DATA SHEET OF TCLP SLUDGE TESTING

ENVIRONMENT LABORATORY OF PT.SUCOFINDO

FOR/ENV-LP/02-01
No. Lab : LSB/7103/10-102-05/000011/09/2020-1
Mark of Sample : GYPSUM
Tgl. Terima : 18/09/2020
Tgl. Selesai : 05/10/2020
Acuan : TCLP-PPRI No. 101/2014 LAMPIRAN III (Anorganik)

No. Lab 000011/1 000002+R11:AG97/2 000002/3

Pengujian Simplo Duplo Simplo Duplo Simplo Duplo
Arsenic, mg/L
Pembacaan AAS -0.42 -0.42 -0.34 -0.34 0.12 0.12
Blanko 0.00 0.00 0.00 0.00 0.00 0.00
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi As -0.001 -0.001 -0.001 -0.001 0.0005 0.0005
Rata-rata -0.001 -0.001 0.0005
% RPD 0.0% 0.0% 0.0%
Hasil Akhir < 0.0003 < 0.0003 < 0.001
Barium, mg/L
Pembacaan ICP-OES 0.1886 0.1892 0.7266 0.7384 0.6452 0.6542
Blanko 0.0004 0.0004 0.0004 0.0004 0.0004 0.0004
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi Ba 0.38 0.38 1.5 1.5 2.58 2.62
Rata-rata 0.38 1.5 2.5972
% RPD 0.3% 1.6% 1.4%
Hasil Akhir 0.38 1.5 2.60
Boron, mg/L
Absorbansi 0.809 0.820 0.000 0.000 0.049 0.049
Intercept 0.0376 0.0376 0.0376 0.0376 0.0376 0.0376
Slope 0.0381 0.0381 0.0381 0.0381 0.0381 0.0381
Pengenceran 2 2 2 2 2 2
Kadar Boron 40.466 41.043 -1.972 -1.972 0.5716 0.5978
Rata-rata 40.75 -1.97 0.585
% RPD 1.4% 0.0% 4.5%
Hasil Akhir 40.75 < 0.10 0.58
Boron ,mg/L
Pembacaan ICP-OES 0.4558 0.4657 0.7559 0.7601 0.5643 0.5015
Blanko 0.0404 0.0404 0.0404 0.0404 0.0404 0.0404
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi B 0.83 0.85 1.43 1.44 2.096 1.844
Rata-rata 0.84 1.44 1.9700
% RPD 2.36% 0.59% 12.75%
Hasil Akhir 0.84 1.44 1.97
Cadmium ,mg/L
Pembacaan ICP-OES -0.0037 -0.0036 -0.0014 -0.0014 0.0007 0.0007
Blanko 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi Cd -0.0074 -0.0072 -0.003 -0.003 0.003 0.003
Rata-rata -0.0073 -0.003 0.0028
% RPD 2.74% 0.00% 0.00%
Hasil Akhir < 0.06 < 0.06 < 0.06
Chromium, mg/L
Pembacaan ICP-OES 0.0034 0.0033 0.0019 0.0019 0.0071 0.0074
Blanko 0.0011 0.0011 0.0011 0.0011 0.0011 0.0011
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi Cr 0.005 0.004 0.002 0.002 0.02 0.03
Rata-rata 0.005 0.002 0.0246
% RPD 4.4% 0.0% 4.9%
Hasil Akhir < 0.10 < 0.10 < 0.10
Copper, mg/L
Pembacaan ICP-OES 0.1057 0.1075 0.0035 0.0034 0.0028 0.0029
Blanko 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi Cu 0.21 0.22 0.007 0.007 0.01 0.01
Rata-rata 0.21 0.007 0.0114
% RPD 1.7% 2.9% 3.5%
Hasil Akhir 0.21 < 0.06 < 0.06
Cyanide, mg/L
Absorbansi 0.000 0.000 0.000 0.000 0.000 0.000
