Materials Testing Technology
Materials Testing Technology
Materials Testing Technology
TECHNOLOGY
NESTOR B. CAOILE
Division Chief
DPWH- Bureau of Research and Standards
• WHAT IS QUALITY CONTROL?
• Quality Control are activities done by the
contractor to ensure the right materials and right
procedures used and done in the construction of a
certain projects. This includes the testing of construction
materials before its incorporation in the works.
MATERIALS QUALITY CONTROL
AND ASSURANCE
WHAT IS ASSURANCE?
WHAT IS QUALITY
ASSURANCE?
ASSURANCE is the degree of certainty.
QUALITY ASSURANCE is a function of
the owner to verify that the work is done
in accordance with specifications. Some
call it acceptance inspection.
WHAT IS MATERIALS
TESTING ?
is the basic means or a tool by which an engineer or an
inspector can be used to determined whether
the materials should be allowed to be incorporated
or be rejected into the work.
It should be emphasized that what are specified are the minimum number of
testing only. Additional number of test can be require to the materials if the
owner/inspector is in doubt of the quality of materials or the finished structure.
When the Testing of Materials Should Be Conducted
* Moisture Content
* Moisture - Density Relation
* Abrasion
* Field Density Test (FDT)
* California Bearing Ratio (CBR)
Concrete Aggregates ( Course and Fine )
* Sampling and Preparation of Samples
* Wash Test and Sieve Analysis
* Specific Gravity and Absorption
* Soundness
* Unit Weight
* Organic Impurities and Mortar Strength ( Fine Aggregates )
* Abrasion
Asphalt Aggregates ( Composite )
* Sampling and Preparation of Samples
* Wash Test and Sieve Analysis
* Plastic / Liquid Limit
* Abrasion
* Specific Gravity and Stripping
MODULE II
• Sampling and Testing of Cement and Concrete Mix
Cement
* Sampling and Preparation of Samples
* Normal Consistency and Time of Setting
* Autoclave Expansion
* Specific Gravity
* Compressive Strength
* Fineness
* Determination of Slump
Paints
• MODULE IV
• Sampling and Testing of Asphaltic Materials
and Asphalt Mix
Asphaltic Materials
Sampling / Preparation of Samples
* Asphalt Cement
* Emulsified Asphalt
* Cutback Asphalt
1. By method of quartering
SIGNIFICANCE:
Moisture content has an important characteristic in the soil
material where the behavior of soil is markedly influenced by the
amount of moisture it contains.
Moisture content is the ratio of the mass of water in the soil to
the mass of water in the dry soil after it has been dried to a
constant mass at a temperature of 110 deg. Centigrade.
II. PARTICLE SIZE ANALYSIS OF SOILS
SIGNIFICANCE :
Grain size distribution is widely used in the classification and
identification of soils. It is an important criteria in the classification of
highway sub-grade materials. It is also related to permeability and
capillarity of cohesionless soils.
SIGNIFICANCE:
It is a measure of the potential cohesion which in turn depend upon the total
size of the contact areas, or the fineness and shape of the grains.
Required Soil Sample(Sampling) : Material passing 0.425 mm ( No. 40 ) sieve
weighing 100 g minimum
CALCULATION:
W1 - W2
% Moisture = _____________ x 100
W2
The Plastic Limit is defined as the minimum moisture content at which the
soil can be readily molded without breaking or crumbling.
AASHTO T 99 Method C
- The highest point on the curve indicates the Maximum Dry Density
( MDD ) and the corresponding moisture content is called Optimum
Moisture Content ( OMC ).
VII. DETERMINATION OF DENSITY OF SOIL IN –
PLACE BY THE
SAND - CONE METHOD
SIGNIFICANCE:
Field density test is widely used as a control test to ensure adequate
compaction of in-placed embankment, sub-base, base and gravel surface
courses in a road construction.
Density of soil is defined as the weight/mass per unit volume. It is a very
significant engineering property of soils as strength is dependent upon
density.
VII. DETERMINATION OF DENSITY OF SOIL IN –
PLACE BY THE
SAND - CONE METHOD
Sand Cone Apparatus
Sieve no. 12
Los Angeles Abrasion machine
VIII. ABRASION TEST
Passing Retained A B C D
37.5 mm 25 mm 1250 + 25 - - -
25 mm 19 mm 1250 + 25 - - -
SIGNIFICANCE:
The CBR depends not only on the nature of the material but to a
large extent on its moisture content and its state of compaction.
