Dynamic Failure of Metallic Cellular Materials

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DYNAMIC FAILURE OF METALLIC CELLULAR MATERIALS

S. LEE and H.D. ESPINOSA


Department of Mechanical Engineering, Northwestern University, Evanston, IL 60208-3111, USA.

ABSTRACT
The quasi-static and dynamic compressive behavior of open-cell foams, textile cores, and pyramidal truss
cores were investigated using a combination of experimental apparatus. Quasi-static tests were performed
using a miniature loading stage and a Kolsky bar apparatus was used for intermediate deformation rates. For
high deformation rates, a gas gun was employed. Optical observations of the sample deformation were
performed in real time by means of high-speed photography. The deformation modes were investigated in
detail from acquired images and digital image correlation. For the open cell foams, comparison between
deformation fields under quasi-static and Kolsky bar loading revealed a moderate micro-inertia effect, where
the inertia associated to the bending and buckling of ligaments delayed strain localization. Gas gun
experiments performed on the same samples revealed a totally different deformation mode. A crashing shock
wave was generated at the impact surface and propagated through the specimen. In these experiments both
forward and reverse impact tests were performed to interrogate the state of stress in front and behind the
shock wave front. Through these experiments, it was confirmed that the generation and propagation of shock
waves within foam materials greatly enhance their energy absorption. For the case of textile cores, the
mechanical response was found to be similar to the open cell foam materials. No significant difference in
load-deformation histories and failure modes were observed between quasi-static and intermediate
deformation rates. As in the case of open cell foams, at high deformation rates, the failure mode was governed
by the development of a crushing shock wave. For the truss cores, significant deformation rate effects on peak
stress and energy absorption were identified. Inertia effects appeared to dominate the core response because of
two effects: i) the propagation of a plastic wave along the truss members, and ii) buckling induced lateral
motion. In this article we provide a quantification of load-deformation response and associated failure modes
across the sample as captured by high speed photography and image correlation.

1 INTRODUCTION
Materials combining light-weight and mechanical energy absorption are of primary interest in the
protection design in automotive, locomotive, naval structures, and aerospace. Metallic cellular
materials have been promising and attracting in many applications [1]. These materials offer low
densities and are highly efficient in absorbing mechanical energy from external loading. Exploiting
minimum weight design, material fabrication, structural integrity, dynamic experiments, and large-
scale simulations, dramatic improvements can be made in the design of cellular materials
exhibiting periodic cellular topologies.
Major contributions have been recently made in the mechanical characterization of foams
materials at high rates of deformation. Reid and Peng [2] observed an increase of strength for
higher deformation rates on cellular structures. On the other hand, Deshpande and Fleck [3] did not
observe any rate dependency for the crashing stress of aluminum foams. These discrepancies from
different experiments might be explained by failure and deformation mode transition such as the
formation of shock waves within the specimen at very high strain rates. A model for shock waves
in closed cell aluminum foams was proposed by Reid and co-workers [4]. It is shown in this model
that the stress in the sample is not homogeneous and that therefore the measured stress is
dependent on which end of the sample the data is recorded experimentally. Another potential
source of rate dependency is micro-inertia which has been hypothesized and modeled but not
directly observed on foam materials.
Previous studies on the behavior of cellular materials have been mainly performed on foam
materials with randomly shaped and distributed cells. Newly proposed approaches utilize metallic
core materials which are topologically-structured at small scale. Metallic woven textile materials
were first developed by Sypeck and Wadley [5]. Theoretical and numerical analysis on the textile
cores were performed and design optimization was pursued by Zok et al. [6]. Quasi-static
compression, shear, and bending experiments were carried out on the textile cores by Mumm et al.
[7]. Another new cellular material following similar manufacturing ideas is the so-called truss core.
Truss cores with tetragonal and pyramidal topologies were theoretically studied by Wicks and
Hutchinson [8]. They were predicted to offer the best combination of compressive strength and low
weight. Experimental measurements and numerical simulations were performed to validate this
prediction by Chiras et al. [9]. Whereas these truss cores were studied theoretically and
numerically, limited experimental data was reported and the performed experiments were limited
to quasi-static loading.
This article presents results from experiments on aluminum open cell foam, stainless steel
textile core, and stainless steel pyramidal truss cores at three different deformation rates. Quasi-
static tests were performed on a sub-miniature loading frame, intermediate strain rate tests were
performed on a stored energy Kolsky bar, and high strain rate compression tests were performed
using a light gas gun. In addition to compressive stress-strain curves at various strain rates, real-
time observations were made in all tests by means of high speed digital imaging. Correlation
techniques were used to reveal the mode of deformations and failure for the cellular materials. The
results are compared for all the explored deformation rates. In addition, dynamic failure modes of
textile and truss cores are reported as well as the measured load-deformation behaviors at different
deformation rates.

