V30 KF installation manual
V30 KF installation manual
V30 KF installation manual
Table of contents
1 Introduction 5
2 Measures for your protection 6
3 Standard equipment 7
4 The titrator 10
4.1 Titrator configuration 10
4.2 Titrator rear panel connections 11
4.3 Openings on the titration beaker 11
5 Installation (components) 13
5.1 Connecting the power supply 13
5.2 Titration stand 14
5.2.1 Installing the titration stand 14
5.2.2 Installing the solvent bottle 15
5.2.3 Installing the waste bottle 16
5.2.4 Connecting the measuring electrode 17
5.3 Inserting a burette 17
5.4 Internal magnetic stirrer 17
5.5 Stromboli oven sample changer 18
6 Optional accessories 19
7 Technical data 24
7.1 Titrator 24
7.2 Supported devices (periphery) 27
8 Service and maintenance 29
8.1 Cleaning 29
8.2 Transporting the titrator 29
9 Disposal 30
10 Declaration of system validation 31
11 Product life cycle model 32
12 Declaration of conformity 33
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Introduction
1 Introduction
Simple and compact
The instruments in METTLER TOLEDO's Titration Compact Line are modern, compact titrators for use in a
wide variety of application areas. They can be used, for example, in quality control as well as in
research and development and satisfy the most demanding of requirements.
The titrators in the Titration Compact Line perfectly combine simple, easy-to-understand operation with
an extremely high level of precision and outstanding reliability. Thanks to automatic titrant recognition
(Plug & Play burettes), the titrator independently identifies which titrant is required without intervention
from the operator. Settings no longer need to be adjusted manually, even when connecting a printer or a
Stromboli oven sample changer.
Titration Compact instruments can either be controlled by touchscreen or by using LabX PC software. The
large color touchscreen allows intuitive control by the user and flexibility in its adjustment options. All
functions can be activated directly from the home screen via shortcuts which can be freely created, mak
ing everyday use extremely easier. Controlling the titrator by touchscreen and all adjustable parameters
are described separately and in detail in the operating instructions.
This installation information explains all the steps necessary for installing and commissioning your
device. The "Quick Guide" will then guide you through the first titration process using a practical exam
ple. If you have any additional questions, METTLER TOLEDO is always available to assist you.
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Measures for your protection
Risk of explosion
● Always test the titration vessel for firm seating in the titration head. If it falls off,
you could injure yourself if working with toxic titrants and solvents or strong
acids or bases.
Risk of corrosion ● When using chemicals and solvents, comply with the instructions of the pro
ducer and the general lab safety rules!
All Karl Fischer reagents are readily flammable and toxic.
● In the case of skin contact, immediately wash off with copious amounts of
water!
● If eye contact occurs, rinse intensively with copious amounts of water and
consult a physician!
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Standard equipment
3 Standard equipment
All parts are specified with their ordering code and quantity in cases where more than one part is includ
ed. When ordering, some parts are only available in a minimum order quantity. In such cases, the corre
sponding minimum order quantity is quoted. The standard equipment and optional accessories are listed
in the appropriate operating instructions.
Description Order number
O-ring 51190366
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Standard equipment
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Standard equipment
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The titrator
4 The titrator
Part Description
A Titrant bottle drying tube
B Solvent bottle drying tube
C Waste bottle drying tube
D Solvent manager
E Waste bottle
F Solvent bottle
G Titration arm
H Titration beaker
I Internal magnetic stirrer
J On/Off button
K Indicator light (LED)
L Touchscreen
M Burette drive
n Burette arrestment knob
o Burette 5 mL
p Drying tube for the titration beaker
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The titrator
Part Description
Q Double platinum pin electrode
R Titrant bottle
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The titrator
Part Connection
A Solvent bottle dispensing tube
B Burette dispensing tube
C Measuring electrode
D Stopper
E Drying tube silicone tube
F Waste bottle extraction tube
G Three hole adapter
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Installation (components)
5 Installation (components)
Installation for all titrator types is described in this chapter. Standard equipment for the various types of
titrators varies and also depends on the optional accessories. For this reason, installation steps may
vary.
a) Connect the power supply unit to the "POWER SUPPLY" socket on the rear of the titrator and to the
mains supply.
b) Secure the connection at the titrator by screwing the plug connector firmly into place.