IX. CALIFORNIA BEARING RATIO TEST ( CBR )
TESTING OF
PORTLAND CEMENT
1. Specific Gravity
2. Fineness Test by the no.
200 Sieve
3. Normal Consistency Test
4. Time of Setting by Gillmore
Needle
5. Autoclave Expansion Test
6. Air Content of Hydraulic
Cement
7. Compressive Strength of
Cement
8. Chemical Analysis of Cement
a. Insoluble Residue Test
b. Sulfur Trioxide Test
c. Magnesium Oxide Test
d. Loss on Ignition Test
Specific Gravity Test
The value of which is
used in the design of
concrete mixtures
Fineness Test by the
no. 200 Sieve
Determines the fineness
of cement which affect
the strength of concrete
% Fineness a
(Passing = 100 - x 100
No. 200) b
Where:
a = wt. of residue
b = wt. of original sample in
grams
Normal Consistency Test
Determines the normal
consistency of hydraulic
cement which is used to
determine the amount of
water required to prepare
paste for testing.
a
Normal = x 100
Consistency b
Where :
a = amount of water required
b = original wt. of cement sample
4. Time of Setting by Gillmore
Needle
5. Autoclave Expansion Test
6. Air Content of Hydraulic
Cement
7. Compressive Strength of
Cement
Time of Setting by
Gillmore Needle
1. Specific Gravity
- It is a gauge to a uniformity of supply of an asphalt (if it is being
adulterated or diluted).
- Important during computation and design (Job-Mix) essentials in the
determination of the effective asphalt content and the percentage of air
voids in compacted mix specimens and compacted pavement.
- Results is of value for making volume correction when measurements are
made at elevated temperature.
2. Solubility
- Determines the bitumen content in asphalt cement that is soluble in a
solvent (carbon disulfide and carbon tetrachloride).
- Measures the purity of the asphalt cement.
- Portion of the asphalt cement that is soluble represent the active
cementing constituents.
- Impurities such as salts, free carbon and non-organic contaminants does
not dissolve in a solvent.
3. Spot Test
- Determines if asphalts is overheated or not during production.
4. Loss of Heating
- Determines the loss of volatiles in the asphalt.
5. Flash Point
- Indicates the safe heating temperature of the asphalt, the
temperature to which the material maybe safely heated without
danger of instantaneous flash (catching fire or explode) in the
presence of an open flame.
6. Penetration
- Determines the relative hardness or consistency of an asphalt
cement, by measuring the distance of the standard needle used
that penetrate vertically to the sample under the fixed condition
of temperature, load, and time.
7. Ductility
- Measures the ability of asphalt to stretch without breaking
- A gauge to adhesiveness of asphalt, the higher the ductility the
more adhesive the asphalt.
8. Viscosity
- Liquidity or fluidity of asphalt.
- Consistency test of the liquid asphalt.
- Determines the flow characteristics of asphalt in the range
of temperature during application.
9. Distillation
- Determines the relative proportions of asphalt and diluent
present in liquid asphalt.
- also used to measure the amount of diluent that distills off
at various temperature denoting its evaporation
characteristics, this in turn, indicates the relative rate at
which the material will cure “after application”.
XI. Specifications:
Calculation:
wt. of original - wt. of sample
sample after extraction
% Asphalt Content = ----------------------------------------------- x 100
(by wt. of mix) wt. of original sample
Calculation:
A
Bulk Specific Gravity, Gmb = -------------------
B - C
where:
A = mass of specimen in air, g
B = mass of surface – dry specimen, g.
C = mass of specimen in water, g.
Calculation:
Load Load
Stability (Compressive Strength) = -------------- = ------------
Area D2/4
Wet Stability
Index of Retained Strength, (IRS), % = ---------------------- x 100
Dry Stability
MISCELLANEOUS CONSTRUCTION
MATERIALS
TESTS ON REINFORCING STEEL BARS
1. Variation in Mass
The test determines the actual size of the bar based on weight
Measurement per one-meter length and determines its variation to
the standard nominal mass per respective size of the steel bar
Variation in Mass, % :
DPWH Specification:
DPWH Specification:
DPWH Specification:
Strength Requirements:
Individual - 5.5 Mpa (800 psi) Minimum
Average - 6.9 Mpa (1000 psi) Minimum
Absorption - 240 kg/m3 Maximum
Strength Requirements:
Significance :
Compression test is performed on concrete masonry units such as solid
load, hollow load, and non-load bearing blocks in order to determine
its strength properties. The test is important for the evaluation of
compressive strength as a basis of acceptance.
Test Sample : 3 – full-size units taken from each lot of 10,000 units
or fraction thereof
Calculation :
Maximum Load, newtons ( or pound-force )
Compressive Strength = _________________________________________
Gross Cross Sectional Area of the Unit, mm2
Gross Cross Sectional Area of the Unit, mm2 = is the total area of a
section perpendicular to the direction of the load,
including areas within cells.
