Chemical Analysis of Portland Slag Cement IS 4032

VEL/CTH/REG/OBS/32
IS:4032-1985
CIVIL TEST HOUSE
VELCITI CONSULTING ENGINEERS (P) LTD.
Work Sheet
Determination of Loss on Ignition in Slag Cement
Laboratory Sample .ID
Received Date
Date of Test
Report Date
Sample Description
Source of Sample Sampling Date
Sample Location NP/ Stockpile / Sampled By
Sampling Method Sample Brought By
Test Method IS 4032-1985 (6.2) Condition of Sample
Sample Preparation
IS 4032-1985 (6.2) Temp.
Method
Tested By
Test Summary
Specimen reference 1 2
Weight of sample used W2 g (1g)
Weight of crucible W3 g
Weight of crucible and (900-1000 0C ignited Sample in g
Weight of crucible and (900-1000 0C ignited Sample W4 g (second heating)
Percentage loss on ignition of the sample= (W4-W3/W2)*100
Average loss on ignition of the sample in %
Remarks: Tested by Checked by

VEL/CTH/REG/OBS/42
IS:4032-1985
CIVIL TEST HOUSE
Work Sheet
Determination of Insoluble Residue in Slag Cement
Received Date
Date of Test
Report Date
Sample Description
Sample Preparation
IS 4032-1985 (4.10) Temp.
Method
Tested By
Test Summary
Weight of crucible and (900-1000 0C )ignited residue of the Sample in g W4a g
Re Weight of crucible and (900-1000 0C )ignited residue of the Sample in W4 g
Weight of ignited residue in Blank determination in g W1
Percentage of Insoluble Residue of the sample= ((W4-W3)-W1)/W2)*100
Average Insoluble Residue of the sample in %

VEL/CTH/REG/OBS/33
IS:4032-1985
CIVIL TEST HOUSE
Work Sheet
Determination of Sulphuric Anhydride in Slag Cement
Received Date
Date of Test
Report Date
Sample Description
Sample Preparation
IS 4032-1985 (6.11) Temp.
Method
Tested By
Test Summary
Re Weight of crucible and (800-9000C) ignited residue W4a g
Weight of crucible and (800-9000C) ignited residue W4 g
Weight of ignited residue in g W= W4-W3
SO3 Percent of the sample= (W-W1)*34.3
Average SO3 Percent of the sample

VEL/CTH/REG/OBS/
34
CIVIL TEST HOUSE IS:4032-1985
Work Sheet
Determination of Silica in Slag Cement
Received Date
Date of Test
Report Date
Sample Description
Sample Preparation
IS 4032-1985 (6.3) Temp.
Method
Tested By
Test Summary
Weight of sample used W2 g (0.5g)
Weight of crucible and (1100-12000C) ignited residue W4a g
Re Weight of crucible and (1100-12000C) ignited residue W4 g
Weight of crucible and (1100-12000C) ignited Impurities W5a g (After
HF Treatment)
Re Weight of crucible and (1100-12000C) ignited Impurities W5g

(After HF Treatment)
Weight of ignited SiO2 residue in g W= W4-W5
Silica (SiO2) Percent of the sample= (W-W1)*200
Average Silica SiO2 Percent of the sample

VEL/CTH/RE
G/OBS/35
Work Sheet
Determination of Ferric Oxide in Slag Cement
Received Date
Date of Test
Report Date
Sample Description
Sample Location Sampled By
Test Method IS:4032 (6.5) Condition of Sample
Sample Preparation
IS:4032 (6.5) Temp.
Method
Tested By
Test Summary
Weight of sample used for SiO2 determination in g W (0.5g)
Volume of sample solution used for Fe2O3 test in ml (25ml)
Volume of 0.01 M EDTA used for Titration in ml V
Do the Blank determination same as the sample & note the volume, as V0
Iron Oxide(Fe2O3) Percent of the sample =0.7985*(V-V0)/W

(1 ml of 0.01 M EDTA ≡0.7985 mg of Fe2O3)
Average Ferric Oxide Content (as Fe2O3), in %

TEST 2 BUILD PRIVATE LIMITED
Know your Material
IS:4032-1985
Work Sheet
Determination of Aluminium Oxide in Slag Cement
Received Date
Date of Test
Report Date
Sample Description
Sample Preparation
Temp.
Method
Tested By
Test Summary
Volume of sample solution used for Fe2O3 test in ml (25ml)
Volume of 0.01 M EDTA used for Al2O3 in ml V= V1-V2-(V3*E)
Total Volume of EDTA used in the titration in ml=V1
Volume of EDTA used for iron in ml=V2
Total Volume of bismuth nitrate solution used in titration in ml=V3
Equivalance of 1ml of bismuth nitrate solution E=V4/100

