PENGUJIAN KADAR NO3 DAN KETIDAKPASTIAN DALAM AIR & AIR LIMBAH MENGGUNAKAN FLOW

INJECTION ANALYZER
Laboratorium Penguji
LP-739-IDN
Parameter : NO3 Metode : IKM.SKY-160 (Flow Injection Analysis)
Tanggal : 11/23/2021 Rentang Metode : 0,01 - 0,2 mg/L

n Kadar Abs Validasi Metode NO3

1 0.000 0.0027 Kurva Kalibrasi NO3 %R 97.94 %
2 0.010 0.0201 0.3500 sd 0.50 %
3 0.050 0.0797 0.3000 %R uji 102.40 %
f(x) = 1.50103448275862 x + 0.00436551724137931
4 0.100 0.1560 0.2500 R² = 0.999892156978179 U %R 0.52
5 0.200 0.3037 %RPD 0.00 %

Absorbansi
0.2000
6 U %RPD 0.00
0.1500
7
Jumlah 0.360 0.5622 0.1000
Rerata 0.072 0.1124 0.0500
Slope 1.501 0.0000
Intercept 0.0044 0.000 0.050 0.100 0.150 0.200 0.250
sd residual 0.0015 Konsentrasi
(mg/L)
 ( xi x ) 2 0.027

Laporan
Job No. Kadar NO3 (mg/L) U hasil U gab NO3 (%)
Kadar ± U95% (%)
21111346-1 0.0557 0.00081 1.54 0.06 ± 3.08 Analis Diverifikasi
21111346-1r 0.0556 0.00081 1.54 0.06 ± 3.08

…............ Yuthika Rizki N.

Sumber Ketidakpastian Faktor Pengenceran Laporan

Kadar NO3
Kadar NO3 U gab NO3
Job. No Pipet volume Labu Ukur Fp (dari alat) U hasil
(mg/L) (%) Kadar ± U95% (%)
(mg/L)
Vol U95% Kor Vol. Kor t°C kal t°C uji Koef. Muai U Pipet Vol U95% k Kor Vol. Kor t°C kal t°C uji Koef. Muai U Labu Ukur
10 0.02 0.01 9.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 10 0.10 1.000 #REF! #REF! 1.0000 ± #REF!
2 0.02 0.01 1.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 50 0.08 4.000 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.12 2.400 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.09 1.800 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.10 2.000 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.12 2.400 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.02 0.400 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.12 2.400 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.15 3.000 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.11 2.200 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.09 1.800 #REF! #REF!
 PENGUJIAN KADAR NH3 DAN KETIDAKPASTIAN DALAM AIR & AIR LIMBAH MENGGUNAKAN FLOW
INJECTION ANALYZER
Laboratorium Penguji
LP-739-IDN
Parameter : NH3 Metode : IKM.SKY-160 (Flow Injection Analysis)
Tanggal : 12/6/2021 Rentang Metode : 0,01 - 0,2 mg/L

n Kadar Abs Validasi Metode NO3

1 0.000 0.0000 Kurva Kalibrasi NH3 %R 97.94 %
2 0.050 0.0163 0.2500 sd 0.50 %
3 0.200 0.0558 %R uji 102.30 %
0.2000 f(x) = 0.271485781990521 x + 0.00110912322274881
4 0.400 0.1083 R² = 0.999800047950193 U %R 0.52
5 0.800 0.2188 0.1500 %RPD 0.43 %

Absorbansi
6 U %RPD 0.38
7 0.1000
Jumlah 1.450 0.3992
0.0500
Rerata 0.290 0.0798
Slope 0.271 0.0000
Intercept 0.0011 0.000 0.100 0.200 0.300 0.400 0.500 0.600 0.700 0.800 0.900
sd residual 0.0014 Konsentrasi
(mg/L)
 ( xi x ) 2 0.422

Laporan
Job No. Kadar NH3 (mg/L) U hasil U gab NH3 (%)
Kadar ± U95% (%)
21111346-1 1.2239 0.00877 0.96 1.22 ± 1.93 Analis Diverifikasi
21111346-1rea 1.5559 0.01121 0.97 1.56 ± 1.93

…............ Yuthika Rizki N.

