with a Solvent Rack port on the rear panel

Connect the 15-pin D-Sub port (→ Fig. 3, page 10) on the rack's rear panel to the Solvent
Rack port on the pump, using the appropriate cable from the accessories kit. The Solvent
Rack is powered via the pump.
The degasser is ready for operation and can now be controlled by either the pump firmware
(→ section 4.2.1, page 16) or Chromeleon (→ section 4.2.2, page 16).
Please note: Turning off the pump, automatically turns off the degasser, too.
• For pumps without a Solvent Rack port on the rear panel

The Solvent Rack cannot be connected to these pumps. In this case, operate the degasser in
stand-alone mode as described in section 4.1.
15
4.2.1 Operating the Degasser with the Pump Firmware
If the pump is operated in stand-alone mode, follow the steps below to turn the degasser on or
off:
• On the pump's Main menu, select the Configuration menu. Use the cursor keys to select to
select the Options menu and confirm you’re your selection by pressing the ↵ (Enter) key.
• Set the Degasser option to Yes. If the setting is No, the degasser is turned off.
Please note: Dionex recommends always leaving the degasser on.
4.2.2 Operation with Chromeleon
If the pump is controlled by Chromeleon, follow the steps below to turn the degasser on and
off:
• Open a Chromeleon control panel.

• Select Command... on the Control menu to open the Commands dialog box. (You can also
open this dialog box, by pressing the F8 key.)
• Click the "+" character beside Pump to display the items underneath.
• Set the Degasser option to On to turn on the degasser.
Please note: Dionex recommends always leaving the degasser on.
For information about the commands and properties available for the P680 pumps, refer to the
Operating Instructions for the P680 Pumps or to the Chromeleon online Help.
4.3 Operation after a Power Failure

After a power failure, instruments operating in the stand-alone mode return to a reliable
condition; all functions in progress when the power loss occurred are aborted. For example,
the pump flow is stopped. As soon as the power returns, the instrument performs a self-test.
The test results appear on the front panel display of the pump.
However, if the HPLC system is controlled by Chromeleon, the program file (PGM File) can
include a command that automatically restarts operation as desired after a power failure. For
more details, refer to the Chromeleon online Help.
16
5 Troubleshooting
5.1 List of the Most Frequently Observed Error Messages
The following table contains a summary of the most frequently observed error messages, lists
possible causes, and suggests appropriate remedial actions.
Note: If the Solvent Rack is controlled by a P680 pump, any error messages
related to the rack will appear on the front panel display of the pump. To
clear an error message, press Esc. If several error messages appear, press
Esc repeatedly to clear them one by one.
Problem Cause Remedial action

Degasser malfunction. The vacuum level monitoring Turn the rack off and on again.
function of the Solvent Rack Ti do so, either turn the pump off
degasser has responded. and on again or turn the degasser
off and on again, using the
Degasser option on the pump's
Options menu (→ Operating
Instructions for the P680 HPLC
Pumps).
Contact Dionex Service if the
message appears again.
Solvent Rack leak detected. There is a leak in the system. Find and eliminate the leak
and dry the leak sensor
(→ section 6.3, page 21).
A fitting connection is loose. Tighten the fitting connection
and dry the leak sensor
(→ section 6.3, page 21).
Please note: For information about the error messages that might appear during
operation of your pump, refer to the Operating Instructions for the P680
HPLC Pumps. If a message that is not listed in the manual appears, please
note the exact wording of the message and contact Dionex Service.
5.2 Chromeleon Error Messages

If the Solvent Rack is operated with a P680 pump and controlled by Chromeleon, any error
messages referring to the degasser are logged in the Chromeleon Audit Trail.
For a list of all Chromeleon error messages, refer to the Chromeleon installation program
(= Server Configuration). Double-click the pump in the left window section and select the
Error Levels tab page in the dialog box. You can also open the dialog box by clicking the pump
on the left pane and then selecting the Properties on either the Edit menu or context menu.
17
5.3 List of the Most Frequently Observed Problems

The following table provides a summary of the most common operating problems, lists
probable causes, and suggests remedial actions:
Problem Probable Cause Remedial Action