Where V4 =Volume of EDTA solution in ml.
Do the Blank determination same as the sample & note the volume, as V0
Aluminium Oxide(Al2O3) Percent of the sample =0.5098*(V - V0)/W

(1 ml of 0.01 M EDTA ≡0.5098 mg of
Al2O3)
Average Aluminium Oxide Content (as Al2O3), in %

VEL/CTH/REG/OBS/
37
Work Sheet
Determination of Calcium Oxide in Slag Cement
Received Date
Date of Test
Report Date
Sample Description
Test Method IS:4032 (6.7.2 EDTA Method) Condition of Sample
Sample Preparation
IS:4032 (6.7.2 EDTA Method) Temp.
Method
Tested By
Test Summary
Volume of sample solution used for CaO test in ml (10ml)
Volume of 0.01 M EDTA used for Titration in ml V
Do the Blank determination same as the sample & note the volume,
as V
Calcium Oxide(CaO) Percent of the 0sample =(0.05608*25*(V-
V0))/W (1 ml of 0.01 M EDTA ≡0.5608
mg of CaO)
Average Calcium Oxide Content (as CaO), in %

VEL/CTH/REG/OBS/3
8
Work Sheet
Determination of Magnesium Oxide in Slag Cement
Received Date
Date of Test
Report Date
Sample Description
Test Method IS:4032 (6.8.2 EDTA Method) Condition of Sample
Sample Preparation
IS:4032 (6.8.2 EDTA Method) Temp.
Method
Tested By
Test Summary
Volume of sample solution used for MgO test in ml (10ml)
Volume of 0.01 M EDTA used in CaO determination V
Volume of 0.01 M EDTA used for Titration in ml V1
Magnesium Oxide(CaO) Percent of the sample =(0.04032*25*V1-V)/W

(1 ml of 0.01 M EDTA ≡0.4032 mg of MgO)
Average Magnesium Oxide Content (as MgO), in %

VEL/CTH/RE
G/OBS/39
Work Sheet
Determination of Manganic Oxide in Slag Cement
Received Date
Date of Test
Report Date
Sample Description
Sample Preparation
IS:4032 (6.10) Temp.
Method
Tested By
Test Summary
Weight of sample used in g S (1 to 3g)
Manganic oxide( Mn2O3) equivalent of the NaAsO2 solution g/ml C=(0.03*0.236*30)/(a*b),(a)

Volume of KMnO4 solution required byNa2C2O4,(b) Volume of NaAsO2 solution
require by 30 ml of KMnO4 solution.(Each ml of NaAsO2 approximately equivalent to 0.0003 g
of Mn2O3)
Manganic oxide( Mn2O3) percentage of the sample in %=(C(V-V0)/S)*100
Volume of NaAsO2 solution required by the sample (V)
Do the Blank determination same as the sample & note the volume, as V 0
Average Maganic Oxide Content (as Mn2O3), in %

VEL/CTH/REG/OBS/40
BS EN 196-2
CIVIL TEST HOUSE
Work Sheet
Determination of Chloride in Slag Cement
Received Date
Date of Test
Report Date
Sample Description
Test Method BS EN 196-2 (4.5.16) Condition of Sample
Sample Preparation
Temp.
Method
Tested By
Test Summary
Weight of sample used for Cl determination in g M26 (5.00±0.05g) weigh to 0.0005 g
Volume of the Ammonium thiocyanate solution used for titration of the test solution V17
Volume of the Ammonium thiocyanate solution used for titration of the blank solution V18
Chloride content (Cl) Percent of the sample =(0.8865*V18-V17)/V18*M26
Average Chloride Content (as Cl-), in %

VEL/CTH/REG/OBS/41
IS:4032-1985
CIVIL TEST HOUSE
Work Sheet
Determination of Alkali Content in Slag Cement
Received Date
Date of Test
Report Date
Sample Description
Sample Preparation
Temp.
Method
Tested By
Test Summary
Weight of sample used for Alkali determination in g W (1.000±0.001g)
Calibrates the Apparatus as per IS 4032( 4.11.3.2) (manufacturers instruction) using Na2O and
K2O standarad solution
Flamephotometer readings of Na2O in ppm
Na2O content of the sample in %= Na2O in ppm*0.01
Average Na2O content of the sample in %
Flamephotometer readings of K2O in ppm
K2O content of the sample in %=K2O in ppm*0.01
Average K2O content of the sample in %
Equivalent Alkali Content of the sample in % =K2O*0.658+Na2O
Average Equivalent Alkali content of the sample in %

Chemical Analysis of Portland Slag Cement IS 4032

Uploaded by

Copyright:

Available Formats

Chemical Analysis of Portland Slag Cement IS 4032

Uploaded by

Document Information

Original Description:

Copyright

Available Formats

Share this document

Share or Embed Document

Sharing Options

Did you find this document useful?

Is this content inappropriate?

Copyright:

Available Formats

Chemical Analysis of Portland Slag Cement IS 4032

Uploaded by

Copyright:

Available Formats

VEL/CTH/REG/OBS/32

Weight of crucible and (900-1000 0C ignited Sample in g

Weight of crucible and (900-1000 0C ignited Sample W4 g (second heating)

Percentage loss on ignition of the sample= (W4-W3/W2)*100

Average loss on ignition of the sample in %

Remarks: Tested by Checked by

Weight of crucible and (900-1000 0C )ignited residue of the Sample in g W4a g

Re Weight of crucible and (900-1000 0C )ignited residue of the Sample in W4 g

Weight of ignited residue in Blank determination in g W1

Percentage of Insoluble Residue of the sample= ((W4-W3)-W1)/W2)*100

Average Insoluble Residue of the sample in %

Remarks: Tested by Checked by

Re Weight of crucible and (800-9000C) ignited residue W4a g

Weight of crucible and (800-9000C) ignited residue W4 g

Weight of ignited residue in g W= W4-W3

Weight of ignited residue in Blank determination in g W1

SO3 Percent of the sample= (W-W1)*34.3

Average SO3 Percent of the sample

Remarks: Tested by Checked by

Re Weight of crucible and (1100-12000C) ignited Impurities W5g

Weight of ignited residue in Blank determination in g W1

Silica (SiO2) Percent of the sample= (W-W1)*200

Average Silica SiO2 Percent of the sample

Volume of sample solution used for Fe2O3 test in ml (25ml)

Volume of 0.01 M EDTA used for Titration in ml V

Iron Oxide(Fe2O3) Percent of the sample =0.7985*(V-V0)/W

Average Ferric Oxide Content (as Fe2O3), in %

Remarks: Tested by Checked by

Volume of sample solution used for Fe2O3 test in ml (25ml)

Volume of 0.01 M EDTA used for Al2O3 in ml V= V1-V2-(V3*E)

Total Volume of EDTA used in the titration in ml=V1

Volume of EDTA used for iron in ml=V2

Total Volume of bismuth nitrate solution used in titration in ml=V3

Equivalance of 1ml of bismuth nitrate solution E=V4/100

Aluminium Oxide(Al2O3) Percent of the sample =0.5098*(V - V0)/W

Average Aluminium Oxide Content (as Al2O3), in %

Remarks: Tested by Checked by

Remarks: Tested by Checked by

Volume of sample solution used for MgO test in ml (10ml)

Volume of 0.01 M EDTA used in CaO determination V

Volume of 0.01 M EDTA used for Titration in ml V1

Magnesium Oxide(CaO) Percent of the sample =(0.04032*25*V1-V)/W

Average Magnesium Oxide Content (as MgO), in %

Remarks: Tested by Checked by

Manganic oxide( Mn2O3) equivalent of the NaAsO2 solution g/ml C=(0.03*0.236*30)/(a*b),(a)

Manganic oxide( Mn2O3) percentage of the sample in %=(C(V-V0)/S)*100

Volume of NaAsO2 solution required by the sample (V)

Average Maganic Oxide Content (as Mn2O3), in %

Remarks: Tested by Checked by

Chloride content (Cl) Percent of the sample =(0.8865*V18-V17)/V18*M26

Average Chloride Content (as Cl-), in %

Remarks: Tested by Checked by

Weight of sample used for Alkali determination in g W (1.000±0.001g)

Flamephotometer readings of Na2O in ppm

Na2O content of the sample in %= Na2O in ppm*0.01

Average Na2O content of the sample in %

Flamephotometer readings of K2O in ppm

K2O content of the sample in %=K2O in ppm*0.01

Average K2O content of the sample in %

Magnesium Oxide(CaO) Percent of the sample =(0.0403225V1-V)/W

Manganic oxide( Mn2O3) equivalent of the NaAsO2 solution g/ml C=(0.030.23630)/(a*b),(a)

Chloride content (Cl) Percent of the sample =(0.8865V18-V17)/V18M26