2 ALUMINUM FOAM MATERIALS


2.1 Materials
The specimens were Duocel 6101-T6 Aluminium alloy foam with open cell architecture. The
average cell size was 0.5 mm and the specimens had 7% relative density. The dimensions of the
specimens were 25.4 mm × 17.78 mm × 17.78 mm.

2.2 Response at different deformation rates


Fig. 1 shows curves of nominal stress (F/A0) versus nominal strain (δ/L0) for quasi-static and
dynamic compression tests on the Aluminum foam material. The deformation rates were 7×10-3 s-1
for the quasi-static case, ~250 s-1 for the Kolsky bar and 2500~3300 s-1 for the gas gun. The gas
gun experiment was performed using the forward
configuration, i.e., the specimen is attached to a
transmission bar and it is impacted by a lunched
bar. Details of the experimental set ups are given
in [10]. Examination of the stress-strain lots
reveals that the deformation rate seems to have no
effect on the plateau stress of about 2.5 MPa
throughout the explored strain rates. The
densification occurs at a nominal strain of about
60%. The gas gun experiments show a stiffer
densification response during the final crushing
stages. This is connected to the arrival of the
Figure 1: Stress-strain curves of compression crashing front to the transmission bar as will be
of Al foam at different strain rates. discussed later in the context of the formation of a
crashing shock wave in the sample.
Although the deformation rate does not seem to have an effect on the overall compressive
behavior, it seems to control the cells local deformation and failure modes. Fig. 2 shows snapshots
of the specimen for quasi-static and Kolsky bar tests with superimposed x-direction strain fields
obtained by digital image correlation. The images show that the overall nominal deformation in the
dynamic case is more distributed than in the quasi-static case in which cell collapse is concentrated
in one or two bands. The large deformations leading to cell crushing involve significant motion of
material through bending and buckling of cell walls and ligaments. At high deformation rates, this
motion results in a micro-inertia effect, and the result is that it takes more force and time to crush
the cells. This phenomenon did not manifested itself in an appreciable increase in nominal crashing
stress but the DIC analysis clearly shows that at intermediate strain rates the specimen seems to
offer more resistance to strain localization. Fig. 3 shows a failure mode comparison between quasi-
static and gas gun experiments. The stress was measured in the back side of the sample (forward
impact configuration). As observed in the images, a major change in failure mode occurs with the
development of a shock wave at high enough strain rates. The foam collapse produces a shock
front perpendicular to the loading axis. This front propagates along the impact direction with a
specific velocity [10]. In order to measure the stress behind the crushing shock front, a reverse
impact experiment was performed.
δ/L0: 0.004 0.012 0.029 0.039 0.056 0.073 0.083

Figure 2: Differences in local deformations during quasi-static and Kolsky bar experiments.

δ/L0: 0.253 0.333 0.414 0.498 0.579 0.660 0.744

Figure 3: Different failure modes of deformations in comparison of quasi-static and gas gun experiments.
10.0
9.0
Forward Impact, 3279 1/s 2.3 Reverse impact experiments
8.0
Reverse Impact, 3472 1/s In a reverse impact test, the specimen is
7.0 launched with the striking bar. As a result,
6.0 the transmitter bar records the loads behind
F/A0 , MPa

5.0 the shock front initiated from the impact


4.0
surface. It implies that the reverse impact test
3.0
measures the crushing load while the forward
2.0
1.0
impact test measures the load transmitted
0.0 through the core. A comparison between
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 forward and reverse impact results is shown
δ /L 0
in the Fig. 4. The average of load measured
Figure 4: Comparison between reverse and forward
impact test results in gas gun experiments.
in reverse impact is higher than that of the forward impact and consistent with theoretical
predictions [4, 10]. Considering the fact that these two tests were carried out at almost the same
strain rate, it can be concluded that the crushing load is higher than the load transmitted through
the foam at high speeds of deformation. The fluctuations in the reverse impact test seem to be the
result of local instabilities of cells clusters within the foam.

