Appendix A

FLOWCHART OF METHODOLOGY

Gathering of Materials

Preparation of Dye Solution

Preparation of Treatments

Application of Dye and Control

Gathering of Data

Statistical Analysis
 Appendix B

DUMMY TABLES

Table B1. Color of cloth after dye application

Setup Solution Numerical Observation

Equivalent

S0 15 More or less Orange-

Red
S1 3 More or less Orange-
1 Red
S2 9 More or less Orange-
Red
S3 13 More or less Orange-
Red
S4 17 Flesh-colored
S0 15 More or less Orange-
Red
S1 11 More or less Orange-
2 Red
S2 14 Light Cherry Red
S3 16 Light Rose Red
S4 17 Flesh-colored

Legend:
Table B2. Intensity of the dye based on the ratings of respondents

Treatments
Respondents
Setup 1 Setup 2

S0 S1 S2 S3 S4 S0 S1 S2 S3 S4

H1 2 2 2 1 3 3 3 2 2 3

H2 3 2 1 1 3 3 2 2 2 3

H3 3 3 2 1 3 3 3 2 2 3

H4 3 3 3 1 3 3 3 3 2 3

S1 2 2 1 1 3 3 3 3 2 3

S2 3 3 2 1 3 3 2 2 2 3

S3 3 3 2 1 3 3 3 2 2 3

T1 3 3 3 1 3 3 3 3 2 3

T2 3 3 3 1 3 3 3 3 3 3

D1 3 2 2 1 3 3 3 3 2 3

Legend:

Hn – Housewife
Sn – Student
Tn – Tailor
Dn – Designer
Ratings:

1 – Satisfactory Intensity
2 –Average Intensity
3 – Poor Intensity
Table B3. Color Fastness of dye after one week exposure to sunlight.

Day Setup Observations

1 The color remains the same.

1
2 The color remains the same.

1 S0R0 and S0R2 lighten while the other clothes’ color remains the
2 same.
2 The color remains the same.

1 The color remains the same except S0R1 and S0R2.

3
2 The color remains the same except for S0R0.

1 All the replicates of S0 lightens including S2R3 and S3R3.

4
2 The color remains the same except for S0R2.

1 All replicates of S0 lighten with S1R0, S1R3, S2R2, S2R3S3R2, and

5 S3R3.
2 The color remains the same except for S0R1 and S0R2.

1 All replicates of S1 and S2 lighten, with S3R2, S3R3, S0R1, and S0R2.
6
2 S0R0 lightens.

1 The clothes or replicates from S0 to S3

7
2 S1R1 lightens.
Table B4. Numerical Equivalent of Treated Fabric after one week exposure to sunlight.

Solutions Replicate Setup 1 Setup 2

DAY DAY
1 2 3 4 5 6 7 1 2 3 4 5 6 7
S0 S0R0 5 4 4 4 4 3 3 5 5 4 4 4 4 4
S0R1 5 5 4 4 4 4 3 5 5 5 5 4 4 4

S0R2 5 4 4 4 4 4 3 5 5 5 4 4 4 3

S1 S1R0 5 5 5 5 4 4 4 5 5 5 5 5 5 5

S1R1 5 5 5 5 5 4 4 5 5 5 5 5 5 4

S1R2 5 5 5 5 4 4 3 5 5 5 5 5 5 5

S2 S2R0 5 5 5 5 5 4 4 5 5 5 5 5 5 5

S2R1 5 5 5 5 4 4 4 5 5 5 5 5 5 5

S2R2 5 5 5 4 4 4 3 5 5 5 5 5 5 5

S3 S3R0 5 5 5 5 5 4 3 5 5 5 5 5 5 5

S3R1 5 5 5 5 4 4 3 5 5 5 5 5 5 5

S3R2 5 5 5 4 4 3 3 5 5 5 5 5 5 5

S4 S4R0 5 5 5 5 5 5 5 5 5 5 5 5 5 5

S4R1 5 5 5 5 5 5 5 5 5 5 5 5 5 5

S4R2 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Ratings:

5 – If there is no color change in the dyed cloth

4 – If there is only a small difference in color but a large amount of dye color still
remains.
3 – If a lot of dye color was removed but there is still a significant amount of dye
color left.
2 – If the color of the cloth is distinctly light and very little dye color is left
1 – If the dye is completely removed from the cloth
Table B4. Water fastness of treated fabric after being immersed to water.

Solutions Replicate Setup 1 Setup 2

S0 S0R0 A small amount of dye remained on The color remains the same
the dyed fabric. and no stain was created.
S0R1 Only a small amount of dye The color remains the same
remained. and no stain was created.
S0R2 Only a light color of the dye The color remains the same
remained and the others were and no stain was created.
removed in water.
S1 S1R1 The undyed fabric was stained. The color remains the same
and no stain was created.
S1R2 The dyed fabric became lighter and The color remains the same
stains were created on the undyed and no stain was created.
fabric.
S1R3 When immersed with water, the dye The color remains the same
came off and caused a stain. and no stain was created.
S2 S2R1 Small amount of stain was created The color remains the same
however the dyed fabric became and no stain was created.
much lighter.
S2R2 A large amount of the dye color was The color remains the same
removed. and no stain was created.

