Neraca Massa Fracination

Menghitung berat molekul rata rata triglserida
% berat
BM
Komponen
kg/kmol
0.3
116
C6h1202
0.9
144
c8h16o2
4
172
c10h20o2
49.6
200
c12h24o2
16
228
c14h28o2
8
256
c16h32o2
c18h32o2 linoleic
5.4
280
c18h34o2 oleic
13.7
282
c18h36o2 steric
2
284
c20h30o2
0.1
302
H20
18.02
H3PO4
98
Jumlah
100
2380.02
Data Kapasitas Panas
Komponen
c14h28o2
c16h32o2
c18h36o2
c18h34o2
c18h32o2
air
Jumlah
A
80.266
86.29
99.012
278.686
241.348
92.053
BT
CT2
2.82E+00
3.52E+00
3.59E+00
2.54E+00
2.31E+00
-4.00E-02
-6.01E-03
-7.32E-03
-7.25E-03
-5.44E-03
-5.07E-03
-2.11E-04
SFC
8% 15 C
2% 15 C
58
60
DT3
5.13E-06
6.10E-06
5.90E-06
4.92E-06
4.75E-06
5.35E-07
TMIN
329
337
344
288
269
273
CPO masuk
Asam laurat (C12:0)
Asam miristat (C14:0)c14h28o2
Asam Palmitat (C16:0) c16h32o2
Asam stearat (C18:0)
Asam oleat (C18:1)
Asam linoleat (C18:2)
Asam linolenat (C18:3)
jumlah
asumsi Komposisi
TMAX
CP. 25
680
698
719
703
698
615
1.7
43
5.4
38
11.9
100
6.84E+02
6.04E+02
7.56E+01
Komposisi
0-0.4
0.6-2
41.1-47
3.7-5.6
38.2-43.6
6.6-12.1
0.0-0.6
%
56
64
71
15
-4
0
Sumber : http://repository.usu.ac.id/bitstream/123456789/22472/1/Appendix.p
22472/1/Appendix.pdf
Membuat crude olein

Basis satu kristalizer
CPO
Air
Impurities asumsi sangat kecil
40000 Kg
99.7 %
0.3 %
0%
CPO masuk
asumsi Komposisi

Asam stearat (C18:0) c18h36o2
Asam oleat (C18:1)c18h34o2
Asam linoleat (C18:2) c18h32o2
2
42.1
5.6
38.2
12.1
100
Massa masuk kristalizer

CPO masuk
Air
Jumlah
Yield
Stearin mengkristal 0.43 %
Masuk (kg)
797.6
16789.48
2233.28
15234.16
4825.48
120
40000
%
%
%
%
%
KMol
3.498245614
65.58390625
7.8636619718
54.0218439716
17.2338571429
6.6592674806
154.860782431
32023.64 Kg
7976.36 Kg
Neraca masuk HE 111
CPO masuk
Asam miristat (C14:0)c14h28o2 padat
Asam Palmitat (C16:0) c16h32o2 larutan
Asam stearat (C18:0) c18h36o2 padat
Asam oleat (C18:1)c18h34o2 larutan
Asam linoleat (C18:2) c18h32o2 padat
Air
Jumlah
Masuk (kg)
797.6
Keluar (Kg)
797.6
16789.48
16789.48
2233.28
2233.28
15234.16
15234.16
4825.48
120
40000
4825.48
120
40000
Neraca Panas masuk

Tin=
Tref
CPO masuk
Air
JUMLAH
40 c
25 c
Masuk (kg) Masuk (Kmol)
797.6
3.498245614
16789.48
65.58390625
2233.28
7.8636619718
15234.16
54.0218439716
4825.48
17.2338571429
120
6.6592674806
40000
154.86078243
Panas Steam yang dibutuhkan

Maka Q yang harus ditambahkan ke sistem :
1171136.6351
Q steam
msteam =
steam
Bar
Hv
1.985
2706
2 2706.29329609
2.701
2720
M steam=
Msteam perhari
excess 25 %
Hl
503.7
504.5924581
546.3
531.9235996672 Kg/stegh jam