3 WOVEN TEXTILE CORE MATERIALS


3.1 Specimens
Stainless steel 304 woven textile core materials were fabricated at University of Virginia. The
relative density of the core was 12.6%. SS 304 wires of 0.508 mm diameter were woven into a
layer which has diamond-shaped cells. The average cell size was 3.24 mm × 3.24 mm along the
wires. The woven layers were stacked into 15.45 mm thickness. The thickness of the textile core in
the loading direction was 17.63 mm and the width was 18.55 mm.

3.2 Response at different deformation rates


The stainless steel 304 woven textile core
specimens were compressed at different regimes
of deformation rates. In quasi-static loading, the
relative velocity between two compression
platens was 1×10-4 m/s, corresponding to a
strain rate of 7×10-4 s-1. The dynamic
experiments were performed at a relative
velocity of 4~6 m/s (deformation rate of
230~330 s-1) in the Kolsky bar apparatus, while
deformation velocities in the range of 72~104
m/s (deformation rate of 4129~5921 s-1) were
achieved in the gas gun set-up. Curves of load
Figure 5: Stress-strain curves of compression of
versus relative deformation of textile cores under
textile cores at different strain rates.
δ/L0: 0.006 0.015 0.027 0.044 0.054 0.071 0.081

δ/L0: 0.043 0.195 0.350 0.511 0.661

Figure 6: Failure sequences of woven textile cores at different strain rates.


different loading rates are given in Fig. 5. The curves show minor difference across the explored
deformation rates. The load reaches a peak value after an initial elastic region and thereafter is
almost constant, which can be considered as a plateau. The specimen behavior exhibits a
progressive densification with an associated monotonic increase in stress. The peak stress appears
to increase slightly with the increase in deformation rate, but the area under the force-deformation
curve is much less sensitive to the loading rate. The rate insensitivity of the textile cores to the
force-deformation response is similar to the one observed in the investigated Al foam.
On the other hand, the failure mode has a well defined transition from quasi-static and Kolsky
bar to gas gun where the shock wave formation is also observed. In gas gun tests, diamond-shaped
cells adjacent to the impact surface collapsed first as shown in Fig. 6. A crushing front, parallel to
the front face sheet, propagates through the core. This crushing front is associated to a shock front
corresponding to a jump in stress and density. To measure the shock wave effect, reverse impact
tests were carried out on the textile cores. Fig. 5 shows a comparison between forward and reverse
impact results. Because brazing materials joining the core and the face sheet remained in gaps
between ligaments in the reverse test, the initial peak load was determined by this extra mass and
associated inertia effect. The shock wave effect is clearly observed after the initial spurious peak.
While this stress is higher than one measured in the forward impact tests the evolution is similar.
Again, the signal has many peak and valleys that can be correlated to multiple instabilities in the
core.

4 TRUSS CORE MATERIALS


4.1 Materials
The sandwich panels with pyramidal truss core made of stainless steel 304 were fabricated at the
University of California at Santa Barbara. The tested specimens had a relative density of 3.5% and
a 4-sided pyramid structure. The core thickness was 11.65 mm and the span of one cell: 16.82
×15.39 mm2. Truss members had a width of 1.18 mm and a thickness of 1.18 mm. The face sheet
thickness is 2.2 mm. This unit cell repeated over the whole panel in x- and y-directions so that it is
representative of the truss core materials. The unit cell specimens were cut from the sandwich
panel and extra materials were left at the joints to maintain the periodicity by strong enough joints.

4.2 Response at different deformation rates


Uniform compression tests were performed on unit cell specimens. In quasi-static loading, the
relative velocity between face sheets was 8×10-5 m/s, corresponding to a strain rate of 7×10-3 s-1.
The dynamic experiments in the Kolsky bar were performed at a relative velocity of 2.5~6.4 m/s,
which corresponds to a strain rate of 263~550 s-1. In the gas gun, deformation velocities of
84.5~115 m/s were reached resulting in a nominal
strain rate of about 7257~9875 s-1. Fig. 7 shows
plots of load versus relative displacement under
quasi-static and dynamic loading. In all cases, after
an initial nominal stress increase, the load reaches a
peak value and then drops. This load-displacement
behavior is characteristic of structures exhibiting
instability. The buckling instability was observed
with high speed photography. Inspection of Fig. 7
reveals that the peak load attained in the gas gun is
the highest followed by the peak load measured in
Figure 7: Stress-strain curves of pyramidal the Kolsky bar experiments. As expected from a
truss core being crushed at theoretical view point, the peak load measured in
different strain rates. the quasi-static experiments is the lowest. In terms
δ/L0: 0.010 0.086 0.172 0.001 0.101 0.296 0.470