The power supply is suitable for all supply voltages ranging from 100–240 VAC ±10% and 50–60 Hz.
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Installation (components)
Part Description
a Silicone tube (133 mm)
B Threaded ring
C Lid
D Connecting piece
E NS 7.5 stopper
F Three hole adapter
G O-ring
H Titration vessel
I Lid
J Fastening screw
K Drying tube
L Groove in the titration arm
M Titration arm
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Installation (components)
Part Description
A Drying tube
B Threaded sleeve
C Screw top
D Flat seal
E Dispensing tube
F Adjusting sleeve
G Teflon seal
Check all drying tubes and closing points once again for firm seating in order to ensure that the system
is leaktight.
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Installation (components)
Part Description
A Draining tube
B Silicone tube (170 mm)
C Threaded sleeve
D Drying tube
E Solvent Manager
F Connecting cable
G Silicone tube (850 mm)
H Flat seal
I Adjusting sleeve
J Teflon seal
K Adapter for immediate draining
● Do not use the adapter for immediate draining in connection with samples
which cannot be fully dissolved. Risk of blockage.
● Do not use the adapter for immediate draining in connection with a
homogeniser. This could destroy the adapter.
● Check all drying tubes and closing points once again for firm seating in order to ensure that the sys
tem is leaktight.
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Installation (components)
a) Place the measuring electrode into the appropriate opening of the cell
b) Using the triaxial cable, connect the measuring electrode to the "SENSOR" socket on the rear of the
titrator.
When rinsing burettes and tubes, place the tips of dispensing tubes into a waste container.
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Installation (components)
a) Switch off the titrator and the Stromboli oven sample changer.
b) Using the cable provided, connect the "TTL/IO" socket of the oven sample changer to the "TTL-I/O"
socket on the rear of the titrator.
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Optional accessories
6 Optional accessories
All parts are specified with their ordering code and quantity in cases where more than one part is includ
ed. When ordering, some parts are only available in a minimum order quantity. In such cases, the corre
sponding minimum order quantity is quoted. The standard equipment and optional accessories are listed
in the appropriate operating instructions.
O-ring 51190366
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Optional accessories
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Optional accessories
Visco-Spoon™ 51107668
Injection needle
80 x 0.8 mm for 1 ml injections (100 pcs) 71484
80 x 1.2 mm for 10 ml injections) (12 pcs) 71483
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Optional accessories
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Optional accessories
Installation information
- English 51710611
- German 51710612
- French 51710613
- Spanish 51710614
- Italian 51710615
- Chinese 51710616
- Russian 51710617
Quick guide
- English 51710604
- German 51710605
- French 51710606
- Spanish 51710607
- Italian 51710608
- Chinese 51710609
- Russian 51710610
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Technical data
7 Technical data
7.1 Titrator
Power supply Input voltage 100–240 VAC ±10 %
Input frequency 50–60 Hz
Power consumption 30 VA
Primary connection socket 3 pin, IEC C14
Connected loads 24 V AC, 1.0 A
Secondary connection plug 2 pin, DC plug
CPU Processor XScale
SDRAM 64 MB
Flash memory 256 MB (industrial CF card)
Dimensions Width 210 mm
Depth 333 mm
Height 308 mm (with titration stand)
320 mm (ready-to-operate
device)
weight 4.2 kg
Materials Titrator housing Crastin® PBT
Cover sheet PET
Protective cover Copolymer
Chassis Stainless steel
Titration stand Crastin® PBT
Lid (titration beaker) Polypropylene
Threaded ring Polypropylene
Three hole adapter Polypropylene
Dispensing tube / extraction tube FEP
Air tubes Silicone
O-ring (screw top) EPDM
O-ring (threaded ring) FEP / silicone
Sealing ring (bottle) PTFE / silicone
Seal (dispensing tube / extraction PTFE
tube)
Connecting piece Polypropylene
Ambient conditions Ambient temperature +5 °C – 40 °C
Relative humidity Max. 80 % (non-condensing) at
31 °C, linear fall to 50 % at 40
°C
Use In interior spaces
Overvoltage category II
Pollution degree 2
COM Socket 9-pin male D-sub
Configuration Full-duplex
Baud rate 1200…19200
Handshake X-On / X-Off
Galvanic isolation No
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Technical data
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Technical data
Power Management
The devices have a power management system which prevents the titrator from switching off unexpected
ly in the event of a power overload. Tasks which would cause a power overload, because a number of
pumps, stirrers and burette drives are already in use, cannot be started at all. A notification brings the
start attempt to the attention of the user. It is advisable, if possible, to connect pumps and stirrers directly
to sample changers or other devices which have their own power supply, such as a TBox, instead of to
the titrator itself.
