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    Test Injections Report

    Uploaded by

    Riad Manamanni
    This document reports the results of test injections on a chromatography system. It shows that the retention time, area, and height for caffeine peaks met the specifications, demonstrating the system is ready for use. Chromatograms and data tables with results are included.

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd

    Test Injections Report

    Uploaded by

    Riad Manamanni
    35 views3 pages
    This document reports the results of test injections on a chromatography system. It shows that the retention time, area, and height for caffeine peaks met the specifications, demonstrating the system is ready for use. Chromatograms and data tables with results are included.

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    © © All Rights Reserved

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    This document reports the results of test injections on a chromatography system. It shows that the retention time, area, and height for caffeine peaks met the specifications, demonstrating the system is ready for use. Chromatograms and data tables with results are included.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    35 views3 pages

    Test Injections Report

    Uploaded by

    Riad Manamanni
    This document reports the results of test injections on a chromatography system. It shows that the retention time, area, and height for caffeine peaks met the specifications, demonstrating the system is ready for use. Chromatograms and data tables with results are included.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    You are on page 1of 3

    TEST INJECTIONS REPORT

    AC Q U I SI TI O N I N F O R M ATI O N

    System Name: Del_Patrol2 Acquired By: Jennb


    Project Name: SQT_PATrol_TUV_CM_rev C Column serial Number: 11581505610K
    Sample Set Method: 010 Test Injections Sample Kit 1 Expiration date: 10/22/2010 12:00:00 AM
    Processing Method Test Injections PM Sample Kit 1 Lot Number: N070015
    Report Method Name: Test Injection Report Build Version: Empower 2 Software Build 2154 SPs
    User Name: System Installed:
    Sample Set Feature Release 5
    Id: 10333 DB ID:
    Result 847558692
    Set Id 10350
    Sample Set Name: Test Injections Sample Set Start Date: 10/25/2010 5:13:39 PM

    Test Injections are performed after preparing the chromatographic system to equilibrate the system and column.
    The SD of the Retention Time, %RSD of Area and Height demonstrates the readiness of the system to be qualified.

    The SD for the Caffeine peak RT should be < or = 1.5 seconds, the %RSD for Area should be < or = 0.75% and
    the %RSD for Height should be < or = 2.4%.

    Caffeine Results Table

    Area %RSD Area Area %RSD Height %RSD Height Height %RSD
    Specification % RSD Pass Fail Specification %RSD Pass Fail
    1 %RSD < or = 0.75 0.23 PASS %RSD < or = 2.4 0.2 PASS

    Caffeine Retention Time (sec) Results Table

    Retention time (sec) Retention time (sec)


    Retention time (sec)
    Standard Deviation Standard Deviation
    Standard Deviation
    Specification Pass Fail
    1 SD RT < or = 1.5sec 0.0 PASS

    Printed 8:29:43 AM US/Eastern 11/17/2010 Page: 1 of 3


    TEST INJECTIONS REPORT

    AC Q U I SI TI O N I N F O R M ATI O N

    System Name: Del_Patrol2 Acquired By: Jennb


    Project Name: SQT_PATrol_TUV_CM_rev C Column serial Number: 11581505610K
    Sample Set Method: 010 Test Injections Sample Kit 1 Expiration date: 10/22/2010 12:00:00 AM
    Processing Method Test Injections PM Sample Kit 1 Lot Number: N070015
    Report Method Name: Test Injection Report Build Version: Empower 2 Software Build 2154 SPs
    User Name: System Installed:
    Sample Set Feature Release 5
    Id: 10333 DB ID:
    Result 847558692
    Set Id 10350
    Sample Set Name: Test Injections Sample Set Start Date: 10/25/2010 5:13:39 PM

    Test Injections Chromatograms

    Caffeine Solution

    1.50

    1.00
    AU

    Caffeine

    0.50

    0.00

    1.50

    1.00
    AU

    Caffeine

    0.50

    0.00

    1.50

    1.00
    AU

    Caffeine

    0.50

    0.00
    0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 2.00 2.20
    Minutes

    Printed 8:29:43 AM US/Eastern 11/17/2010 Page: 2 of 3


    TEST INJECTIONS REPORT

    AC Q U I SI TI O N I N F O R M ATI O N

    System Name: Del_Patrol2 Acquired By: Jennb


    Project Name: SQT_PATrol_TUV_CM_rev C Column serial Number: 11581505610K
    Sample Set Method: 010 Test Injections Sample Kit 1 Expiration date: 10/22/2010 12:00:00 AM
    Processing Method Test Injections PM Sample Kit 1 Lot Number: N070015
    Report Method Name: Test Injection Report Build Version: Empower 2 Software Build 2154 SPs
    User Name: System Installed:
    Sample Set Feature Release 5
    Id: 10333 DB ID:
    Result 847558692
    Set Id 10350
    Sample Set Name: Test Injections Sample Set Start Date: 10/25/2010 5:13:39 PM

    Chromatographic Peak Results

    Retention Time Retention time Area Height Points


    Injection Name Result Id
    (min) (sec) (µV*sec) (µV) Across Peak
    1 1 Caffeine 0.953 57.16 2500166.422 1615250.50 54 10380
    2 2 Caffeine 0.953 57.16 2497171.110 1613416.99 54 10381
    3 3 Caffeine 0.952 57.11 2489101.762 1607562.44 54 10382
    Mean 57.15 2495479.765 1612076.64
    Std. Dev. 0.03 5722.951 4015.46
    % RSD 0.229 0.25

    Printed 8:29:43 AM US/Eastern 11/17/2010 Page: 3 of 3

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