12766.16639201 Kg/hari
15957.70799002 Kg/hari
15.95770799 Ton hari
39880
120
Komponen
c14h28o2
c16h32o2
c18h36o2
c18h34o2
c18h32o2
air
Jumlah
80.0591 Kg
19.9409 Kg
A
80.266
86.29
99.012
278.686
241.348
92.053
313.15 K
298.15 K
Cpdt
Q
1514.1161753 5296.75027
1682.60654189
110351.91
1880.68276617 14789.0535
4460.36988188 240957.406
3874.06173919 66765.0266
1376.06964592 9163.61584
14787.90675 447323.76
Kj
steam
2201.700838
1063.84719933 Kg/jam
Neraca Panas KELUAR dengan pendin

Tin=
Tref
CPO masuk
Asam miristat (C14:0)c1
Asam Palmitat (C16:0) c
Asam stearat (C18:0) c1
Asam oleat (C18:1)c18h3
Asam linoleat (C18:2) c
Air
JUMLAH
BT
CT2
2.82E+00
3.52E+00
3.59E+00
2.54E+00
2.31E+00
-4.00E-02
-6.01E-03
-7.32E-03
-7.25E-03
-5.44E-03
-5.07E-03
-2.11E-04
DT3
5.13E-06
6.10E-06
5.90E-06
4.92E-06
4.75E-06
5.35E-07
TMIN
3.29E+02
3.37E+02
3.44E+02
2.88E+02
2.69E+02
2.73E+02
TMAX
CP. 25
6.80E+02
6.98E+02
7.19E+02
7.03E+02 6.84E+02
6.98E+02 6.04E+02
6.15E+02 7.56E+01
s KELUAR dengan pendingin air pendingin

70 c
343.15 K
25 c
298.15 K
Masuk (kg) Masuk (mol)
Cpdt
Q
797.6
3.498245614 6286.078 21990.24374
16789.48
65.58390625 7234.653 474476.81513
2233.28
7.8636619718 7873.664 61915.835006
15234.16
54.021843972 14956.01 807951.07967
4825.48
17.233857143 13046.97 224849.59299
120
6.6592674806 4096.071 27276.830358
40000
154.8607824 53493.4 1618460.397
Membuat crude olein

CPO
Air
40000 Kg
99.7 %
0.3 %
0%
CPO masuk
asumsi Komposisi

2
42.1
5.6
38.2
12.1
100

CPO masuk
Air
Jumlah
Yield
Stearin mengkristal 0.43 %
Masuk (kg)
797.6
16789.48
2233.28
15234.16
4825.48
120
40000
%
%
%
%
%
KMol
3.498245614
65.58390625
7.8636619718
54.0218439716
17.2338571429
6.6592674806
154.860782431
32023.64 Kg
7976.36 Kg
Neraca Kristalizer
CPO masuk
Asam miristat (C14:0)c14h28o2 padat
Asam Palmitat (C16:0) c16h32o2 larutan
Asam stearat (C18:0) c18h36o2 padat
Asam oleat (C18:1)c18h34o2 larutan
Asam linoleat (C18:2) c18h32o2 padat
Air
Jumlah
Masuk (kg)
797.6
Keluar (Kg)
797.6
16789.48
16789.48
2233.28
2233.28
15234.16
15234.16
4825.48
120
40000
4825.48
120
40000
Neraca Panas masuk

Tin=
Tref
CPO masuk
Asam miristat (C14:0)c14h28o2(s)
Asam Palmitat (C16:0) c16h32o2 (l)
Asam stearat (C18:0) c18h36o2 (s)
Asam oleat (C18:1)c18h34o2 (l)
Asam linoleat (C18:2) c18h32o2 (s)
Air
JUMLAH
Panas Pendingin yang dibuthkan
70 c
25 c
797.6
3.498245614
0
16789.48
65.58390625
0
2233.28
7.8636619718
0
15234.16
54.0218439716
0
4825.48
17.2338571429
0
120
6.6592674806
40000
154.86078243
-1331008.57028
Air pendingin masuk suhu 30