Dimension measurement of Concrete Hollow Block (CHB)
DETERMINATION OF ABSORPTION AND MOISTURE CONTENT
OF CONCRETE MASONRY UNITS
Significance
Absorption and moisture content tests of concrete masonry units are performed
so as to determine the actual percentage of water and the absorption
characteristic of the concrete when subjected in a saturated condition. The
values of this are necessary in the evaluation relative to its permissible value of
acceptance.
Apparatus 1. Oven with temperature control up to 115 ºC
2. Balance sensitive within 0.5 % of the weight
1. Three (3) full size units shall be used and taken from six (6) units
selected from each lot of 10,000 units or fraction thereof.
WORK SHEET FOR TESTS ON CONCRETE HOLLOW BLOCKS
Project __________________________________________________________________________________________
Proposed use ______________________________________ Spec’s Item No. _________________________________
Tested by__________________________________________ Computed by __________________________________
Lab. _______________(Name and designation) (Date) (Name and designation) (Date)
Sample Identification 1 2 3
5. Compressive Strength:
66,000# 76,000# 67,000#
Ultimate Load, kg
Compressive Strength, MN/m2 4.9 5.6 5.0
Compressive Strength, MN/2 (Avg. of 3 units) 5.2
II 50.0 75.0 27.6 Mpa (4000 psi) 27.6 Mpa (4000 psi)
III 65.0 100.0 27.6 Mpa (4000 psi) 27.6 Mpa (4000 psi)
IV 100.0 150.0 34.5 Mpa (5000 psi) 27.6 Mpa (4000 psi)
V 140.0 175.0 41.4 Mpa (6000 psi) 41.4 Mpa (6000 psi)
Basis of Acceptance:
Load Bearing Test - shall be determine by the results of :
a. three –edge bearing tests to produce a 0.3 mm crack and the
ultimate load (strength) of the pipe.
b. Absorption test on selected samples of concrete from the wall of
the pipe.
c. Visual inspection of the finished pipe to determine its
conformance with the accepted design and its freedom from
defects.
QUALITY CONTROL OF RCCP AND SIGNIFICANCE
RCP are tested to assure uniformity of quality
To check compliance with design and other
specification requirements
Alternative Requirements:
1 - set consisting of 3 cylinder samples -
For not more than 25 pipes cast in the field
1 – Inspection Report for each size for not more
than 25 pipes cast in the field
- For cement, fine aggregate and water – testing is
sample for Item 405 (Structural Concrete)
TESTS ON RCCP AND SIGNIFICANCE
- Proof of design.
Absorption Test
- Performed to establish the fact that the finished,
shippable pipe meets the absorption limits stated in
the specification.
EXTERNAL LOAD CRUSHING STRENGTH TEST OF CONCRETE
PIPE BY THREEE – EDGE BEARING METHOD
Significance :
The crushing test can be either a quality control test performed to
establish that the finished pipe has sufficient strength to withstand
the crushing loads stated in the specifications or a proof of design
testing performed to prove the adequacy of design.
Record the load to produce a 0.3 mm crack. The 0.3 mm crack load is the
maximum load applied to the pipe before a crack having a width of 0.3 mm
occurs throughout a continuous length of 300 mm or more measured parallel to
the longitudinal axis of pipe barrel.