S2R3 The dyed fabric became lighter and The color remains the same
there were stains on the undyed and no stain was created.
fabric.
S3 S3R1 A lot of the dye was removed in the The color remains the same
water and some dye caused a stain and no stain was created.
on the undyed fabric.
S3R2 A lot of stain was created on the The color remains the same
undyed fabric and a small amount of and no stain was created.
dye remained.
S3R3 A lot of the dye color was removed The color remains the same
when immersed with water and and no stain was created.
caused stain to the undyed fabric.
S4 S4R1 The color remains the same and no The color remains the same
stain was created. and no stain was created.
S4R2 The color remains the same and no The color remains the same
stain was created.. and no stain was created.
S4R3 The color remains the same and no The color remains the same
stain was created. and no stain was created.
Table B5. Numerical Equivalent of Water Fastness of treated fabric.

Solutions Replicate Setup 1 Setup 2

S0 S0R0 4 5
S0R1 4 5
S0R2 4 5
S1 S1R1 3 5
S1R2 4 5
S1R3 3 5
S2 S2R1 3 5
S2R2 3 5

S2R3 3 5
S3 S3R1 3 5
S3R2 2 5

S3R3 2 5
S4 S4R1 5 5
S4R2 5 5
S4R3 5 5

Ratings:

5 – If there is no color change in the dyed cloth

4 – If there is only a small difference in color but a large amount of dye color still
remains.
3 – If a lot of dye color was removed but there is still a significant amount of dye
color left.
2 – If the color of the cloth is distinctly light and very little dye color is left
1 – If the dye is completely removed from the cloth
Table B6. Color Fastness of fabric after applying chlorine and detergent.

Solutions Replicate Setup 1 Setup 2

Chlorine Detergent Chlorine Detergent
S0 S0R0 2 3 3 3
S0R1 1 4 2 4
S0R2 2 3 2 4
S1 S1R1 3 4 5 5
S1R2 3 4 5 5
S1R3 3 3 5 5
S2 S2R1 3 3 5 5
S2R2 3 4 5 5

S2R3 2 3 5 5
S3 S3R1 2 3 5 5
S3R2 2 2 5 5

S3R3 2 2 5 5
S4 S4R1 1 1 5 5
S4R2 1 1 5 5
S4R3 1 1 5 5

Ratings:

5 – If there is no color change in the dyed cloth

4 – If there is only a small difference in color but a large amount of dye color still
remains.
3 – If a lot of dye color was removed but there is still a significant amount of dye
color left.
2 – If the color of the cloth is distinctly light and very little dye color is left
1 – If the dye is completely removed from the cloth
 Appendix C

Table C1. Budget Plan

Material Quantity Cost Per Unit Source Total Cost

Greige Cloth Five (5) meters 20.00 pesos PTRI 100.00

Red Banana Six (6) kilograms 30.00 pesos Toril, Davao City 180.00

Mordant .5 liters 50.00 pesos PTRI 25.00

Distilled Water Two (2) liters 33.00 pesos Toril, Davao City 100.00

Assume Total: 405. 00 PHP

 Appendix D

Table D1. Time table of activities

Activity Time Allotment Date

Identification of the Eight (8) hours June 18, 2011

research problem
Title Defense Fifteen (15) minutes June 22, 2011

Draft of Chapter 1 Two (2) hours and thirty June 4 – June 11, 2011
(30) minutes

Submission of Chapter 1 One (1) day July 15, 2011

Preparation of Chapter 2 Five (5) days July 16 – 21, 2011

Submission of Chapter 2 One (1) day July 22, 2011

Revision of Chapter 1 and Seven (7) days July 25 – July 31, 2011
2, title page and certificate
of approval
Submission of the final One (1) day August 1, 2011
draft of chapter 1 and 2,
title page and certificate of
approval
Preparation of Chapter 3, Eight (8) days August 15 – 22, 2011
Preliminaries, Appendices
and Bibliography
Submission of Chapter 3, One (1) day August 23, 2011
Preliminaries, Appendices
and Bibliography
Experimentation One (1) week May 1 – May 8, 2012

Gathering of Data One (1) day May 9, 2012

 Appendix E

RISK ASSESSMENT

The only chemical used in this research is the mordant red iron (III) oxide.

According to Physical & Theoretical Chemistry Lab (2005), this substance is

synonymous to the black oxide of iron, English red, and ochre. It appears red to reddish-

brown powder, with a melting point of 1565 oC and specific gravity of 5.24. It is a stable

substance, although its dust may act as an irritant. It is non-hazardous for air, sea, and

road freight. For personal protection, it is advised to use safety goggles when using.