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Technical data
3 Stirrer +
1 Stirrer -
4 Pump +
5 Pump -
2 Pump 2 +
5 Pump 2 -
Balances
Balances can connect to the COM interface of the titrator. METTLER TOLEDO balances must be equipped
with an RS-232 interface or an appropriate adapter. For a list of connection cables, see Optional acces
sories.
Manufacturer Type RS LocalCAN Note
METTLER TOLEDO AB / PB • • COM interfaces
AB-S / PB-S • COM interfaces
AG / PG / • COM interfaces
PR
AT / MT / • COM interfaces
UMT
AX / MX / • - COM interfaces
UMX
PG-S • - COM interfaces
XP • - COM interfaces
XS • - COM interfaces
Sartorius Various • COM interfaces
• Standard - Option
Printer
Printers can be connected to the USB1 or USB2 interface of the titrator. PCL-compatible printers from var
ious manufacturers are supported. The METTLER TOLEDO USB-P25 is a robust and easy-to-operate
matrix printer which prints onto standard quality paper. A current list of supported printers can be found
on the Internet at: http://www.mt.com/titration-printers.
Manufacturer Type Note
Various Generic PCL printers Connection via USB1 or USB2
METTLER TOLEDO USB-P25 Connection via USB1 or USB2
A standard USB hub can be used if more than two devices are to be connected to the USB connections of
the titrator.
Sample changer
Barcode reader
Sample data can be read in via an appropriate barcode. The barcode reader can also be used to enter
text in open input fields. Barcode readers can be connected to the USB1 or USB2 interface of the titrator.
A standard USB hub can be used if more than two devices are to be connected to the USB connections of
the titrator.
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Technical data
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Service and maintenance
8.1 Cleaning
● Clean the housing of the titrator using a cloth moistened with alcohol.
● The titration stand can be fully dismantled in order to clean it.
● Empty the titration beaker and remove it from the titration stand.
● Remove all burettes and tube connections.
When sending or transporting the titrator over long distances, please use all of the original packaging.
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Disposal
9 Disposal
In compliance with European Directive 2002/96/EC on Waste Electrical and Elec
tronic Equipment (WEEE), this device must not be disposed of together with
domestic waste. The same principle applies to countries outside the EU, in accor
dance with their national regulations.
Please dispose of this product in accordance with local regulations, in a separate
collection point for electrical and electronic devices.
In cases of doubt, please contact your local authority or the dealer from whom you
purchased the device.
If this device is passed on to a third party (e.g. for further use in a private or com
mercial/industrial context), the general principle of this regulation must be commu
nicated at the same time.
Thank you for your contribution towards environmental protection.
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Declaration of system validation
We hereby give notice that this product / system and its software and accessories, were developed, test
ed and successfully certified on the basis of the product life-cycle policies of Mettler-Toledo AG, Analyti
cal. These policies are based on ISO Standard 9001:1994. Life-cycle checkpoint details were reviewed
and approved by the Project Supervisory Group (PSG). The products / systems were tested in respect of
functionality and specification prior to shipment. In order to support GLP and validation requirements, we
will make the following documents available to authorized persons for inspection:
● Performance specifications
● Software specifications
● Quality plan
● Project management system
● Test Plan
● Customer requirements
● Review reports
● Source code
Mettler-Toledo AG, Analytical will retain possession of all documents and their reproductions and may
wish to conclude a nondisclosure agreement with those requesting access to these documents.
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Product life cycle model
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Declaration of conformity
12 Declaration of conformity
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Declaration of conformity
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Declaration of conformity
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Subject to technical changes.