B Tech Syllabus-ChemE2022 1

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B. TECH.

SYLLABUS
Department of Chemical Engineering

Faculty of Technology
Dharmsinh Desai University,
Nadiad – 387 001, Gujarat, India.
(2021-2022 onwards)

https://www.ddu.ac.in
TEACHING SCHEME FOR THE COURSE DEPLOMA
CHEMICAL ENGINEERING
L – Lecture T – Tutorial P – Practical
Th. – Theory Ext - External S – Sessional
TW – Term Work Teaching Scheme – hr/week V – Viva

SEMESTER-I
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
BSC101 Mathematics-I 3 1 0 60 40 0 0 100 4
ESC102 Thermodynamics-I 3 0 2 60 40 25 25 150 4
Basic Electrical
ESC103a 3 0 2 60 40 25 25 150 4
Engineering
ESC105a Engineering Mechanics 3 1 0 60 40 0 0 100 4
Computer
ESC103 2 0 3 40 0 25 25 90 3.5
Programming
ESC106a Workshop Practice-I 0 0 2 0 0 25 25 50 1
MC-II Environmental Studies 2 0 0 40 0 0 0 40 0
TOTAL 16 2 9 320 160 100 100 680 20.5

SEMESTER-II
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
BSC104 Mathematics-II 3 1 0 60 40 0 0 100 4
ESC101 Engineering Graphics 3 0 3 60 40 25 25 150 4.5
BSC103 Chemistry 3 0 0 60 0 0 0 60 3
ESC103b Basic Electronics 3 0 2 60 40 25 25 150 4
BSC105b Mechanics of Solids 3 0 2 60 40 25 25 150 4
ESC106b Workshop Practice-II 0 0 3 0 0 25 25 50 1.5
TOTAL 15 1 10 300 160 100 100 660 21

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 1


SEMESTER-III
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
Introduction to
PCCXXX 2 0 2 40 0 25 25 90 3
Chemical Engineering
BS107 Chemistry-II 3 0 3 60 40 25 25 150 4.5
General Chemical
PCC113 3 0 2 60 40 25 25 150 4
Technology
Material & Energy
PCC101 Balance 3 1 0 60 40 0 0 100 4
Computations
BS102 Physics 2 0 2 40 0 25 25 90 3
HSMC101 English 2 0 2 40 0 0 50 90 3
TOTAL 15 1 11 300 120 150 100 670 21.5

SEMESTER-IV
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
PCC104 Heat Transfer 3 0 3 60 40 25 25 150 4.5
PCC105 Mass Transfer - I 3 1 0 60 40 0 0 100 4
PCC106 Fluid Mechanics 3 0 3 60 40 25 25 150 4.5
Particles and Fluid
PCC111 3 0 3 60 40 25 25 150 4.5
Particle Processing
PCC103 Thermodynamics -II 3 1 0 60 40 0 0 100 4
Effective Technical
HSMC201 3 0 0 40 0 0 0 40 3
Communication
TOTAL 18 2 9 340 200 75 75 690 24.5

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 2


SEMESTER-V
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
Chemical Reaction
PCC108 3 0 3 60 40 25 25 150 4.5
Engineering-I
PCC109 Mass Transfer-II 3 1 3 60 40 25 25 150 5.5
PEC101 Core Elective-I 3 1 0 60 40 0 0 100 4
OEC101 Open Elective-I 3 0 0 60 0 0 0 60 3
Numerical Techniques
PCC107 in Chemical 3 0 2 60 40 25 25 150 4
Engineering
Financial and
HS103 Management 3 0 0 40 0 0 0 40 3
Accounting
TOTAL 18 2 8 340 160 75 75 650 24

SEMESTER-VI
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
Chemical Reaction
PCC112 3 0 3 60 40 25 25 150 4.5
Engineering-II
Chemical System
PCCXXX 3 1 0 60 40 0 0 100 4
Modeling
Instrumentation and
PCC117 3 1 3 60 40 25 25 150 5.5
Process Control
Process Equipment
PCCXXX 3 0 3 60 40 25 25 150 4.5
Design and Drawing
Core Elective-II (1),
PEC102 3 0 0 60 0 0 0 60 3
(2), (3)
OEC102 Open Elective-II 3 0 0 60 0 0 0 60 3
TOTAL 18 2 9 360 160 75 75 670 24.5