No function The Solvent Rack is not Check the connection of the
connected properly to the mains. external power supply unit
and/or the connection to the
pump (→ section 4, page 15).
The degasser is turned off. Verify that the degasser is turned
on:
- If the pump is operated in
stand-alone mode:
→ section 4.2.1, page 16
- If the pump is controlled by
Chromeleon:
→ section 4.2.2, page 16
Poor degassing There is a leak in the system. Inspect the capillaries and
solvent lines for leakage; tighten
loose fitting connections.
The pump's flow rate is too high. Reduce the flow rate
Reproducible ghost peaks in The degasser channels are Rinse the degaser channels
the chromatogram. contaminated. → section 6.2, page 20
18
6 Maintenance
6.1 General Notes
The Dionex Solvent Racks are made of high-quality components and materials to minimize
maintenance requirements. The painted surfaces are relatively resistant to weak acids, alkali,
and organic solvents. Nevertheless, immediately wipe up all liquids spilled onto the rack
surface, using a lint-free cloth or paper. If surfaces are exposed for longer periods, these
liquids can cause damage!
The following sections describe all maintenance procedures that can be carried out by the user.
Dionex personnel should perform any additional servicing, as well as annual inspections to detect
contamination, excessive wear, etc. If unexpected problems occur, please contact Dionex
Service.
Warning: Keep in mind that the fluid components of the system may be filled with
toxic solvents. Before starting maintenance, rinse toxic solvents from the
instrument and put on protective clothing.
Important: Before you return any instrument to Dionex for repair, contact Dionex
Service or your local distributor. An RMA (Return Material
Authorization) number is required for the return in order to properly track
and account for your instrument. Always use the original packaging when
shipping the Solvent Rack. Shipping the rack in anything other than the
original packaging will void the warranty. Refer to the warranty statement
in the terms of sale for more information.
Important: Use original Dionex spare parts only. Dionex assumes no liability for
damage caused by repairs with third-party parts!
For instructions on shutting down the unit, refer to page 22.
19
6.2 Maintenance Intervals

To avoid contamination of the degasser:
• Prepare fresh solvents at regular intervals.

• Clean the solvent lines at regular intervals.
• Rinse the degasser channels at regular intervals:
This is especially important for the channel that degases the acqueous solvent (for reverse-
phase chromatography). Usually, it is sufficient to rinse all channels with organic solvent.
(Please use a fresh bottle.) When you use water and acetonitrile or methanol, it is usually
sufficient to rinse the degasser channels once a week. However, please adapt the rinsing
interval to the solvents in use. In persistent cases, e.g., reproducible ghost peaks in the
chromatogram, follow the steps below:
• Replace the column with a backpressure capillary.
• Rinse the degasser channels for 1 hour with 20% nitrid acid at the flow rate normally used
for your application.
• Rinse the degasser channels with HPLC-grade water until the pH value is neutral. (Use
fresh HPLC-grade water or a new bottle.)
• Rinse the degasser channel for two hours, using HPLC-grade acetonitrile (use a new bottle)
at the flow rate normally used for your application.
• Prepare fresh solvents for your application using new bottles, and connect them to the
degasser channels.
• Install new filters.
• Reinstall the column and equilibrate the system.
In addition, have a Dionex Service Representative check the instrument once a year for
contamination, excessive wear, etc.
20
6.3 Leak Sensor
Please note: Check the Solvent Rack for leaks at regular intervals and tighten leaking
all tubing and capillary connections.
Leak sensor
Fig. 9: Leak Sensor
When the leak sensor detects a leak, the red Status LED on the front panel lights and the error
message "Solvent Rack leak detected" is displayed on the front panel of the pump.
If a leak is detected, follow these steps:
• Inspect the degasser inlets and outlets and the connected solvent lines for leaks. Tighten
leaking connections.
• Put on appropriate protective clothing and dispose of any liquid in the tray. Using a lint-free
cloth or paper, dry the sensor as shown in Fig. 10.
Fig. 10: Drying the leak sensor
Please note: The red Status LED on the front panel will remain illuminated as long as
the leak sensor is exposed to moisture.
21
6.4 Shutting Down the Instrument