Intercept -0.0021 -0.0021 -0.0021 -0.0021 -0.0021 -0.0021
Slope 2.6680 2.6680 2.6680 2.6680 2.6680 2.6680
Pengenceran 1 1 1 1 1 1
Kadar Cyanide 0.001 0.001 0.001 0.001 0.0008 0.0008
Rata-rata 0.001 0.001 0.001
% RPD 0.0% 0.0% 0.0%
Hasil Akhir < 0.03 < 0.03 < 0.03
Flouride, mg/L
Absorbansi 0.389 0.388 0.477 0.478 0.546 0.547
Blanko 0.502 0.502 0.502 0.502 0.499 0.502
Intercept 0.0005 0.0005 0.0005 0.0005 0.0005 0.0005
Slope 0.1511 0.1511 0.1511 0.1511 0.1511 0.1511
Pengenceran 10 10 10 10 1 10
Kadar Flouride 7.4 7.5 1.6 1.6 -0.314 -3.010
Rata-rata 7.5 1.6 -1.6622
% RPD 0.9% 4.2% 162.2%
Hasil Akhir 7.5 1.6 < 0.07
Lead ,mg/L
Pembacaan ICP-OES -0.0016 -0.0016 0.0037 0.0036 -0.0255 -0.0256
Blanko 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi Pb -0.003 -0.003 0.007 0.007 -0.102 -0.102
Rata-rata -0.003 0.007 -0.1022
% RPD 0.0% 2.7% 0.4%
Hasil Akhir < 0.07 < 0.07 < 0.07
Mercury, mg/L
Pembacaan AAS 0.81 0.81 0.57 0.57 0.13 0.13
Blanko 0.83 0.83 0.83 0.83 0.83 0.83
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi Hg 0.0000 0.0000 -0.0005 -0.0005 0.000 0.000
Rata-rata 0.0000 -0.0005 0.0000
% RPD 0.0% 0.0% 0.0%
Hasil Akhir < 0.0003 < 0.0003 < 0.002
Nitrate, mg/L
Absorbansi 0.386 0.387 0.200 0.199 0.343 0.345
Intercept 0.0121 0.0121 0.0121 0.0121 0.0121 0.0121
Slope 0.5556 0.5556 0.5556 0.5556 0.5556 0.5556
Pengenceran 10 10 10 10 10 10
Kadar Nitrate 6.7 6.7 3.4 3.4 5.955 5.991
Rata-rata 6.7 3.4 5.9735
% RPD 0.3% 0.5% 0.6%
Hasil Akhir 6.7 3.4 5.97
Nitrite, mg/L
Absorbansi 0.019 0.019 0.015 0.015 0.027 0.025
Intercept 0.0028 0.0028 0.0028 0.0028 0.0028 0.0028
Slope 2.9179 2.9179 2.9179 2.9179 2.9179 2.9179
Pengenceran 1 1 1 1 1 1
Kadar Nitrate 0.006 0.006 0.004 0.004 0.008 0.008
Rata-rata 0.006 0.004 0.0080
% RPD 0.0% 0.0% 8.6%
Hasil Akhir < 0.03 < 0.03 < 0.03
Nitrate+ Nitrite, mg/L
Kadar Nitrate 6.729 6.747 3.382 3.364 5.955 5.991
Kadar Nitrite 0.006 0.006 0.004 0.004 0.008 0.008
Kadar Nitrate + Nitrite 6.735 6.753 3.386 3.368 5.964 5.999
Rata-rata 6.7 3.4 5.981
% RPD 0.3% 0.5% 0.6%
Hasil Akhir 6.7 3.4 5.98
Selenium, mg/L
Pembacaan AAS 0.0 0.0 0.0 0.0 0.2 0.2
Blanko -0.1 -0.1 -0.1 -0.1 -0.1 -0.1
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi Se 0.0002 0.0002 0.0002 0.0002 0.000 0.000
Rata-rata 0.0002 0.0002 0.000
% RPD 0.0% 0.0% 0.0%
Hasil Akhir < 0.0003 < 0.0003 < 0.001
Silver, mg/L
Pembacaan ICP-OES 0.0124 0.0121 -0.0022 -0.0021 0.0035 0.0036
Blanko 0.1480 0.1480 0.1480 0.1480 0.1480 0.1480