Air pendingin masuk suhu 50
CPdT air masuk 30

CPdT air keluar 50
459.7569
2287.7928
M air yang dibutuhkan

Mair 12Kristalizer
728.1085467521 kmol /jam

157446.19215 Kg/6 jam
Neraca Panas keluar saat menggunakan air chiller

Tin=
24 c
Tref
25 c
CPO masuk
0
0
Asam miristat (C14:0)c14h28o2(s)
797.6
3.498245614
0
0
Asam Palmitat (C16:0) c16h32o2 (l)
16789.48
65.58390625
0
0
Asam stearat (C18:0) c18h36o2 (s)
2233.28
7.8636619718
0
0
Asam oleat (C18:1)c18h34o2 (l)
15234.16
54.0218439716
0
0
Asam linoleat (C18:2) c18h32o2 (s)

Air
JUMLAH
4825.48
120
40000
17.2338571429
6.6592674806
154.86078243
Panas yang dibutuhkan dari peralihan air pendgin ke air chiller

Maka air chiler yang digunakan
282.7914375408 kmol /jam
12 cristalizer
61150.82045383 kg/jam
total air
218597.0126035 Kg/hari
39880
120
Komponen
c14h28o2
c16h32o2
c18h36o2
c18h34o2
c18h32o2
air
Jumlah
80.0591 Kg
19.9409 Kg
A
80.266
86.29
99.012
278.686
241.348
92.053
343.15 K
298.15 K
Cpdt
Q
6286.07769905 21990.2437
0
7234.65316814 474476.815
0
7873.66435992
61915.835
0
14956.0070569
807951.08
0
0
13046.9685992 224849.593
0
0
4096.07069205 27276.8304
53493.441575 1618460.4

Tin=
Tref
CPO masuk
Asam miristat (C14:0)c
Asam Palmitat (C16:0)
Asam Palmitat (C16:0) c
Asam stearat (C18:0) c
Asam oleat (C18:1)c18h
Asam oleat (C18:1)c18h3
Asam linoleat (C18:2)
Air
JUMLAH
Kj
Kj/kmol
Kj/kmol
13120.5160125 Kg
297.15 K
298.15 K
Cpdt
-78.8558953842
-84.5257079083
-97.2158823908
-277.412486936
Tin
Q
0
-275.85729
0
-5543.5261
0
-764.472837
0
-14986.3341
0
Tout
CPdT air masuk 7 C
CPdT air keluar 20 C
-240.193060047 -4139.45288
-92.072906023 -613.138109
-870.2759387 -26322.781
-313774.6079 Kj
5095.90170449 Kg/jam
218.5970126 Ton air
BT
CT2
2.82E+00
3.52E+00
3.59E+00
2.54E+00
2.31E+00
-4.00E-02
-6.01E-03
-7.32E-03
-7.25E-03
-5.44E-03
-5.07E-03
-2.11E-04
DT3
5.13E-06
6.10E-06
5.90E-06
4.92E-06
4.75E-06
5.35E-07
TMIN
3.29E+02
3.37E+02
3.44E+02
2.88E+02
2.69E+02
2.73E+02
TMAX
CP. 25
6.80E+02
6.98E+02
7.19E+02
7.03E+02 6.84E+02
6.98E+02 6.04E+02
6.15E+02 7.56E+01

35 c
308.15 K
25 c
298.15 K
Cpdt
Q
0
0
0
0
797.6
3.498245614 941.4795 3293.5265016
0
0
0
0
16789.48
65.58390625 1036.66 67988.191501
0
0
0
0
2233.28
7.8636619718 1167.089 9177.5904414
0
0
0
15234.16
54.021843972 2912.23 157324.06042
0
0
0
4825.48
17.233857143 2527.128 43552.164663
120
6.6592674806 918.4633 6116.2930748
40000
154.8607824 9503.05 287451.8266
8C
20
C
-1570.3174 Kj/kmol
-460.7555 Kj/kmol
281.15
293.15
Pencairan bak stearin

