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    Lead Nitrate Final

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    sonicumin

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    © All Rights Reserved
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    Lead Nitrate Final

    Uploaded by

    sonicumin
    20 views2 pages

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    20 views2 pages

    Lead Nitrate Final

    Uploaded by

    sonicumin

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    © All Rights Reserved
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    ANALYSIS OF SIMPLE SALT

    S. No. EXPERIMENT OBSERVATION Inference


    IDENTIFICATION OF ACID
    RADICAL
    1. Colour of the salt colourless Absence of copper ,
    nickel, ferric,
    manganese salts
    2. Smell of the salt No characteristic smell Absence of
    ammonium or acetate
    salt
    3. Action of heat- Take a pinch of Decrepitation May be presence of
    salt and heat it in a dry test nitrate of lead or
    tube. barium
    4. Flame test- Take a pinch of salt No characteristic flame Absence of copper ,
    and make a paste with few barium, strontium,
    drops of con. HCl and introduce calcium salts
    it in the luminous part of the
    flame.
    5. Ash test- Take a pinch of salt No coloured ash Absence of zinc Zn2+,
    and add few drops of cobalt aluminium Al3+,
    nitrate solution. Dip a filter magnesium Mg2+
    paper and burn it. Look into the
    colour of the ash.

    DRY TESTS
    6. Dil. HCl test- To a pinch of salt No characteristic change Absence of carbonate
    add dil HCl sulphide, sulphide.
    7. Conc H2SO4 test- To a pinch of No characteristic Absence of chloride,
    salt, add con sulphuric acid and observation nitrate, bromide and
    warm acetate
    8 Chromyl chloride test- To a No reddish orange vapours Absence of chloride.
    pinch of salt add a pinch of are evolved.
    K2Cr2O7 and con H2SO4 and heat.
    Pass the fumes into a test tube
    containing NaOH and add acetic
    acid and lead acetate solution
    9 MnO2 test- To a pinch of salt add No characteristic fumes are Absence of chloride,
    half a pinch of MnO 2 and con observed bromide, iodide.
    H2SO4 and heat.
    10 Cu turnings test- To a pinch of Brown gas is evolved Presence of Nitrate.
    salt, add Cu turnings and conc.
    H2SO4 and heat. Pass the fumes
    into a solution of FeSO 4 solution
    11 NaOH test- To a pinch of salt, No pungent smelling gas Absence of
    add sodium hydroxide and heat ammonium
    12 Ferric chloride test- To a pinch No red precipitate Absence of acetate
    of salt add 1 ml of ferric chloride
    solution. Heat
    ANALYSIS OF SIMPLE SALT

    13 Ester test- To a pinch of salt add No fruity smelling liquid Absence of acetate
    few ml of ethyl alcohol and con
    H2SO4 and heat.

    IDENTIFICATION OF ACID RADICAL


    Preparation of Sodium carbonate extract: To a part of salt add two parts of sodium carbonate and
    10 ml of distilled water. Boil the contents, cool and filter. The filtrate is called as sodium carbonate
    extract.
    Ammonium molybdate test: To a No canary yellow precipitate Absence of
    part of the extract ,add a few drops phosphate PO43 -
    of Conc.HNO3 and boil. Then add
    ammonium molybdate solution.

    CONFIRMATORTY TEST FOR ACID


    RADICAL.

    Brown ring test: To a part of the A brown ring is formed at the Presence of
    extract, add dil H2SO4 till the junction of two liquids. nitrate,NO3- is
    effervescence ceases and then add confirmed
    freshly prepared FeSO 4 solution
    and con H2SO4 to the sides of the
    test tube.

    THE ACID RADICAL IS NITRATE

    IDENTIFICATION OF BASIC RADICAL


    PREPARATION OF ORIGINAL SALT SOLUTION:
    A small amount of salt is dissolved in 5 mL of distilled water.
    Group Analysis
    1 To the salt concentrated solution of No characteristic change Absence of group 0 –
    sodium hydroxide is add and ammonium ,NH4+
    warmed. A glass rod dipped in dil
    HCl is shown near the mouth of the
    test tube.
    2. To the OS add dil. HCl White precipitate of PbCl2 is Presence of group I –
    obtained. lead Pb2+

    CONFIRMATORY TEST FOR BASIC RADICAL:


    1. To the salt solution add potassium Yellow precipitate is obtained Presence of lead
    iodide. which dissolves on heating radical, Pb2+ is
    and reappears as golden confirmed.
    spangles on cooling.

    RESULT:
    THE ACID RADICAL IS NITRATE
    THE BASIC RADICAL IS LEAD
    THE GIVEN SIMPLE SALT IS LEAD NITRATE.

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