This document summarizes alkaloids, including:
1. Alkaloids are naturally occurring chemical compounds found in several plants like opium and coca.
2. They are classified based on their chemical structure and include true, proto and pseudo alkaloids.
3. Common extraction methods are described like maceration in ethanol or acid-base extraction.
[END SUMMARY]
This document summarizes alkaloids, including:
1. Alkaloids are naturally occurring chemical compounds found in several plants like opium and coca.
2. They are classified based on their chemical structure and include true, proto and pseudo alkaloids.
3. Common extraction methods are described like maceration in ethanol or acid-base extraction.
[END SUMMARY]
This document summarizes alkaloids, including:
1. Alkaloids are naturally occurring chemical compounds found in several plants like opium and coca.
2. They are classified based on their chemical structure and include true, proto and pseudo alkaloids.
3. Common extraction methods are described like maceration in ethanol or acid-base extraction.
[END SUMMARY]
This document summarizes alkaloids, including:
1. Alkaloids are naturally occurring chemical compounds found in several plants like opium and coca.
2. They are classified based on their chemical structure and include true, proto and pseudo alkaloids.
3. Common extraction methods are described like maceration in ethanol or acid-base extraction.
[END SUMMARY]
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P Pr ro of f. .D Da ay ya ar r A Ar rb ba ai in n/ /S SE EM ME ES ST T~ ~5 5/ /a al lk ka al lo oi id d. .h ht tm ml l 3 urlu| d| |apargar Veloda Cu|veror- F|lzgera|d re|al|l |eo|r pra|l|s dar rurg||r ul| d||a|sara|ar.
C Co on nt to o Heksan Ekstrak heksan (cek Mar MeOH Pekatkan Partisi EtoAc-2% Asam Tartrat EtOAc (fraksi netral/basa sgt lemah) 2% Asam Tartrat Basakan (NH3/Na2CO3) Ekstrak dengan Alkaloid basa lemah Larutan air basa (boleh jadi mengandung Sampel
P Pr ro of f. .D Da ay ya ar r A Ar rb ba ai in n/ /S SE EM ME ES ST T~ ~5 5/ /a al lk ka al lo oi id d. .h ht tm ml l 4 Perurr|ar Kr|sla||sas| |argsurg Kr|sla||sas|-der|val|sas| 0rad|erl pl exlracl|or Kroralogral| (serapar, parl|s|) F||lras| (sepradex) Kara|ler|sas| / E|us|das| 3lru|lur TL sp (3eryaWa |a|ra|, sudul pular opl||) uv, (seryaWa Aroral||/||alar |oryugas|) lR (ul| gugus lurgs|) V3 (8V) 1l RVl (ul| pos|s| dar ||alar l) 13C RVl (ul| pos|s| dar ||alar C) 8eoerapa pe|arul ul| s|sl|r KLT ClC|3/Ve0l (9:1; 19:1) ClC|3/Tr|el||ar|r (9:1) EloAc El0Ac - Ve0l (19:1), (9:1), (1:1)
Perggo|orgar a||a|o|d oerdasar|ar precursor 8|os|rles|s a||a|o|d 8|os|rles|s oeoerapa pre|ursor relaoo||l se|urder dar relaoo||l pr|rer ulara A|ka|o|d turunan L|s|n
P Pr ro of f. .D Da ay ya ar r A Ar rb ba ai in n/ /S SE EM ME ES ST T~ ~5 5/ /a al lk ka al lo oi id d. .h ht tm ml l 5 |os|ntesa A|ka|o|d turunan ||s|n
