PAKFOOD PUBLIC COMPANY LIMITED / OKEANOS PLANT

MICROBIOLOGICAL and CHEMICAL STANDARD for COOKED PRODUCTS : S-LB-012

REVISED : # 07
ISSUED DATE : AUGUST 28, 2007
MICROBIOLOGICAL AND CHEMICAL STANDARD
□ CUSTOMER STANDARD □ RAW PRODUCT
☑ TYC STANDARD ☑ COOKED PRODUCT
□ VALUE ADDED PRODUCT
A. ANTIBIOTIC
CATEGORY ANTIBIOTIC SPECIFICATION METHOD FREQUENCY TEST BY
RAW MATERIAL OXYTETRACYCLINE(ppm.) ND(Std.conc.minimum0.025) BIO-ASSAY EVERY PONDS INHOUSE LAB
TETRACYCLINE GROUP(ppm.) ND (LOD=0.02) HPLC when RM positive* PRIVATE LAB
OXOLINIC ACID (ppm.) ND (LOD=0.02) HPLC EVERY PONDS INHOUSE LAB
CHLORAMPHENICOL (ppb.) ND (LOD=0.025) ELISA EVERY PONDS INHOUSE LAB
MALACHITE GREEN(ppb) ND (LOD=0.05) LC-MSMS EVERY 3 MONTH DOF or PRIVATE LAB
NITROFURANS (ppb.) ND(AOZ, AMOZ LOD=0.02, LC-MSMS SUPPLIER CONTROL to ASL DOF or PRIVATE LAB
SEM ,AHD LOD=0.05) EVERY 3 MONTH
FINISHED PRODUCT TETRACYCLINE GROUP(ppm.) ND (LOD=0.02) HPLC DOF,PRIVATE LAB
OXOLINIC ACID (ppm.) ND (LOD=0.02) HPLC VERIFY EVERY DOF,INHOUSE LAB
CHLORAMPHENICOL (ppb.) ND (LOD=0.025) ELISA TWO MONTH DOF,INHOUSE LAB
NITROFURANS (ppb.) ND(AOZ, AMOZ LOD=0.02, LC-MSMS DOF,PRIVATE LAB
SEM ,AHD LOD=0.05)
REMARK : FREQUENCY :*Positive tested by BIO-ASSAY daily
B. CHEMICAL
CATEGORY ANTIBIOTIC SPECIFICATION METHOD FREQUENCY TEST BY
RAW MATERIAL SULFITE (ppm.) < 10 MODIFIED MONIER WEEKLY INHOUSE LAB
WILLIAMS METHOD
PHOSPHATE (%) <0.5 MOLYBDENUM BLUE MONTHLY INHOUSE LAB
FINISHED PRODUCT SULFITE (ppm.) <10 MODIFIED MONIER EVERY SHIPMENT INHOUSE LAB
WILLIAMS METHOD
PHOSPHATE (%) <0.5 MOLYBDENUM BLUE EVERY SHIPMENT INHOUSE LAB
SALT CONTENT(%) <2 VOLUMETRIC METHOD EVERY SHIPMENT INHOUSE LAB
MOISTURE (%) 75-84 MOISTURE BALANCE DEPEND ON CUSTOMER INHOUSE LAB
REQUIREMENT
SODIUM (mg/100g) <300 ATOMIC ABSORPTION DEPEND ON CUSTOMER PRIVATE LAB
SPECTROPHOTOMETRIC METHOD REQUIREMENT
C. MICROBIOLOGICAL
CATEGORY MICROBIOLOGICAL SPECIFICATION METHOD FREQUENCY TEST BY
RAW MATERIAL Aerobic Plate Count (CFU/g) < 1,000,000 BAM On line EVERY PONDS INHOUSE LAB
Coliform (MPN/g) < 250 BAM On line INHOUSE LAB
E. coli (MPN/g) <10 BAM On line INHOUSE LAB
S. aureus (MPN/g) <100 BAM On line INHOUSE LAB
Salmonella spp.(/25g) ND ISO 6579 INHOUSE LAB
V. cholerae (/25 g) ND BAM On line INHOUSE LAB
V. parahaemolyticus(MPN/ g) <3 BAM On line INHOUSE LAB
FINISHED PRODUCT Aerobic Plate Count (CFU/g) < 50,000 BAM On line DAILY :4 period INHOUSE LAB
Coliform (MPN/g) < 10 BAM On line RELEASE : 5 SAMPLE/ INHOUSE LAB
E. coli (MPN/g) <3 BAM On line SHIPMENT INHOUSE LAB
S. aureus (MPN/g) <3 BAM On line INHOUSE LAB
Salmonella spp.(/25g) ND ISO 6579 INHOUSE LAB
V. cholerae (/25 g) ND BAM On line INHOUSE LAB
V. parahaemolyticus(MPN/ g) < 0.3 BAM On line INHOUSE LAB
L. monocytogenes(/25g) ND BAM On line INHOUSE LAB
D. SANITATION
DESCRIPTION SPECIFICATION FREQUENCY
APC Coliform E. coli S.aureus Salmonella spp. V.cholerae V. parahaemolyticus
CFU/100cm2 MPN/100cm2 MPN/100cm2 /100cm2 /100cm2 /100cm2 /100cm2
EQUIPMENT ONCE/WEEK
1. BEFORE WORK < 100 ND ND ND ND ND ND
2. AFTER CLEAN < 100 ND ND ND ND ND ND
3. DURING WORK < 5,000 < 10 ND ND ND ND ND
PERSONNEL ONCE/WEEK
1. AFTER CLEAN < 100 ND ND ND ND ND ND
2. DURING WORK < 5,000 < 10 ND ND ND ND ND
AIR TEST 50/15min NT NT NT NT NT NT TWICE /MONTH
WATER & ICE < 100/ml ND(MPN/100ml)ND(MPN/100ml) ND/100ml ND/100ml ND/100ml ND/100ml ONCE/WEEK

................................................. : QA SENIOR SUPERVISOR

................................................. : QA MANAGER