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi Ag -0.27 -0.27 -0.300 -0.300 -0.578 -0.578
Rata-rata -0.27 -0.300 -0.5778
% RPD 0.2% 0.1% 0.1%
Hasil Akhir < 0.10 < 0.10 < 0.10
Zink, mg/L
Pembacaan ICP-OES 0.5181 0.5190 0.5188 0.5191 0.3131 0.3124
Blanko 0.0103 0.0103 0.0103 0.0103 0.0103 0.0103
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi Zn 1.02 1.02 1.02 1.02 1.211 1.208
Rata-rata 1.02 1.02 1.210
% RPD 0.2% 0.1% 0.2%
Hasil Akhir 1.02 1.02 1.21
Antimony ,mg/L
Pembacaan ICP-OES 0.0053 0.0054 0.0231 0.0238 -0.0159 -0.0156
Blanko 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi Sb 0.011 0.011 0.046 0.048 -0.064 -0.062
Rata-rata 0.011 0.047 -0.0630
% RPD 1.87% 2.99% 1.90%
Hasil Akhir < 0.10 < 0.10 < 0.10
Berrilium, mg/L
Pembacaan ICP-OES -0.0001 -0.0001 -0.0001 -0.0001 -0.0001 -0.0001
Blanko 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi Be -0.0002 -0.0002 -0.0002 -0.0002 0.00 0.00
Rata-rata -0.0002 -0.0002 -0.0004
% RPD 0.0% 0.0% 0.0%
Hasil Akhir < 0.0027 < 0.0027 < 0.0027
Molibdenum, mg/L
Pembacaan ICP-OES -0.0023 -0.0022 -0.0056 -0.0054 0.0721 0.0742
Blanko 0.0081 0.0081 0.0081 0.0081 0.0081 0.0081
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi Mo -0.021 -0.021 -0.03 -0.03 0.26 0.26
Rata-rata -0.021 -0.03 0.2602
% RPD 1.0% 1.5% 3.2%
Hasil Akhir < 0.037 < 0.037 0.26
Nikel ,mg/L
Pembacaan ICP-OES -0.0018 -0.0018 0.0088 0.0086 0.0146 0.0161
Blanko 0.0000 0.0000 0.0000 0.0000 0.0000 0.0000
Volume Labu (ml) 100 100 100 100 100 100
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 2 2 2 2 2 2
Konsentrasi Ni -0.004 -0.004 0.018 0.017 0.058 0.064
Rata-rata -0.004 0.017 0.0614
% RPD 0.00% 2.30% 9.77%
Hasil Akhir < 0.10 < 0.10 < 0.10
Chromium Hexavalent, mg/L
Absorbansi 0.005 0.005 0.001 0.001 0.017 0.018
Intercept 0.0014 0.0014 0.0014 0.0014 0.0014 0.0014
Slope 0.7984 0.7984 0.7984 0.7984 0.7984 0.7984
Pengenceran 2 2 2 2 10 10
Kadar Cr6+ 0.009 0.009 -0.001 -0.001 0.195 0.208
Rata-rata 0.009 -0.001 0.2017
% RPD 0.0% 0.0% 6.2%
Hasil Akhir 0.009 < 0.004 0.20
Chloride, mg/kg
Titran Sampel 0.8 0.8 0.4 0.4 0.3 0.3
Titran Blanko 0.7 0.7 0.7 0.7 0.7 0.7
Normalitas AgNO3 0.014 0.014 0.014 0.014 0.0140 0.0140
Konstanta (BM Cl) 40 40 40 40 40 40
Vol. contoh (ml) 50 50 50 50 50 50
Pengenceran 10 10 2 2 10 10
Kadar Cl 11.2 11.2 -6.7 -6.7 -44.80 -44.80
Rata-rata 11.2 -6.7 < 5.0
% RPD 0.0% 0.0% #VALUE!
Hasil Akhir 11.2 < 0.004 -44.80

Analyzed by: Approved by: