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    Organic Letters - Data Preparation Checklist

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    Josephine Torres
    This document provides a checklist for preparing data to accompany a manuscript being submitted to the Organic Letters journal. It outlines requirements for consistency between the manuscript and supporting information, general supporting information guidelines, experimental details, spectra, and essential data needed for new and known compounds. Requirements include compound identification and numbering, reaction details, purity analyses, and labeled and high-quality NMR, HRMS, and other spectral data.

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    Organic Letters - Data Preparation Checklist

    Uploaded by

    Josephine Torres
    128 views2 pages
    This document provides a checklist for preparing data to accompany a manuscript being submitted to the Organic Letters journal. It outlines requirements for consistency between the manuscript and supporting information, general supporting information guidelines, experimental details, spectra, and essential data needed for new and known compounds. Requirements include compound identification and numbering, reaction details, purity analyses, and labeled and high-quality NMR, HRMS, and other spectral data.

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    orlef7_authguide orlef7_si_review_checklist

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    orlef7_si_review_checklist

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    This document provides a checklist for preparing data to accompany a manuscript being submitted to the Organic Letters journal. It outlines requirements for consistency between the manuscript and supporting information, general supporting information guidelines, experimental details, spectra, and essential data needed for new and known compounds. Requirements include compound identification and numbering, reaction details, purity analyses, and labeled and high-quality NMR, HRMS, and other spectral data.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    128 views2 pages

    Organic Letters - Data Preparation Checklist

    Uploaded by

    Josephine Torres
    This document provides a checklist for preparing data to accompany a manuscript being submitted to the Organic Letters journal. It outlines requirements for consistency between the manuscript and supporting information, general supporting information guidelines, experimental details, spectra, and essential data needed for new and known compounds. Requirements include compound identification and numbering, reaction details, purity analyses, and labeled and high-quality NMR, HRMS, and other spectral data.

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    ORGANIC

     LETTERS  –  DATA  PREPARATION  CHECKLIST  


    (For  additional  details,  refer  to  the  Organic  Letters  Guidelines  for  Authors)  
    NOTE:    Additional  data  may  be  requested  for  compounds    
     
     
    Manuscript/Supporting  Information  (SI)  Consistency  
    ☐    Compounds  are  identified  consistently  between  the  manuscript  and  SI:  
    ☐    Compound  numbers        
    ☐    Structures  
    ☐    Experimental  details  and  spectra  in  the  SI  are  in  the  sequence  that  corresponds      
                 to  the  manuscript    
     
     
    Supporting  Information  –  General  
    ☐    Manuscript  title  and  all  authors  are  listed  on  the  first  page  of  each  SI  file  
    ☐    Pages  are  numbered  in  all  files  for  publication  
    ☐    Table  of  contents  is  included    
    ☐    Files  are  combined  -­‐  do  not  submit  a  series  of  files  of  images/structures  
    ☐    Introductory  Section  is  present  and  describes:  
    ☐    Standard  techniques      
    ☐    Instruments  (NMR,  microwave  reactors,  etc.)    
    ☐    Suppliers  for  commercial  compounds  
    ☐    Citations  to  references  for  non-­‐commercial  known  compounds    
    ☐    Hazardous  reactions  or  toxic  compounds  
     
     
    Experimental  Details  
    ☐    Synthetic  procedures/data  include:  
    ☐    Reactant  quantities  
    ☐    Detailed  purification  techniques      
    ☐    Product  quantities    
    ☐    Isolated  yields  
    ☐    Physical  state/description  of  the  compounds  (i.e.,  color,  solid,  etc.)  
    ☐  1  mmol  scale  detailed  method  included  for  one-­‐step  transformations    
    ☐    Data  is  reviewed  for  accuracy,  omissions  and  typos:  
    ☐    Molecular  formula    
    ☐    HRMS  data:  
    ☐    HRMS  actual  values  are  within  the  ±10  ppm  error  limit  
    ☐    HRMS  molecular  weight  matches  the  structure  shown  
      ☐    Elemental  Analysis:  
    ☐    Elemental  analysis  values  are  within  the  ±0.4%  error  limit  
    ☐    Reported  formula  matches  the  structure  shown  
    ☐    Spectral  data:  
    ☐    1H  and  13C  atoms  have  been  accounted  for  
    ☐    Reported  data  corresponds  to  the  spectra  provided  in  the  SI  
    Spectra  
    ☐    Spectra  are  labeled  with  an  image  of  the  structure  and  a  compound  number  
    ☐    Spectra  are  legible  and  images  are  not  faint  or  blurry  
    ☐    Spectra  are  at  least  a  half  page  in  size  
    ☐    NMR  baseline  is  displayed  with  the  minimum  chemical  shift  range  
    ☐    -­‐1-­‐9  ppm  for  1H  spectra      
    ☐    -­‐10-­‐190  ppm  for  13C  spectra  
    ☐    Extended  range  for  functional  groups  that  resonate  from  9-­‐14  ppm  
    ☐    Peaks  in  the  1H  NMR  are  integrated  
    ☐    Chemical  shift  values  are  included  for  all  peaks  in  the  1H  and  13C  spectra  
     
     
    New  Compounds:    Essential  Data  
    ☐    1H  and  13C  spectra    
    ☐    HRMS  data  or  elemental  analysis  data  
     
     
    Known  Compounds  -­‐  Synthesized  by  a  new/improved  method:    Essential  Data    
    ☐    A  reference  in  the  experimental  details  section  
    ☐    Include  one  or  more  of  the  following:    1H  or  13C  NMR  spectra,  elemental  analysis,        
               HPLC,  GC  

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