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 3


SEMESTER-VII
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
PCC116 Design and
2 0 4 60 40 25 25 150 4
Simulation Lab
PCC113 Process Technology
3 1 0 60 40 0 0 100 4
and Economics
PCC102 Transport Phenomena 3 0 3 60 40 25 25 150 4.5
ESC107 Material Science 3 0 0 40 0 0 0 40 3
PEC104 Core Elective-III (1),
3 0 0 40 0 0 0 40 3
(2)
OEC103 Open Elective-III 3 0 0 40 0 0 0 40 3
TOTAL 17 1 7 300 120 50 50 520 21.5

SEMESTER-VIII
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
HS104 Universal Human
2 1 0 40 0 0 0 40 3
Value-II
PEC103 Core Elective-IV 2 0 2 40 0 25 25 90 3
PROJ Industrial Internship 0 3 12 0 0 150 100 250 9
PROJ Working Project 1 0 4 0 0 50 50 100 3
TOTAL 5 4 18 80 0 175 225 480 18

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 4


SEMESTER-I
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
BSC101 Mathematics-I 3 1 0 60 40 0 0 100 4
ESC102 Thermodynamics 3 0 2 60 40 25 25 150 4
Basic Electrical
ESC103a 3 0 2 60 40 25 25 150 4
Engineering
ESC105a Engineering Mechanics 3 1 0 60 40 0 0 100 4
Computer
ESC103 2 0 3 40 0 25 25 90 3.5
Programming
ESC106a Workshop Practice-I 0 0 2 0 0 25 25 50 1
MC-II Environmental Studies 2 0 0 40 0 0 0 40 0
TOTAL 16 2 9 320 160 100 100 680 20.5

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 5


B. TECH. – SEMESTER-I (CH)
MATHEMATICS-I (BSC101)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 1 0 4 4 60 40 0 50 150

A. COURSE CONTENT
TOPICS
1. Calculus: Integral Calculus
Evolutes and involutes, Applications of definite integrals to evaluate surface areas and
volumes of revolutions
2. Calculus
Rolle’s Theorem, Mean value theorems, Taylor’s and Maclaurin theorems with
remainders; Indeterminate forms and L'Hospital's rule, Maxima and minima.
3. Linear Algebra Matrices, Vectors, Determinants, Linear Systems
Matrices, Vectors: Addition and Scalar Multiplication, Matrix Multiplication, Rank of a
matrix, Solutions of Linear Systems: Existence, Uniqueness, Determinants, Cramer’s Rule,
Inverse of a matrix, Eigenvalues, Eigenvectors, Symmetric, Skew-symmetric, Linear.
Independence of vectors, Diagonalization
4. Sequence and Series
Convergence of sequence and series, Introduction to tests for convergence; Power series,
Series for exponential, Trigonometric and logarithm functions; Fourier series: Half range
sine and cosine series, Parseval’s theorem.
5. Multivariable Calculus (Differentiation)
Partial derivatives, Total derivative; Tangent plane and normal line; Taylor series
expansion for function of two variables, Jacobians, Maxima, minima and saddle points;
Method of Lagrange multipliers, Introduction to Vector Differential Calculus; Directional
derivatives, Gradient, Curl and divergence

B. TEXT / REFERENCE BOOKS


1. B. S. Grewal, Higher Engineering Mathematics, Khanna Publishers, 40th Edition, 2007
2. G.B. Thomas and R.L. Finney, Calculus and Analytic geometry, 9th Ed. Pearson, 2002
3. Erwin Kreyszig, Advanced Engineering Mathematics, 9th Edition, John Wiley & Sons,
2006
4. D. Poole, Linear Algebra: A Modern Introduction, 2nd Edition, Brooks/Cole, 2005
5. Veerarajan T., Engineering Mathematics for first year, Tata McGraw-Hill, New Delhi,
2008
6. Ramana B.V., Higher Engineering Mathematics, Tata McGraw Hill New Delhi, 2010
7. N.P. Bali and Manish Goyal, A text book of Engineering Mathematics, Laxmi
Publications, Reprint, 2010
8. V. Krishnamurthy, V.P. Mainra and J.L. Arora, An introduction to Linear Algebra,
Affiliated East–West press, Reprint 2005

