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    Strontium Nitrate FINAL

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    Meghana

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    © All Rights Reserved
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    Strontium Nitrate FINAL

    Uploaded by

    Meghana
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    Strontium Nitrate FINAL

    Uploaded by

    Meghana

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    © All Rights Reserved
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    ANALYSIS OF SIMPLE SALT

    S. EXPERIMENT OBSERVATION INFERENCE


    No.
    IDENTIFICATION OF ACID RADICAL:
    1. Colour of the salt colourless Absence of copper ,
    nickel, ferric,
    manganese salt.
    2. Smell of the salt No characteristic smell Absence of
    ammonium or acetate
    salt
    3. Action of heat- Take a pinch of salt Decrepitation May be presence of
    and heat it in a dry test tube. nitrate of lead or
    barium
    4. Flame test- Take a pinch of salt and Crimson red flame May be strontium salt
    make a paste with few drops of
    con.HCl and introduce it in the
    luminous part of the flame.

    5. Ash test- Take a pinch of salt and No coloured ash Absence of zinc Zn2+,
    add few drops of cobalt nitrate aluminium Al3+,
    solution. Dip a filter paper and magnesium Mg2+
    burn it. Look into the colour of the
    ash.
    DRY TESTS
    6. Dil. HCl test- To a pinch of salt add No characteristic change Absence of carbonate
    dil HCl sulphide, sulphide.
    7. Con H2SO4 test- To a pinch of salt, No characteristic Absence of chloride,
    add conc sulphuric acid and warm observation nitrate, bromide and
    acetate
    8 Chromyl chloride test- To a pinch No reddish orange vapours Absence of chloride.
    of salt add a pinch of K2Cr2O7 and are evolved.
    con H2SO4 and heat. Pass the fumes
    into a test tube containing NaOH
    and add acetic acid and lead
    acetate solution
    9 Cu turnings test- To a pinch of salt, Brown gas is evolved Presence of Nitrate.
    add Cu turnings and conc. H 2SO4
    and heat. Pass the fumes into a
    solution of FeSO 4 solution
    10 MnO2 test- To a pinch of salt add No characteristic fumes are Absence of chloride,
    half a pinch of MnO 2 and conc observed bromide, iodide salt
    H2SO4 and heat
    11 NaOH test- To a pinch of salt, add No pungent smelling gas Absence of
    sodium hydroxide and heat ammonium,NH4+
    12 Ferric chloride test- To a pinch of No red ppt Absence of acetate
    salt add 1 ml of ferric chloride
    solution. Heat
    ANALYSIS OF SIMPLE SALT

    13 Ester test- To a pinch of salt add No fruity smelling liquid Absence of acetate
    few ml of ethyl alcohol and conc
    H2SO4 and heat.

    Preparation of Sodium carbonate extract: To a part of salt add two parts of sodium carbonate and
    10 ml of distilled water. Boil the contents, cool and filter. The filtrate is called as sodium carbonate
    extract.
    Ammonium molybdate Absence of
    test: To a part of the extract Phosphate.
    ,add a few drops of No canary yellow
    Conc.HNO3 and boil. Then PO43-
    precipitate
    add ammonium molybdate
    solution.

    CONFIRMATORTY TEST FOR ACID


    RADICAL.

    1. Brown ring test: To a part of A brown ring is formed at the Presence of nitrate is
    the extract, add dil H2SO4 till the junction of two liquids. confirmed
    effervescence ceases and then add
    freshly prepared FeSO 4 solution
    and conc H2SO4 to the sides of the
    test tube.

    THE ACID RADICAL IS NITRATE

    IDENTIFICATION OF BASIC RADICAL


    PREPARATION OF ORIGINAL SALT SOLUTION:
    A small amount of salt is dissolved in 5 mL of distilled water.
    Group Analysis
    1 To the salt con solution of sodium No characteristic change Absence of group 0 –
    hydroxide is add and warmed. A ammonium,NH4+
    glass rod dipped in dil HCl is shown
    near the mouth of the test tube.
    2. To the OS add dil. HCl No characteristic change Absence of group I –
    lead,Pb2+
    3 To the OS, add dil.HCl and Yellow No characteristic change Absence of group 1 –
    ammonium sulphide Cu2+
    4 To the OS, add NH4Cl and NH4OH No characteristic change Absence of group III –
    Fe3+ and Al3+
    5 To the OS, add NH4Cl and NH4OH No characteristic change Absence of group IV
    and Yellow ammonium sulphide radicals- Co2+,Ni2+,Zn2+
    6 To the OS , add NH4Cl and NH4OH White precipitate is obtained Presence of group V
    and (NH4)2CO3 Ba2+ , Sr2+ , Ca2+

    CONFIRMATORY TEST FOR BASIC RADICAL:


    1. Dissolve the white precipitate White precipitate of SrSO 4 js Strontium radical,Sr2+
    obtained in hot dilute acetic acid obtained. is confirmed.
    and add (NH4)2SO4 solution.
    ANALYSIS OF SIMPLE SALT

    RESULT:
    THE ACID RADICAL IS NITRATE
    THE BASIC RADICALIS IS STRONTIUM
    THE GIVEN SIMPLE SALT IS STRONTIUM NITRATE.

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