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    MA 3 Solo EN Brochure - Extended Ver4.0 - February 2023 - Hires

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    MA 3 Solo EN Brochure - Extended Ver4.0 - February 2023 - Hires

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    fian.jambi2019
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    MA-3-Solo-EN-Brochure_Extended-Ver4.0_February-2023_Hires

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    11 views10 pages

    MA 3 Solo EN Brochure - Extended Ver4.0 - February 2023 - Hires

    Uploaded by

    fian.jambi2019

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    © All Rights Reserved
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    Figure 2.

    Cold vapor atomic absorption spectroscopy

    Data example #1 Data example #2

    Measurement result by MA-3 Solo Sample name Number of samples Mean value (ng) CV (%)
    Sample Authentication range
    name or measurement result Amount of Number of Mean CV Mercury standard
    5 0.050 4.6
    sample samples value (%) solution 0.05 ng
    Standard Mercury standard
    Coal 0.0895 ~ 0.0961 5 0.099 2.9
    sample (NIST 50 ~ 57 mg 5 0.0915 mg/kg 2.1 solution 0.1 ng
    1632d) mg/kg
    (SRM)
    Mercury standard
    *1 5 101 0.4
    Wastewater 11.6 mg/L 200 µL 3 12.3 mg/L 3.7 solution 100 ng
    Crude 3.75 mg/kg
    *2
    200 µL 5 3.88 mg/kg 2.4
    petroleum
    *3
    Naphtha 0.31 ug/kg 200 µL 10 0.45 ug/kg 12.19
    Actual
    samples *3
    Condensate 2.75 ug/kg 200 µL 3 2.41 ug/kg 1.76
    Crude 62.9 ug/kg
    *3
    90 ~ 125mg 3 64.2 ug/kg 3.12
    petroleum
    *3
    Fuel Oil 395.2 ug/kg 60 ~ 75mg 3 396.8 ug/kg 0.12
    Specification
    Measurement Range 5ng/L – 50 µg/L (For measurement of 20ml)
    Precision RSD 3% (for 15ng/L or more)
    Sample volume 20 ml
    Dimension 464 x 366 x 176 (Carrying case)
    Weight 6 Kg (Including carrying case)

    Sn2+ + Hg2+ Sn4+ + Hg0

    CALIBRATION
    STD SVOL STD LOW MEAS Dev.
    0.004
    y= ax+Blank [ppm] [µL] [ng] [Height] [ng] [%]
    a= 1.78460E-03
    0.01 0 0 0.000036 0.001 -
    b= 3.35000E-05
    r= 0.9998 0.01 50 0.5 0.000908 0.490 2.0
    0.003 0.01 100 1.0 0.001826 1.004 0.4
    0.01 150 1.5 0.002664 1.474 1.7
    ABS [HEIGHT]

    0.01 200 2.0 0.003638 2.020 1.0


    0.002

    Ave SD C.V.
    No. Concentration Trials
    0.001 [ppt] [ppt] [%]
    1 50 ppt 5 48.89 0.81655 1.67
    2 25 ppt 5 24.27 0.15652 0.64
    0.000 3 10 ppt 5 9.88 0.38503 3.90
    0.00 .5 1.01 .5 2.0
    STD [ng] 4 5 ppt 5 4.89 0.25836 5.28
    A. Sampling Setup
    B. Measurement of Mercury Collector Tube

    STD Add Recovery SD C.V.


    Name Trials
    (ng) (%) (%) (%)
    Propane 3 1.701ng 96.60 0.8888 0.92

    MA-3 Solo AM-5 (AFS)


    (Gas Tube Analysis Kit) (Continuous Ambient Air Monitor)
    Ave.
    Vol. (L) Hg (ng) Conc. (ng/m3)
    (ng/m3)
    11/16 11:25~14:03 69.5 0.169 2.43 2.75
    11/16 14:05~17:41 93.2 0.224 2.40 2.63
    11/17 8:00~11:00 61.8 0.161 2.61 2.42
    11/18 11:25~14:14 82.6 0.201 2.43 2.41
    11/18 14:14~15:54 50.3 0.109 2.17 2.32
    Specifications
    Thermal decomposition mer- Measuring objects Solid sample; liquid sample; gaseous sample *1 *2
    cury analyzer MA-3 Solo Analysis method Thermal decomposition-gold amalgam collection cold atomic absorption spectrometry
    Measurement principle Non-dispersion double-beam cold atomic absorption spectrometry
    Light source Low-pressure mercury discharge lamp
    Detector Semiconductor detector (with 254 nm bandpass filter)
    Detection limit; Precision Detection limit: 0.01 ng; Precision: RSD 3% (0.1 ng or greater) *3
    Measuring range 0 to 10,000 ng
    Analysis time 5 to 12 minutes
    Flow rate at measurement 0.2 L/min
    Exhaust gas treatment Activated carbon filter for removing mercury
    Sample heating temperature Up to 850°C
    Heating control 3 Step setting (temperature time arbitrary setting possible)
    Carrier gas Self-purified ambient air
    Sample bottle Dedicated ceramic boat (Capacity: 1.5 mL)
    Size/Weight 403 W × 252 D ×300 H (mm), 13 kg (~28 lbs)
    Power source AC100-240 V, 50/60 Hz, 1.1 KVA
    Usage environment Temperature: 15 to 35°C; Humidity: 10 to 80% RH (no dew condensation)
    Standard accessories Sample boat (10); boat stands; boat tongs; L-cysteine
    Control/Data processing system OS Windows 10 Pro
    MA3Solo_Win Communication USB
    Display (Japanese/English) Peak waveform; calibration curve graph; measurement process; measurement result; equipment status
    Data processing Calibration curve (linear formula ×3 types; cubic formula × 3 types); unit setup; concentration computation;
    baseline correction; statistical calculation (mean value; standard deviation; CV%)
    Precision control Equipment check; evaluation of calibration curve; blank check; recovery calculation
    Printing Memo; calibration formula/graph; measured value table; statistical calculation; peak waveform
    Measurement date and time; result of equipment check

    Spare parts / Consumables Option for collector tube measurement


    Sample boat (10 pcs/set); sample heating tube; mercury collector tube; tubing/joint Collector tube measurement kit (a set of 5 collector tube L= 65 mm + holder for
    set, additive B and Charcoal pellets (for UOP 938-20 applications) measurement)

    Identify the right mercury analyzer for you

    http://www.hg-nic.com
    Osaka office 14-8 Akaoji-cho, Takatsuki-shi, Osaka 569-1146 Japan
    Distributors
    /Tech. center: TEL +81-72-694-5195 FAX +81-72-694-0663
    E-mail hg-nic@rigaku.co.jp URL www.hg-nic.com
    Singapore office: 61 Bukit Batok Crescent, #04-04A, Singapore 658078
    TEL +65-6873-7068 FAX +65-6873-6372

    ISO 9001: 2015 CERTIFIED Tech-center, Factory & Osaka office/2017.12.27


    ISO 14001: 2004 CERTIFIED Tech-center, Factory & Osaka office/2007.6.8
    MA-3 Solo Brochure/EN/2023.2/Ver4.0
    Copyright © 2018 NIC. All rights reserved.

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