Please observe the following precautions before interrupting operation for more than one
week or before shipping the Solvent Rack:
Please note: Thoroughly rinse the degasser with alcohol after operation. (The alcohol
does not need to be removed afterward.)
Please note: For longer periods of inactivity and when using saliferous buffers (which
may result in salt crystallization in the gas separation membrane, thereby
impairing the degassing performance), rinse with de-ionized water,
followed by either methanol or 2-propanol.
22
7 Technical Information
Solvent bottle capacity: Up to six 1-liter solvent bottles or
up to three 2-liter solvent bottles
Degassing channels: None, 2, 4, or 6 analytical degassing channels, depending on the
model
Degasser membranes: Teflon AF
Channel volume: 670 µl
Max. flow rate per channel: 12 ml/min
Optimized flow rate per channel:* 3.6 ml/min
Pressure drop: 4.5 mmHg/ml/min
Control: Permanent status transfer
Controlled by a Dionex P680 HPLC pump
(with or without Chromeleon) or stand-alone operation
Communication: 15-pin D-Sub connector (through P680 HPLC pump)
PC connection: USB or Ethernet (RJ-45; 10 MBit)
Power supply: 15-pin D-Sub connector (through a P680 HPLC pump) or external
power supply unit (option)
Additional USB ports: Integrated USB hub with three type A USB ports for connection of
other Summit HPLC modules
Safety features: Leak detection, degasser vacuum level monitoring
User input/display: 3 LEDs (Power, Vacuum, and Status)
Wetted parts: Stainless steel, PCTFE, PTFE, PEEK
Environmental conditions: Range of use: Indoor use
Temperature: 10°C to 35°C (50°F to 95°F)
Air humidity: 40 to 85% rel. humidity, non-condensing
Overvoltage Category: II
Polution degree: 2
Power requirements: Max. 30 VA
Dimensions 10 x 40 x 31 cm (9.3 x 15.8 x 15.0 in.)
(h x w x d):
Weight: 2.8 kg (6.2 lb)
* Optimized flow range for isocratic or gradient mixture consisting of methanol and water (50:50)
Technical information: April 2004

All technical specifications are subject to change without notice.
23
24
8 Accessories
Accessories for the SOR-100 Solvent Racks are always maintained at the latest technical
standard. Therefore, part numbers are subject to alteration. However, updated parts will
always be compatible with the parts they replace.
The following accessories are shipped with the instruments:
Accessory SOR-100 SOR-100A-2 SOR-100A-4 SOR-100 A-6

Solvent Rack -P680connection cable -- 1 1 1
(Part no. 1310.2151)*
Dummy plugs 20 10 20 30
Solvent filter 1 1 1 1
(Part no. 2200.0011) (=10 filters) (= 10 filters) (= 10 filters) (= 10 filters)
Solvent Rack sealing plug 4 2 4 6
(Part no. 2261.0206)*
1-Liter solvent reservoir 2 1 2 6
2-Liter solvent reservoir 2 1 2 --
Solvent lines (analytical) -- 2 4 6
(Part no. 5030.2548)*
Set of A-D labels (5 labels each) 1 1 1 1
Operating Instructions, English 1 1 1 1
(Part no. 4820.3057)*
* The part numbers always refer to the packing unit. For more information, please contact your Dionex Sales Representative.
An external power supply unit (part no. 1510.0004) is available as an option for the following
Solvent Racks: SOR-100A-2, SOR-100A-4, and SOR-100A-6.
25
26
9 Technical Appendix - Pinouts
Pi Signal Name Signal Remarks