Sumber Ketidakpastian Faktor Pengenceran Laporan

Kadar NO3
Kadar NO3 U gab NO3
Job. No Pipet volume Labu Ukur Fp (dari alat) U hasil
(mg/L) (%) Kadar ± U95% (%)
(mg/L)
Vol U95% Kor Vol. Kor t°C kal t°C uji Koef. Muai U Pipet Vol U95% k Kor Vol. Kor t°C kal t°C uji Koef. Muai U Labu Ukur
10 0.02 0.01 9.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 10 0.10 1.000 #REF! #REF! 1.0000 ± #REF!
2 0.02 0.01 1.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 50 0.08 4.000 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.12 2.400 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.09 1.800 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.10 2.000 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.12 2.400 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.02 0.400 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.12 2.400 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.15 3.000 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.11 2.200 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.09 1.800 #REF! #REF!
 PENGUJIAN KADAR FENOL DAN KETIDAKPASTIAN DALAM AIR & AIR LIMBAH MENGGUNAKAN FLOW
INJECTION ANALYZER
Laboratorium Penguji
LP-739-IDN
Parameter : NH3 Metode : IKM.SKY-160 (Flow Injection Analysis)
Tanggal : 12/6/2021 Rentang Metode : 0,01 - 0,2 mg/L

n Kadar Abs Validasi Metode NO3

1 0.000 0.0005 Kurva Kalibrasi Fenol %R 97.94 %
2 0.008 0.0031 0.0180 sd 0.50 %
3 0.025 0.0087 0.0160 f(x) = 0.326214419635248 x + 0.000506050792568605 %R uji 96.29 %
0.0140 R² = 0.999986830687757
4 0.050 0.0168 U %R 0.49
0.0120
5 %RPD 0.00 %

Absorbansi
0.0100
6 U %RPD 0.00
0.0080
7
0.0060
Jumlah 0.083 0.0291
0.0040
Rerata 0.021 0.0073
0.0020
Slope 0.326 0.0000
Intercept 0.0005 0.000 0.010 0.020 0.030 0.040 0.050 0.060
sd residual 0.0000 Konsentrasi
(mg/L)
 ( xi x ) 2 0.001

Laporan
Job No. Kadar Fenol (mg/L) U hasil U gab Fenol (%)
Kadar ± U95% (%)
21111346-1 0.0080 0.00009 1.19 0.01 ± 2.38 Analis Diverifikasi
21111346-1r 0.0080 0.00009 1.19 0.01 ± 2.38

…............ Yuthika Rizki N.

Sumber Ketidakpastian Faktor Pengenceran Laporan

Kadar NO3
Kadar NO3 U gab NO3
Job. No Pipet volume Labu Ukur Fp (dari alat) U hasil
(mg/L) (%) Kadar ± U95% (%)
(mg/L)
Vol U95% Kor Vol. Kor t°C kal t°C uji Koef. Muai U Pipet Vol U95% k Kor Vol. Kor t°C kal t°C uji Koef. Muai U Labu Ukur
10 0.02 0.01 9.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 10 0.10 1.000 #REF! #REF! 1.0000 ± #REF!
2 0.02 0.01 1.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 50 0.08 4.000 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.12 2.400 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.09 1.800 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.10 2.000 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.12 2.400 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.02 0.400 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.12 2.400 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.15 3.000 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.11 2.200 #REF! #REF!
5 0.02 0.01 4.99 20 25 0.00021 #REF! 100 0.02 1.96 0.01 99.99 20 25 0.00021 0.061 20 0.09 1.800 #REF! #REF!