CPO
Air
40000 Kg
99.7 %
0.3 %
0%
CPO masuk
asumsi Komposisi

2
42.1
5.6
38.2
12.1
100

Cake padat
Air
Jumlah
Masuk (kg)
797.6
2233.28
4825.48
120
7976.36
Neraca Panas masuk

Tin=
Tref
CPO masuk
Air
JUMLAH
KMol
3.498245614
7.8636619718
17.2338571429
6.6592674806
35.2550322093
24 c
25 c
797.6
3.498245614
2233.28
7.8636619718
4825.48
17.2338571429
120
6.6592674806
7976.36
35.255032209

255074.06689
Q steam
msteam =
steam
Bar
Hv
1.985
2706
2 2706.29329609
2.701
2720
M steam=
Msteam perhari
excess 25 %
%
%
%
%
%
Hl
503.7
504.5924581
546.3
115.8531906297 Kg
1390.238287556 Kg/hari
1737.797859445 Kg/hari
1.7377978594 Ton hari
39880
120
Komponen
c14h28o2
c16h32o2
c18h36o2
c18h34o2
c18h32o2
air
Jumlah
297.15 K
298.15 K
Cpdt
Q
-78.8558953842 -275.85729
-97.2158823908 -764.472837
-240.193060047 -4139.45288
-92.072906023 -613.138109
-508.3377438 -5792.9211
Kj
steam
2201.700838
A
80.266
86.29
99.012
278.686
241.348
92.053

Tin=
Tref
CPO masuk
Air
JUMLAH
BT
CT2
2.82E+00
3.52E+00
3.59E+00
2.54E+00
2.31E+00
-4.00E-02
-6.01E-03
-7.32E-03
-7.25E-03
-5.44E-03
-5.07E-03
-2.11E-04
DT3
5.13E-06
6.10E-06
5.90E-06
4.92E-06
4.75E-06
5.35E-07
TMIN
3.29E+02
3.37E+02
3.44E+02
2.88E+02
2.69E+02
2.73E+02

60 c
333.15 K
25 c
298.15 K
Cpdt
Q
797.6
3.498245614 4450.264 15568.11686
2233.28
7.8636619718 5561.326 43732.383991
4825.48
17.233857143 9789.286 168707.1594
120
6.6592674806 3194.568 21273.485523
7976.36
35.25503221 22995.4 249281.1458
TMAX
CP. 25
6.80E+02
6.98E+02
7.19E+02
7.03E+02 6.84E+02
6.98E+02 6.04E+02
6.15E+02 7.56E+01

olein washing
CPO
Air
8000 Kg
99.7 %
0.3 %
0%
CPO masuk
asumsi Komposisi

2
42.1
5.6
38.2
12.1
100

Cake padat
Masuk (kg)
3368
3056
Jumlah
6424
Neraca Panas masuk

Tin=
Tref
CPO masuk
KMol
13.15625
10.8368794326
0
0
23.9931294326
30 c
25 c
3368
13.15625
3056
10.8368794326
0
0
0
0
6424
23.993129433
JUMLAH
272215.05963
Q steam
msteam =
steam
Bar
Hv
1.985
2706
2 2706.29329609
2.701
2720
M steam=
Msteam perhari
excess 25 %
%
%
%
%
%
Hl
503.7
504.5924581
546.3
123.6385320525 Kg
247.2770641051 Kg/hari
309.0963301314 Kg/hari
0.3090963301 Ton hari
7976
24
Komponen
c14h28o2
c16h32o2
c18h36o2
c18h34o2
c18h32o2
air
Jumlah
303.15 K
298.15 K
Cpdt
Q
475.192132307 6251.74649
1424.99679021 15442.5184
0
0
1900.1889225 21694.265
Kj
steam
2201.700838
80.266
86.29
99.012
278.686
241.348
92.053
Neraca Panas KELUAR dengan pendingin air p