QUALITY TEST ON COMMON
CONSTRUCTION MATERIALS
COMMON MATERIAL TEST REQUIRED
1. Excavated and Subgrade Materials 1. Grading Test
2. Plasticity Test
3. Laboratory Compaction (Standard)
4. Field Density Test (FDT)
2. Embankment Materials 1. Same as No. 1
3. Aggregate Subbase Course Materials 1. Grading Test
2. Plasticity Test
3. Laboratory Compaction (Modified)
4. Abrasion
5. California Bearing Ratio (CBR)
6. Field Density Test (FDT)
4. Aggregate Base Course Materials 1. Same as No. 3
5. Crushed Aggregate Base Course 1. Same as No. 3
Materials 2. Fractured Face
6. Aggregate Surface Course Materials 1. Grading Test
2. Plasticity Test
3. Abrasion
4. Fractured Face
5. California Bearing Ratio (CBR)
COMMON MATERIAL TEST REQUIRED
7. Aggregate Materials for Bituminous 1. Grading Test
Road Surface Course Mix 2. Plasticity Test
3. Abrasion
4. Stripping
5. Bulk Specific Gravity
6. Fractured Face
8. Fine Aggregates 1. Grading Test
2. Bulk Specific Gravity and Absorption
3. Effect of Organic Impurities on Strength of
Mortar
4. Soundness Test
5. Organic Impurities
6. Unit Weight (Loose and Rodded)
7. Clay Lumps and Friable Particles
COMMON MATERIAL TEST REQUIRED
9. Coarse Aggregates 1. Grading Test
2. Bulk Specific Gravity and Absorption
3. Abrasion
4. Soundness Test
5. Unit Weight (Loose and Rodded)
10. Asphalt Cement Penetration Graded 1. Penetration Test
2. Flash Point (Cleveland Open-Cup)
3. Ductility
4. Solubility Test
5. Specific Gravity
6. Thin-film Oven Test/ Loss on Heating
7. Spot Test
COMMON MATERIAL TEST REQUIRED
11. Bituminous Mix 1. Extraction (Bitumen Content)
2. Grading Test Mechanical
3. Bulk Specific Gravity
4. Stability Test
5. Thickness Determination
6. Density Test
12. Emulsified Asphalt (Cationic/Anionic) 1. Viscosity, Saybolt-Furol
2. Storage Stability Test
3. Cement Mixing
4. Sieve Test
5. Specific Gravity Test
6. Distillation Test
7. Penetration Test
8. Ductility Test
9. Solubility Test
COMMON MATERIAL TEST REQUIRED
13. Cutback Asphalt 1. Kinematic Viscosity
2. Flash Point (Tag Open-Cup)
3. Specific Gravity
4. Distillation Test
5. Penetration test
6. Ductility
7. Solubility
8. Spot Test
14. Mineral Filler 1. Grading Test
2. Plasticity Test
3. Loss on Ignition
15. Portland Cement (Physical Test and 1. Air Content of Mortar
Chemical Analysis) 2. Fineness by Air-Permeability Test
3. Autoclave Expansion
4. Compressive Strength
5. Time of Setting by Vicat Apparatus
6. False Set
7. Heat of Hydration
8. Sulfate Resistance
COMMON MATERIAL TEST REQUIRED
9. Specific Gravity/Density
10. Time of Setting by Gillmore Needle
11. Fineness by Turbidimeter
12. Calcium Sulfate
16. Blended Hydraulic Cement (Physical 1. Fineness
Test and Chemical Analysis) 2. Autoclave Expansion
3. Autoclave Contraction
4. Time of Setting Vicat Needle
5. Air Content of Mortar
6. Compressive Strength
7. Magnesium Oxide
8. Sulfur Trioxide
9. Insoluble Residue
10. Loss on Ignition
17. Concrete Joint Sealer 1. Pour Point Temperature
2. Safe Heating temperature
3. Penetration Test
4. Flow
COMMON MATERIAL TEST REQUIRED
18. Concrete Samples/ Concrete Cores 1. Compressive Strength for Cylinders
2. Flexural Strength for beams
3. Thickness Measurement
19. Reinforced Concrete Pipe 1. Strength Test
2. Water Absorption
3. Dimension Measurement
4. Moisture Content
20. Reinforcing Steel Bars 1. Test for Tensile Properties (Yield, Tensile,
Elongation)
2. Test for Bending
3. Actual Unit Mass
4. Variation in Mass
5. Deformation Measurement
6. Phosphorous Content
RECOMMENDED SIZE OF
SAMPLE FOR TESTING
COMMON MATERIAL MINIMUM QUANTITY REQUIRED FOR
SUBMISSION
1. Excavated and Subgrade Materials 50 kgs.
2. Embankment Materials 50 kgs.
3. Aggregate Subbase Course Materials 50 kgs. –Quality Test
20 kgs. – Soil Classification
4. Aggregate Base Course Materials 50 kgs. –Quality Test
20 kgs. – Soil Classification
5. Crushed Aggregate Base Course 50 kgs.
Materials
6. Aggregate Surface Course Materials 50 kgs.
7. Aggregate Materials for Bituminous Road 50 kgs.
Surface Course Mix
8. Fine Aggregates 50 kgs.
9. Coarse Aggregates 50 kgs.
10. Asphalt Cement Penetration Graded 1 Gallon
11. Bituminous Mix 20 kgs.
12. Emulsified Asphalt (Cationic/Anionic) 1 Gallon
COMMON MATERIAL MINIMUM QUANTITY REQUIRED FOR
SUBMISSION
13. Cutback Asphalt 1 Gallon
14. Mineral Filler 5 kgs.
15. Portland Cement Physical Test and 10 kgs.
Chemical Analysis
16. Blended Hydraulic Cement 10 kgs.
17. Concrete Joint Sealer 5 kgs.
18. Concrete Samples/ Core Samples Atleast one (1) but not more than three (3)
in full day’s operation
19. Reinforced Concrete Pipe 1 pipe, 1-m length
20. Reinforcing Steel Bars 1 pc., 1-m length