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    Appendix A Analysis Report

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    MAT-LION
    The document is a solid sample analysis report that provides results from analyzing 4 solid samples. It includes parameters like mineral composition determined through x-ray diffraction, total metal concentrations, and results of bacteriological analyses. The samples are similar and mainly composed of magnetite, hematite, and amorphous material, but differ in minor mineral phases and metal concentrations.

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    Appendix A Analysis Report

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    MAT-LION
    25 views5 pages
    The document is a solid sample analysis report that provides results from analyzing 4 solid samples. It includes parameters like mineral composition determined through x-ray diffraction, total metal concentrations, and results of bacteriological analyses. The samples are similar and mainly composed of magnetite, hematite, and amorphous material, but differ in minor mineral phases and metal concentrations.

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    APPENDIX A ANALYSIS REPORT

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    The document is a solid sample analysis report that provides results from analyzing 4 solid samples. It includes parameters like mineral composition determined through x-ray diffraction, total metal concentrations, and results of bacteriological analyses. The samples are similar and mainly composed of magnetite, hematite, and amorphous material, but differ in minor mineral phases and metal concentrations.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    25 views5 pages

    Appendix A Analysis Report

    Uploaded by

    MAT-LION
    The document is a solid sample analysis report that provides results from analyzing 4 solid samples. It includes parameters like mineral composition determined through x-ray diffraction, total metal concentrations, and results of bacteriological analyses. The samples are similar and mainly composed of magnetite, hematite, and amorphous material, but differ in minor mineral phases and metal concentrations.

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    APPENDIX A

    ANALYSIS REPORT
    Solid Sample Analysis Report

    Station
    Date Sampled
    Sample ID 1 2 3 4
    Sample Appearance Solid Solid Solid Solid

    Parameter with units


    X-ray diffraction (%)
    Fe3O4 25 20 25 25
    FeO Not Detected Not Detected Not Detected Not Detected
    a-Fe2O3 Not Detected Not Detected Not Detected Not Detected
    a-FeOOH 15 15 15 15
    y-FeOOH Not Detected 5 Not Detected Not Detected
    FeCO3 Not Detected 5 Not Detected 15
    FeS Not Detected Not Detected Not Detected Not Detected
    Fe3S4 Not Detected Not Detected Not Detected Not Detected
    a-Iron Not Detected Not Detected Not Detected Not Detected
    a-SiO2 3 Not Detected 2 Not Detected
    CaCO3 3 5 5 1
    NaCl Not Detected Not Detected Not Detected Not Detected
    Sulfur Not Detected 30 Not Detected Not Detected
    Amorphous Balance Balance Balance Balance

    Total Metals (ppm)


    Chloride <4.9 16 103 57
    Sulfate 54,000 43,000 3,700 44,000
    Calcium 7,200 950 9,400 4,700
    Chromium 160 11 98 240
    Copper 190 40 150 220
    Iron 110,000 17,000 65,000 20,000
    Lead 170 25 8,100 160
    Magnesium 660 70 230 310
    Manganese 1,100 160 660 1,300
    Sodium 2,100 1,500 12,000 <500
    Nickel 170 15 100 110
    Zinc 160 420 1 1

    Bacteriology
    Slime Bacteria No Growth No Growth No Growth No Growth
    Fungi No Growth No Growth No Growth No Growth
    Sulfate Reducing
    Bacteria- 100,000 100,000 10,000 10,000
    Bacteria/gram or ml of sludge
    Nitrifying Bacteria None isolated None isolated None isolated None isolated
    Iron-Oxidizing Bacteria None isolated None isolated None isolated None isolated
    Biomass (ATP) – grams of
    ATP/gram or ml of sludge < 6.3x10-11 < 2.4 x 10-10 < 2.6x10-10 < 6.3x10-11

    Internal Corrosion for Pipelines – Advanced Page | 1


    Solid Sample Analysis Report

    Sample ID: Date Collected:


    Analyses/Method Result Rep. Limit Dil. Factor Date Analyzed Analyst Seq. #
    Energy Dispersive X-Ray Spectrometry Units: %
    Aluminum (Al) 0.1 0 1
    Barium (Ba) ND 0 1
    Bromine (Br) ND 0 1
    Calcium (Ca) 0.68 0 1
    Carbon (C) 28.72 0 1
    Chlorine (Cl) 2.57 0 1
    Chromium (Cr) ND 0 1
    Iron (Fe) 17.01 0 1
    Magnesium (Mg) ND 0 1
    Manganese (Mn) ND 0 1
    Nickel (Ni) ND 0 1
    Oxygen (O) 31.71 0 1
    Phosphorus (P) ND 0 1
    Potassium (K) ND 0 1
    Silicon (Si) ND 0 1
    Sodium (Na) 1.89 0 1
    Sulfur (S) 17.33 0 1
    Zinc (Zn) ND 0 1

    Ion Chromatography Units: mg/kg


    Bromide ND 50 10
    Chloride 4,580 500 100
    Fluoride ND 50 10
    Sulfate 57.6 50 10

    Metals by Method 6010B, Total Units: mg/kg


    Calcium 5,410 10 1
    Chromium 110 1 1
    Copper 80.2 1 1
    Iron 189,000 40 20
    Lead ND 500 100
    Magnesium 390 10 1
    Manganese 1,200 0.5 1
    Nickel 30.9 2 1
    Sodium 13,500 50 1
    Zinc 90.6 2 1

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    Liquid Sample Analysis Report

    Analyses Result RL Qual Units DF

    Inorganic Anions E300.0


    Bromide 600 10 H mg/L 100
    Chloride 180,000 1,000 EH mg/L 5000
    Fluoride ND 10 H mg/L 100
    Nitrate ND 5.0 H mg/L 100
    Nitrite ND 5.0 H mg/L 100
    Ortho-Phosphate-P ND 100 H mg/L 100
    Sulfate 210 10 H mg/L 100

    Specific Gravity (Liquids, Hydrometer) ASTM-D891


    Specific Gravity 1.2 0 1

    Metals – Materials Science Group by ICP-OES SW6010R


    Aluminum 584 0 H mg/kg 1
    Barium 1,810 0 H mg/kg 1
    Calcium 10,500 0 H mg/kg 1
    Iron 3,400 0 H mg/kg 1
    Magnesium 1,640 0 BH mg/kg 1
    Manganese 20.3 0 H mg/kg 1
    Phosphorus 65.1 0 H mg/kg 1
    Potassium 382 0 BH mg/kg 1
    Silicon 1.94 0 H mg/kg 1
    Sodium 55,100 0 H mg/kg 1

    Alkalinity A2320
    Alkalinity, Total (as CaCO3) 780 10 H mg/L CaCO3 1

    Total Dissolved Solids A2540C


    Residue, Dissolved 270,000 5.0 BH mg/L 1

    Qualifiers: */X Value exceeds Maximum Contaminant Level B Analyte detected in the associated Method Blank
    E Value above quantitation range H Holding times for preparation or analysis exceeded
    J Analyte detected below quantitation limits M Manual Integration used to determine area response
    ND Not Detected at the Reporting Limit RL Reporting Detection Limit
    S Spike Recovery outside accepted recovery limits

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