Tin=
Tref
CPO masuk
JUMLAH
BT
CT2
2.82E+00
3.52E+00
3.59E+00
2.54E+00
2.31E+00
-4.00E-02
-6.01E-03
-7.32E-03
-7.25E-03
-5.44E-03
-5.07E-03
-2.11E-04
DT3
5.13E-06
6.10E-06
5.90E-06
4.92E-06
4.75E-06
5.35E-07
TMIN
3.29E+02
3.37E+02
3.44E+02
2.88E+02
2.69E+02
2.73E+02
dengan pendingin air pendingin

75 c
348.15 K
25 c
298.15 K
Cpdt
Q
3368
13.15625 8423.586 110822.79769
3056
10.836879433 16894.76 183086.52683
6424
23.99312943 25318.4 293909.3245
TMAX
CP. 25
6.80E+02
6.98E+02
7.19E+02
7.03E+02 6.84E+02
6.98E+02 6.04E+02
6.15E+02 7.56E+01

CPO
Air
40000 Kg
99.7 %
0.3 %
0%
CPO masuk
asumsi Komposisi

2
42.1
5.6
38.2
12.1
100

Cake padat
Masuk (kg)
16789.48
15234.16
Jumlah
32023.64
Neraca Panas masuk

Tin=
Tref
CPO masuk
KMol
65.58390625
54.0218439716
0
0
119.605750222
24 c
25 c
16789.48
65.58390625
15234.16
54.0218439716
0
0
0
0
32023.64
119.60575022
JUMLAH
245842.11211
Q steam
msteam =
steam
Bar
Hv
1.985
2706
2 2706.29329609
2.701
2720
M steam=
Msteam perhari
excess 25 %
%
%
%
%
%
Hl
503.7
504.5924581
546.3
111.6600892672 Kg
1339.921071206 Kg/hari
1674.901339007 Kg/hari
1.674901339 Ton hari
39880
120
Komponen
c14h28o2
c16h32o2
c18h36o2
c18h34o2
c18h32o2
air
Jumlah
297.15 K
298.15 K
Cpdt
Q
-84.5257079083 -5543.5261
-277.412486936 -14986.3341
0
0
-361.9381948 -20529.86
Kj
steam
2201.700838
80.266
86.29
99.012
278.686
241.348
92.053
Neraca Panas KELUAR dengan pendingin air p

Tin=
Tref
CPO masuk
JUMLAH
BT
CT2
2.82E+00
3.52E+00
3.59E+00
2.54E+00
2.31E+00
-4.00E-02
-6.01E-03
-7.32E-03
-7.25E-03
-5.44E-03
-5.07E-03
-2.11E-04
DT3
5.13E-06
6.10E-06
5.90E-06
4.92E-06
4.75E-06
5.35E-07
TMIN
3.29E+02
3.37E+02
3.44E+02
2.88E+02
2.69E+02
2.73E+02
dengan pendingin air pendingin

35 c
308.15 K
25 c
298.15 K
Cpdt
Q
16789.48
65.58390625 1036.66 67988.191501
15234.16
54.021843972 2912.23 157324.06042
32023.64
119.6057502 3948.89 225312.2519
TMAX
CP. 25
6.80E+02
6.98E+02
7.19E+02
7.03E+02 6.84E+02
6.98E+02 6.04E+02
6.15E+02 7.56E+01
Konsumsi Steam
HE 111
HE 241
Bak stearin
Bak Olein
Jumlah
Konsumsi Air pendingin

15957.71 Kg/hari
1737.798 Kg/hari
309.0963 Kg/hari
1674.901 Kg/hari
19679.5 Kg/hari
Cristalizer CT
157446.1921497
Cristalizer Chiller
61150.82045383
Jumlah
218597.012603
Kg/hari
Kg/hari
Kg/hari
Konsumsi air pendingin

Fraksinasi
Cristalizer CT
13120.52
157446.1921
refenery
kondenser He 751
HE 742
25.26527
2423.255
606.3664093
58158.12335
Jumlah
Kebutuhan air
Asumsi Make up air pendingin 10 %
Make Up Cooling Tower
Air untuk karyawan kantor

