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    ASTM D7504: Impurities in Monocyclic Aromatic Hydrocarbons On Stabilwax

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    ASTM D7504: Impurities in Monocyclic Aromatic Hydrocarbons On Stabilwax

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    Original Title

    Stabilwax Peak Characteristics

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    ASTM D7504: Impurities in Monocyclic Aromatic Hydrocarbons On Stabilwax

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    ASTM D7504: Impurities in Monocyclic Aromatic Hydrocarbons on Stabilwax

    4 22
    3 19 23
    18 24 27 31
    5 9 10 13 16 20 21 29 30
    17 25 28
    7 11 12 14 15 26
    8

    5 7.5 10 12.5 15 17.5 20 22.5

    Time (min)
    GC_PC1355

    Peaks tR (min) Peaks tR (min)


    1. Octane 4.79 16. m-Ethyltoluene 16.02
    2. Nonane 5.60 17. tert-Butylbenzene 16.49
    3. Benzene 6.32 18. Isobutylbenzene 16.62
    4. Decane 7.19 19. Mesitylene 16.77
    5. Toluene 8.55 20. sec-Butylbenzene 16.94
    6. 1,4-Dioxane 9.24 21. Styrene 17.32
    7. Undecane 10.48 22. Allylbenzene 17.60
    8. Ethylbenzene 11.90 23. 1,2,4-Trimethylbenzene 18.22
    9. p-Xylene 12.25 24. Tridecane 18.75
    10. m-Xylene 12.52 25. 1,3-Diethylbenzene 18.93
    11. Cumene 13.88 26. 1,4-Diethylbenzene 19.25
    12. o-Xylene 14.37 27. n-Butylbenzene 19.35
    13. Dodecane 14.81 28. α-Methylstyrene 20.04
    14. Propylbenzene 15.35 29. Phenylacetylene 21.12
    15. p-Ethyltoluene 15.92 30. 1,4-Diisopropylbenzene 22.25
    31. trans-β-Methylstyrene 22.46

    Column Stabilwax, 60 m, 0.32 mm ID, 0.25 µm (cat.# 10627)


    Sample D7504 resolution mix
    Diluent: Cyclohexane
    Injection
    Inj. Vol.: 0.6 µL split (split ratio 100:1)
    Liner: Topaz 4.0 mm ID Precision inlet liner w/wool (cat.# 23305)
    Inj. Temp.: 250 °C
    Oven
    Oven Temp.: 60 °C (hold 10 min) to 150 °C at 5 °C/min (hold 4 min)
    Carrier Gas He, constant flow
    Flow Rate: 1.7 mL/min
    Detector FID @ 265 °C
    Instrument Agilent 7890B GC
    Notes ASTM D7504 covers the determination of trace impurities in monocyclic aromatic
    hydrocarbons. It includes analysis of nonaromatic and individual aromatic compounds
    in benzene, toluene, ethylbenzene, p-xylene, o-xylene, styrene, and mixed xylenes.
    The chromatogram shows a synthetic blend of the most common analytes identified
    and quantified by D7504; all analytes are well resolved on a Stabilwax column.

    © 2019 Restek Corporation. All rights reserved. Restek patents and trademarks are the property of Restek Corporation. (See www.restek.com/Patents-Trademarks for full list.) Other trademarks in Restek literature
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