A||a|o|d lururar po||aselal |os|ntesa A|ka|o|d Turunan Po||asetat (kon||n}
P Pr ro of f. .D Da ay ya ar r A Ar rb ba ai in n/ /S SE EM ME ES ST T~ ~5 5/ /a al lk ka al lo oi id d. .h ht tm ml l 6 Turunan Po||asetat
|os|ntesa asam antra|n||at
P Pr ro of f. .D Da ay ya ar r A Ar rb ba ai in n/ /S SE EM ME ES ST T~ ~5 5/ /a al lk ka al lo oi id d. .h ht tm ml l 7 eberapa a|ka|o|d turunan asam antran||at
Fen||aa|an|n-t|ros|n
P Pr ro of f. .D Da ay ya ar r A Ar rb ba ai in n/ /S SE EM ME ES ST T~ ~5 5/ /a al lk ka al lo oi id d. .h ht tm ml l 8
P Pr ro of f. .D Da ay ya ar r A Ar rb ba ai in n/ /S SE EM ME ES ST T~ ~5 5/ /a al lk ka al lo oi id d. .h ht tm ml l 9 eberapa a|ka|o|d sederhana turunan tryptophan
P Pr ro of f. .D Da ay ya ar r A Ar rb ba ai in n/ /S SE EM ME ES ST T~ ~5 5/ /a al lk ka al lo oi id d. .h ht tm ml l 10
A A| || |a a| |o o| |d d | |r rd do o| | r ro or ro ol le er rp pe er ro o| |d da a| |: :
A A| || |a a| |o o| |d d A As sa a| | a a| |l l| |l l| |l la as s l la ar rr ra a| |o o| |o og g| |s s
1 1. .A Aj jr ra a| || |c c| |r re e C Ca al lr ra ar ra ar rl lr ru us s r ro os se eu us s l ly yp po ol le er rs s| |v ve e 2 2. .A Aj jr ra a| || |r r R Ru uW Wo o| |l l| |a a s sp p A Ar rl l| |a ar rr ry yl lr rr r| |c c 3 3. .C Ca ar rp pl lo ol lr re ec c| |r re e C Ca ar rp pl lo ol lr re ec ca a a ac cu ur r| |r ra al la a A Ar rl l| |c ca ar rc ce er r 1 1. .0 0e es se er rp p| |d d| |r re e R Ra au uW Wo o| |l l| |a a c ca ar re es sc ce er rs s l ly yp po ol le er rs s| |v ve es s 5 5. .l lo oo og ga a| |r re e T Ta ao oe er rr ra ar rl lr re e | |o oo og ga a P Ps sy yc cr ro ol lo or r| |r re el l| |c c . .L Le eu ur ro oc cr ry ys sl l| |r re e C Ca al lr ra ar ra ar rl lr ru us s r ro os se eu us s A Ar rl l| |c ca ar rc ce er r Z Z. . 0 0u u| |r r| |d d| |r re e R Re er r| |j ja a s sp p C Ca ar rd d| |a ac c d de ep pp pr re es ss sa ar rl l 8 8. . R Re es se er rp p| |r r R Ra au uW Wo o| |l l| |a a v vo or r| |l lo or r| |a a r ry yp po ol le er rs s| |v ve e 9 9. . 3 3l lr ry yc cr rr r| |r re e 3 3l lr ry yc cr rr ro os s r ru ux x l lo or r| |c ca a C CN N3 3 d de ep pr re es ss sa ar rl l 1 10 0. .v v| |r rc ca a| |e eu uc co oo o| |a as sl l| |r re e C Ca al lr ra ar ra ar rl lr ru us s r ro os se eu us s A Ar rl l| |c ca ar rc ce er r 1 11 1. .v v| |r rc ca ar r| |r re e v v| |r rc ca a r ra aj jo or r l ly yp po ol le er rs s| |v ve es s Alkaloid indol monoterpenoid
P Pr ro of f. .D Da ay ya ar r A Ar rb ba ai in n/ /S SE EM ME ES ST T~ ~5 5/ /a al lk ka al lo oi id d. .h ht tm ml l 11
P Pr ro of f. .D Da ay ya ar r A Ar rb ba ai in n/ /S SE EM ME ES ST T~ ~5 5/ /a al lk ka al lo oi id d. .h ht tm ml l 12 a|kao|da catharantus le|ar oerras|| d||derl|l||as| |eo|r dar| 90 jer|s v|rca|eucoo|asl|re (vL8), R = Cl3 (1 g/lor) Leurocrysl|re (vCR), R = Cl0 (20 rg/lor)