Air untuk keperluan ini diperkirakan
Air untuk kebersihan dan pertamanan
Keperluan air umpan boiler
Jumlah
15569 Kg/jam
21621.07 m3/jam
21621.07 m3/jam
8 m3/jam
2.5 m3/jam
5 m3/jam
2.083333 m3/jam
43259.72 m3/jam
216210.682 m3/jam
Kebutuhan air untuk karyawan = 40 lit
data 50 ton /hari
make-up water
Water evaporation (We)
Water drift loss (Wd)
Water blowdown (Wb)
S
Dipilih = 3
Wm
= 0,0085 Wc (T1-T2)
= Drift loss x Wc (Perrys

= Wc/2(S-1)
= rasio klorida dalam air sirkulasi terhadap air make up 3 5
= We + Wd + Wb
Wc = aliran air sirkulasi masuk cooling tower
CT Fraksinasi
Water blowdown (Wb)
2230.488 Kg/jam
26.24103 Kg/jam
13120.52 Kg/jam
15377.24 Kg/jam
15.37724477 M3/jam
ntuk karyawan = 40 liter/orang/hari
0,0085 Wc (T1-T2)
(Per. 12.10, Perry's, 1997)
Drift loss x Wc (Perrys hal 12-16 drift loss antara 0,1 Wc/2(S-1)
p air make up 3 5
CT Refenry 742
Water blowdown (Wb)
0,2 Perrys 1997)

,S adalah cycle
411.9534 Kg/jam
4.84651 Kg/jam
2423.255 Kg/jam
2840.055 Kg/jam 2.8401 M3/jam
CT Refenry 751
Water blowdown (Wb)
M3/jam
4.295095 Kg/jam
0.050531 Kg/jam
25.26527 Kg/jam
29.61089 Kg/jam
0.029611 M3/jam

Neraca Massa Fracination

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Neraca Massa Fracination

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Menghitung berat molekul rata rata triglserida

Membuat crude olein

Asam miristat (C14:0)c14h28o2

Massa masuk kristalizer

Neraca masuk HE 111

Neraca Panas masuk

Panas Steam yang dibutuhkan

531.9235996672 Kg/stegh jam

Neraca Panas KELUAR dengan pendin

s KELUAR dengan pendingin air pendingin

Membuat crude olein

Asam miristat (C14:0)c14h28o2

Massa masuk kristalizer

Neraca Panas masuk

Air pendingin masuk suhu 30

CPdT air masuk 30

M air yang dibutuhkan

728.1085467521 kmol /jam

Neraca Panas keluar saat menggunakan air chiller

Asam linoleat (C18:2) c18h32o2 (s)

Panas yang dibutuhkan dari peralihan air pendgin ke air chiller

282.7914375408 kmol /jam

Neraca Panas KELUAR dengan pendin

218.5970126 Ton air

s KELUAR dengan pendingin air pendingin

Pencairan bak stearin

Asam miristat (C14:0)c14h28o2

Massa masuk kristalizer

Neraca Panas masuk

Panas Steam yang dibutuhkan

Neraca Panas KELUAR dengan pendin

s KELUAR dengan pendingin air pendingin

Pencairan bak stearin

Asam miristat (C14:0)c14h28o2

Massa masuk kristalizer

Neraca Panas masuk

Neraca Panas KELUAR dengan pendingin air p

dengan pendingin air pendingin

23.99312943 25318.4 293909.3245

Pencairan bak stearin

Asam miristat (C14:0)c14h28o2

Massa masuk kristalizer

Neraca Panas masuk

Neraca Panas KELUAR dengan pendingin air p

dengan pendingin air pendingin

119.6057502 3948.89 225312.2519

Konsumsi Air pendingin

Konsumsi air pendingin

Air untuk karyawan kantor

Kebutuhan air untuk karyawan = 40 lit

data 50 ton /hari

= Drift loss x Wc (Perrys

Wc = aliran air sirkulasi masuk cooling tower

ntuk karyawan = 40 liter/orang/hari

(Per. 12.10, Perry's, 1997)

0,2 Perrys 1997)

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