n Level
1 Occupied
2 Solvent Rack Error TTL_high with Solvent Rack errors
3 Jumper to pin 9
4 Solvent Rack Leak TTL high with Solvent Rack leaks
5 Occupied
6 V_Degas +24V_supply Supply for the Solvent Rack
7 GND_MOT Ground_supply Reference potential for VC_Degas
8 VCC +5V Voltage for logic devices
9 Jumper to pin 3
10 GND Reference potential for VCC
13 Occupied
14 V_Degas +24V_supply Supply for the Solvent Rack
15 GND_MOT Ground_supply Reference potential for VC_Degas
Fig. 11: 15-pin D-Sub port (female)
27
28
10 Index
A O
Accessories .........................................................26 Operating Instructions...........................................1
Operation ............................................................15
C after Power-Failure ........................................16
Control Elements..............................................6
Chromeleon
Display .............................................................6
Error Messages...............................................17
Safety Measures ...............................................7
Operation........................................................16
Stand-alone ....................................................15
Connections
Via P680 Pump ..............................................15
Device Control ...............................................11
With Chromeleon...........................................16
Electrical Connection .....................................10
With Pump Firmware.....................................16
Fluid ...............................................................12
Rear Panel ......................................................10
P
Connections (Rear Panel) ...................................11
15-pin D-Sub..................................................11 Pinouts ................................................................28
DC Input.........................................................11 Power ..................................................................11
Power .............................................................11 Power-Failure .....................................................16
Control Elements ..................................................6 Problems .............................................................18
D R
DC Input .............................................................11 Rear Panel (Connections) .............................10, 11
Degasser Channels (Rinse) .................................20 15-pin D-Sub..................................................11
Display ..................................................................6 DC Input.........................................................11
Power .............................................................11
E Rinsing Degasser Channels ................................20
Electrical Connection..........................................10
S
Error Messages ...................................................17
Safety Precautions.................................................7
F Scope of Supply....................................................2
Shut Down ..........................................................22
Fluid Connections ...............................................12
Solvent Rack
Degasser .........................................................12
15-pin D-Sub..................................................11
Pump ..............................................................14
Configurations..................................................5
Solvent Supply .........................................12, 14
Solvent Supply..............................................12, 14
I Spare Parts ..........................................................26
Specification .......................................................24
Installation Stand-alone Operation ........................................15
Connections (Rear Panel)...............................10 System Wellness ...................................................6
Electrical Connection .....................................10
Fluid Connections ..........................................12 T
Location ...........................................................9
Troubleshooting..................................................17
Intended Use .........................................................2
Chromeleon Error Messages ..........................17
L Error Messages...............................................17
Most Frequently Problems .............................18
Leak Sensor.........................................................21
U
M
Unit Description....................................................5
Maintenance Unpacking.............................................................2
General Notes.................................................19 User Information...................................................3
Leak Sensor....................................................21
Maintenance Intervals ....................................20 W
Rinsing Degasser Channels............................20
Wellness................................................................6
Shut Down......................................................22
Maintenance Intervals .........................................20
29
30

SOR-100 Solvent Racks Operating Instructions

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SOR-100 Solvent Racks

• Low-Voltage Equipment Directive 73/23/EEC

This declaration is issued for the manufacturer

by the President, Dr. Peter Jochum.

9 Technical Appendix - Pinouts......................................................................................... 27

The information contained in this document is subject to change without notice.

To unpack the Solvent Rack:

• Place the shipping container on the floor. Remove the accessories.

1.3 Intended Use

1.4 Federal Communications Commission (FCC) Note

2.2 Supported Configurations

Model Part No. Description

2.3 Front Panel Display and Controls

Fig. 1: Solvent Rack front panel

No. Front Panel LEDs Description

2.4 System Wellness

2.5 Safety Precautions

For all Solvent Racks with the

TCC-100 Column Compartment

Fig. 2: Summit HPLC system with Solvent Rack

3.2 Electrical Connections

3.3 Rear Panel Connectors

3.3.1 Interfaces for Device Control

3.3.2 DC Input (Power)

3.3.3 15-Pin D-Sub Port

3.4 Fluid Connections

3.4.1 Connecting the Solvent Reservoirs to the Degasser

Fig. 6: Connecting the solvent lines to the reservoir

Route the solvent lines through these openings. A B C A B C

Fig. 7: Connecting the solvent reservoir (here: SOR-100A-6)

3.4.2 Connecting the Degasser to the Pump

The pumps are shipped with

Fig. 8: Opening in the pump's top cover

4.2 Operation with a Dionex P680 HPLC Pump

• For pumps with a Solvent Rack port on the rear panel

• For pumps without a Solvent Rack port on the rear panel

4.2.1 Operating the Degasser with the Pump Firmware

Please note: Dionex recommends always leaving the degasser on.

4.2.2 Operation with Chromeleon

• Open a Chromeleon control panel.

Please note: Dionex recommends always leaving the degasser on.

4.3 Operation after a Power Failure

Problem Cause Remedial action

5.2 Chromeleon Error Messages

5.3 List of the Most Frequently Observed Problems

Problem Probable Cause Remedial Action

6.2 Maintenance Intervals

• Prepare fresh solvents at regular intervals.

6.3 Leak Sensor

If a leak is detected, follow these steps:

Fig. 10: Drying the leak sensor

6.4 Shutting Down the Instrument

Technical information: April 2004

The following accessories are shipped with the instruments:

Accessory SOR-100 SOR-100A-2 SOR-100A-4 SOR-100 A-6

9 Technical Appendix - Pinouts

Pi Signal Name Signal Remarks

2 Solvent Rack Error TTL_high with Solvent Rack errors

4 Solvent Rack Leak TTL high with Solvent Rack leaks

6 V_Degas +24V_supply Supply for the Solvent Rack