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 6


B. TECH. – SEMESTER-I (CH)
THERMODYNAMICS-I (ESC102)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 2 5 4 60 40 25 25 150

A. COURSE CONTENT
TOPICS
1. Introduction
Macroscopic versus microscopic view point, thermodynamic systems and control volume,
thermodynamic properties, processes and cycles, homogeneous and heterogeneous systems,
thermodynamic equilibrium, quasi-static process, pure substance, concept of continuum,
temperature and zeroth law of thermodynamics, ideal gas and gas laws
2. Energy and Energy Transfer
Forms of energy, energy transfer by heat and work, mechanical forms of work, first law of
thermodynamics, energy conversion efficiencies
3. Properties of Pure Substances
Pure substance, phases and phase change process, thermodynamic properties, property
diagrams, ideal gas equation of state, van der waal equation, virial equation of state
4. Energy Analysis of Closed System
PdV work in various quasi-static processes, energy balance, specific heats, internal energy,
enthalpy and specific heats of solids, liquids and ideal gases
5. Energy Analysis of Open System
Conservation of mass, flow work and energy of a flowing fluid, energy analysis of steady
and unsteady flow systems.
6. Second Law of Thermodynamics
Introduction to second law, thermal energy reservoir, heat engine, refrigerator and heat
pump, Clausis and Kelvin-Plank statement, perpetual motion machines, reversible and
irreversible processes, Carnot and reversed Carnot cycle, , entropy principle and isentropic
process, TdS and Maxwell relation
7. Seam Boilers
Introduction, classification, mountings and accessories, classification and comparison of
boiler draught systems
8. Applications of Thermodynamics
Construction and working of pumps, compressors, IC engine- Otto and Diesel engines,
vapour compression refrigeration system, vapour absorption refrigeration system

B. TEXT / REFERENCE BOOKS


1. Yunus A. Cengel, Michael A. Boles., “Thermodynamics- An engineering approach”, Tata
McGraw Hill publishing co. ltd.
2. Nag P.K., “Engineering Thermodynamics”, Tata McGraw Hill publishing co. ltd
3. Smith J.M., Van Ness H.C., Abbott M.M, “Introduction to chemical engineering
thermodynamics”, McGraw Hill publishing co. Ltd
4. Sonntag. R.E., Borgnakke, C. and Van Wylen G.J.,” Fundamental of thermodynamics”,
John Wiley and Sons
5. Moran M.J. and Shapiro H.N., “Fundamentals of engineering thermodynamics”, John
Wiley and Sons

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 7


B. TECH. – SEMESTER-I (CH)
BASIC ELECTRICAL ENGINEERING (ESC103a)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 2 5 4 60 40 25 25 150