Figure 8: Failure sequences of pyramidal truss cores at different strain rates.

of nominal stress, the quasi-static peak stress is 4.0~4.2 MPa, almost half of the peak load in
Kolsky bar loading (6.4 MPa). In the gas gun case, the peak stress is about 9.6~12.0 MPa.
Additionally, comparison of areas under load-deformation responses shows that energy absorption
up to a strain of 0.5 is a strong function of loading rate. In the gas gun experiments the dissipated
energy is twice that of that in the quasi-static and Kolsky bar experiments. Again, the difference
between quasi-static and 500 s-1 is modest. Both curves have the same features indicative of similar
deformation behavior. High speed images later presented are consistent with this interpretation.
In the quasi-static and Kolsky bar experiments, the post-peak load smoothly decreases to what
seems to be a steady state value, which is similar in both loading rates. On the other hand, several
instabilities at different displacement levels are seen in the gas gun loading. Moreover, it is
observed that the location of the multiple peaks in load is a function of the specimens as inferred
from comparison of two experiments conducted at almost identical strain rate.
Examination of high speed images, Fig. 8, reveals a failure mode transition between the
nominal strain rate imparted in the Kolsky bar and gas gun experiments. Careful inspection of the
deformation in the truss members reveals that the buckling modes are dependent on the initial
member imperfections. In some cases anti-symmetric mode of buckling is observed.

5 CONCLUSION
The compressive behavior of open cell aluminum foam, a textile stainless steel core and a
pyramidal truss core was investigated, under various strain rates, using a unique combination of
experiments. For the case of open cell foams, comparison between quasi-static and Kolsky bar
experiments revealed moderate micro-inertia phenomena, where the inertia due to bending and
buckling of the ligaments in the foam resisted strain localization. The gas gun experiments
revealed a totally different deformation mode. A shock wave consisting of crashed material was
generated at the impact surface and propagated through the specimen with a well defined speed.
By performing gas gun experiments in forward and reverse configurations the stress level in front
and behind the plastic or crushing shock front was measured. When the quasi-static, Kolsky bar
and direct gas gun experiments are compared, the plateau or crashing stress is almost insensitive to
strain rate. For the high strain rate experiments, this stress corresponds to the stress level in front of
the propagating shock. We have also shown that generation and propagation of shock waves within
foam materials greatly enhances their energy absorption. In light of this finding, foam materials
should be tailored so that plastic shock waves are triggered in the applications of interest.
In the case of textile cores, the findings were quite similar to the ones observed in open cell
foams. A well define failure mode transition was observed when the deformation rate was
transitioned from 500 s-1 to 1×104 s-1. In the case of pyramidal truss core specimens significant
strain rate effects on peak stress and energy absorption were observed. Micro inertia appears as the
dominant effect in determining the peak nominal stress. A coupling between plastic wave
propagation (control by axial inertia) and buckling (lateral displacement) was observed. A very
unique deformation of the members, at strain rates in the order of 1×104 s-1, arises from
deformation compatibility. Members are crash against the fast moving face sheet and make contact
early on in the crashing process. The experiments also reveal that overall nominal stress – nominal
strain curve is highly dependent on the initial imperfection of the members.
Further study should investigate the effect of the relative density on the peak stress and energy
absorption of the material. The results could then be utilized to determine optimal core designs as a
function of the application.

6 ACKNOWLEDGEMENTS
The authors would like to acknowledge F. Barthelat and N. Moldovan for their assistance in
conducting the experiments. Special thanks are due to Professor J.W. Hutchinson from Harvard
University and Professors A.G. Evans and F. Zok, and Dr. H. Rathbun from University of
California at Santa Barbara for insightful discussions during the investigation reported here. The
authors are also in debt to Professor H. Wadley and Drs. K. Dharmasena and D.T. Queheillalt from
University of Virginia for their aid in the fabrication of samples and helpful discussions. This work
was sponsored by the Office of Naval Research under Award No. 123163-02-N00014-02-1-0700.

7 REFERENCES
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