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    Iodine Value Determination Porim Test Method

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    Adawiyah Ali
    This document provides a standard operating procedure for determining the iodine value of test materials using manual titration. It outlines the responsibilities of personnel, applicable references and standards, required materials and equipment, health and safety considerations, documentation, and step-by-step procedures. The iodine value is a measure of the degree of unsaturation in fatty acids and is calculated based on the titration of a sample with sodium thiosulfate solution.

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    Iodine Value Determination Porim Test Method

    Uploaded by

    Adawiyah Ali
    387 views2 pages
    This document provides a standard operating procedure for determining the iodine value of test materials using manual titration. It outlines the responsibilities of personnel, applicable references and standards, required materials and equipment, health and safety considerations, documentation, and step-by-step procedures. The iodine value is a measure of the degree of unsaturation in fatty acids and is calculated based on the titration of a sample with sodium thiosulfate solution.

    Original Description:

    PORIM Test Method (1995). Test method p3.2

    Original Title

    IODINE VALUE DETERMINATION PORIM TEST METHOD

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    This document provides a standard operating procedure for determining the iodine value of test materials using manual titration. It outlines the responsibilities of personnel, applicable references and standards, required materials and equipment, health and safety considerations, documentation, and step-by-step procedures. The iodine value is a measure of the degree of unsaturation in fatty acids and is calculated based on the titration of a sample with sodium thiosulfate solution.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    387 views2 pages

    Iodine Value Determination Porim Test Method

    Uploaded by

    Adawiyah Ali
    This document provides a standard operating procedure for determining the iodine value of test materials using manual titration. It outlines the responsibilities of personnel, applicable references and standards, required materials and equipment, health and safety considerations, documentation, and step-by-step procedures. The iodine value is a measure of the degree of unsaturation in fatty acids and is calculated based on the titration of a sample with sodium thiosulfate solution.

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    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    of 2

    MENA JAYA OIL & FATS SDN. BHD.

    IODINE VALUE
    Method : Manual Titration
    1

    1.0 PURPOSE
    To check iodine value of test materials using manual titration

    2.0 RESPONSIBILITY
    2.1 Chemist is responsible to ensure the personnel are appropriately trained.
    2.2 QC personnel is responsible to perform iodine value determination and generate test
    report when is required.
    2.3 Manager is responsible to review reports / verification report generated by QC personnel.

    3.0 REFERENCES AND APPLICABLE DOCUMENTS

    3.1 PORIM Test Method (1995). Test method p3.2


    3.2 MPOB Test Methods p3.2:2004
    3.3 ISO 3961:1996

    4.0 MATERIALS AND EQUIPMENTS


    4.1 Test sample
    4.2 100 g L-1 potassium iodide
    4.3 Cyclohexane
    4.4 Wijs Solution
    4.5 0.1N Sodium thiosulphate

    5.0 HEALTH AND SAFETY CONSIDERATIONS

    5.1 Wear and use appropriate Personnel Protective Equipment when handle test materials

    5.2 Solutions very hazardous in case of skin contact (corrosive, irritator) of eye contact
    (corrosive), of ingestion, of inhalation (fatal), may cause damage to organs through
    prolonged and repeated exposure.

    Effective date Doc No : SOP for Iodine Value


    28th August 2018
    Written by : Checked by : Approved by : Page 1 of ____
    Adawiyah Ali
    6.0 DOCUMENTATION REQUIREMENTS

    6.1 Log Book


    6.2 QC report / COA

    7.0 PROCEDURES
    7.1 Weight ~0.2-0.5 g of sample and put into a 250 mL flask.
    7.2 Add 20 mL cyclohexane to dissolve the sample. Warm the flask slightly if necessary.
    7.3 Add 25 mL Wijs solution, insert a stopper, shake gently and placed in the dark for 1 hour.
    7.4 Add 20 mL of 100 g L-1 potassium iodide (Weigh 5 g KI, dissolve in to 50 mL water) and
    100 mL distilled water.
    7.5 Titrate with sodium thiosulphate solution until yellow iodine colour almost disappeared.
    7.6 Add 1-2 mL starch indicator, shake vigorously until blue colour disappear. Repeat the
    same for blank with no sample added.
    Iodine value = [12.69N(V2 –V1)]/W
    N = normality of sodium thiosulphate (Na2S2O3)
    V2 = volume of Na2S2O3 solution used for blank
    V1 = volume of Na2S2O3 solution used for sample
    W = weight of sample in gram (g)

    8.0 CARE AND MAINTENANCE


    8.1 Keep away the solvents from heat/spark/open flames/hot surfaces.2

    8.2 In case of skin contact, remove/take off immediately all contaminated clothing
    and rinse skin with water/shower. In case of eye contact, remove contact lenses (if
    present) and rinse cautiously with water for several minutes.

    8.3 Dispose of waste to an appropriate treatment and disposal facility.

    Effective date Doc No : SOP for Iodine Value


    28th Aug 2018
    Written by : Checked by : Approved by : Page 4 of ____
    Adawiyah Ali

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