A. COURSE CONTENT
TOPICS
1. DC Circuits
Electrical circuit elements (R, L and C), voltage and current sources, Kirchhoff current
and voltage laws, analysis of simple circuits with dc excitation. Superposition, Thevenin
and Norton Theorems. Time-domain analysis of first- order RL and RC circuits
2. AC Circuits
Representation of sinusoidal waveforms, peak and rms values, phasor representation, real
power, reactive power, apparent power, power factor, Analysis of single-phase ac circuits
consisting of R, L, C, RL, RC, RLC combinations (series and parallel), resonance. Three-
phase balanced circuits, voltage and current relations in star and delta connections.
3. Transformers
Magnetic materials, BH characteristics, ideal and practical transformer, equivalent circuit,
losses in transformers, regulation and efficiency. Auto- transformer and three-phase
transformer connections
4. Electrical Machines
Generation of rotating magnetic fields, Construction and working of a three- phase
induction motor, Significance of torque-slip characteristic. Loss components and
efficiency, starting and speed control of induction motor. Single-phase induction motor.
Construction, working, torque-speed characteristic and speed control of separately
excited dc motor. Construction and working of synchronous generators
5. Electrical Installations
Components of LT Switchgear: Switch Fuse Unit (SFU), MCB, ELCB, MCCB, Types of
Wires and Cables, Earthling. Elementary calculations for energy consumption, power
factor improvement. DC-DC buck and boost converters. Single-phase and three-phase
voltage source inverters; sinusoidal modulation
6. Semiconductors, Diodes and Applications
Semiconductor Diode - Ideal versus Practical, Resistance Levels, Diode Equivalent
Circuits, Load Line Analysis; Diode as a Switch, Diode as a Rectifier, Half Wave and
Full Wave Rectifiers with and without Filters; Breakdown Mechanisms, Zener Diode –
Operation and Applications; Opto-Electronic Devices – LEDs, Photo Diode and
Applications; Silicon Controlled Rectifier (SCR) in brief

B. TEXT / REFERENCE BOOKS


1. Basic Electrical, Electronics and Computer Engineering, R. Muthu Subramanian, S.
Salivahanan, K. A. Muraleedharan, 2ndEdition, Tata McGraw Hill
2. Principles of Electronics, V. K. Mehta & Rohit Mehta, 11th Edition, S. Chand &
Company
3. Electrical Technology (Vol: II), B. L. Theraja , A. K. Theraja, 23rdEdition, S. Chand &
Company
4. Basic Electrical Engineering, D.P. Kothari, I. J. Nagrath, 3rd Edition, Tata McGraw Hill

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 8


B. TECH. – SEMESTER-I (CH)
ENGINEERING MECHANICS (ESC105a)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 1 0 4 4 60 40 0 0 100

A. COURSE CONTENT
TOPICS
1. Statics
Resultant force for 2D and 3D force system, concept of free body diagrams, equilibrium
equations for particles and rigid body subjected to 2D and 3D force system, centroid and
centre of gravity, moment of inertia.
2. Dynamics and Vibrations
Rotational Transformation of scalers and vectors, Newton’s Laws for particle motion,
Potential Energy function F=-Grad(V), conservative and non-conservative forces,
Conservation of momentum, angular momentum, collision, energy equation, free
harmonic motion, damped harmonic motion, forced oscillation and resonance, kinematics
in a coordinate system rotating and translating in a plane.

B. TEXT / REFERENCE BOOKS


1. Engineering Mechanics, M. K. Harbola, 2nd Edition, Cengage Learning, 2013
2. Mechanics – J P Den Hartog, Dover Publications, 2003
3. Mechanical Vibrations - J P Den Hartog, Dover Publications, 1985
4. Theory of Vibrations with Applications – W. T. Thomson, 5th Edition, Pearson
Education, 2008
5. Engineering Mechanics: Statics (V.1), Dynamics (V.2), J. L. Meriam and L. G. Kraige,
5th Edition, Wiley, 2017
6. Engineering Mechanics: Statics & Dynamics, Irving H. Shames, 4th Edition, Pearson
Education, 2005
7. Vector Mechanics for Engineers: Statics (V.1), Dynamics (V.2), F. P. Beer and E. R.
Johnson, 10th SI edition, McGraw Hill Education, 2017

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 9


B. TECH. – SEMESTER-I (CH)
COMPUTER PROGRAMMING (ESC103)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
2 0 3 5 3.5 40 0 25 25 90

A. COURSE CONTENT
TOPICS
1. Introduction
Introduction to components of computer system, Idea of algorithm, Introduction to C,
Constants, Variables & Data types in C, Managing input and Output operators
2. Operators and expressions
C Operators: Arithmetic, relational, logical, increment & decrement, assignment and
conditional, Arithmetic Expressions & Precedence Rule, Type conversion in C,
Mathematical
3. Decision Making and Branching
Decision making with If & If...else statements, goto statements
4. Decision Making and Looping
The while statement, the break statement & the do... while loop, the for loop, Jump within
loops - Programs.
5. Arrays
Array 1D, 2D, Character Array as String
6. User Defined Functions
Categories of Functions (Including using built in library), Call by Value, Parameter
passing to function, Recursion.
7. Structure
Defining structure, Assigning value to the structure members, Array of structure
8. Pointer
Idea of pointer, declaration and Initialization of pointer, passing address as function
argument, passing array to function using pointer
9. File Handling

B. TEXT / REFERENCE BOOKS


1. E. Balaguruswamy, Programming in ANSI C, Tata McGraw-Hill
2. Yashvant Kanetkar, Let Us C, 12th Edition, BPB Publication
3. Yashvant Kanetkar, Let Us C, 12th Edition, BPB Publication
4. Brian W. Kernighan and Dennis M. Ritchie, The C Programming Language, Prentice Hall
of India

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 10


B. TECH. – SEMESTER-I (CH)
ENVIRONMENTAL STUDIES (MC-II)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
2 0 0 2 0 40 0 0 0 40

A. COURSE CONTENT
TOPICS
1. The Multidisciplinary Nature of Environmental Studies
Definition, scope and importance & Need for public awareness
2. Natural Resources
Renewable and non-renewable resource: Natural resources and associated problems, Forest
resources: Use and over-exploitation, deforestation, case studies. Timber extraction,
mining, dams, and their effects on forests and tribal people ,Water resources: Use and over-
utilization of surface and ground water, floods, drought, conflicts over water, dams benefit
and problems, Mineral resources: Use and exploitation, environmental effects of extracting
and using mineral resources, case studies, Food resources: World food problems, changes
caused by agriculture and overgrazing, effects of modern agriculture, fertilizer-pesticide
problems, water logging, salinity, case studies, Energy resources: Growing energy needs,
renewable and non-renewable energy sources, use of alternate energy sources, case studies,
Land resources: Land as a resource, land degradation, man induced landslides, soil erosion
and desertification, Role of an individual in conservation of natural resources. Equitable
use of resources of sustainable lifestyles
3. Ecosystems
Concept of an ecosystem, Structure and function of an ecosystem, producers, consumers
and decomposers, Energy flow in the ecosystem, Ecological succession, Food chains,
food webs and ecological pyramids, Introduction, types, characteristic features, structure
and function of the following ecosystem: Forest ecosystem, Grassland ecosystem, Desert
ecosystem and Aquatic ecosystem (ponds, streams, lakes, rivers, oceans, estuaries)
4. Biodiversity and Its Conservation
Introduction definition: Genetic, species and ecosystem diversity, Bio-geographical
classification of India, Value of biodiversity: Consumptive use, productive use, social,
ethical, aesthetic and option values. Biodiversity at global, national and local levels, India
as a mega diversity nation, Hot-spots of biodiversity, Threats to biodiversity, habitat loss,
poaching of wildlife, man-wildlife conflicts, Endangered and endemic species of
India, Conservation of biodiversity: In-situ and ex-situ conservation of biodiversity
5. Environmental Pollution
Definition, Causes, effects and control measures of: Air pollution, Water pollution, Soil
pollution, Marine pollution, Noise pollution, Thermal pollution, Nuclear hazards, Solid
waste management, causes, effects and control measures of urban and industrial wastes,
Role of an individual in prevention of pollution, Pollution case studies, Disaster
management: floods, earthquake, cyclone and landslides
6. Social Issues and The Environment
From unsustainable to sustainable development, Urban problems related to energy, Water
conservation, rain water harvesting, watershed management, Resettlement and
rehabilitation of people: its problems and concerns. Case studies, Environmental ethics:
Issues and possible solutions, Climate change: Global warming, acid rain, ozone layer
depletion, nuclear accidents and holocaust, Case studies, Wasteland reclamation,
Consumerism and waste products, Environment Protection Act: Air (Prevention and
Control of Pollution) Act, Water (Prevention &Control of Pollution) Act, Wildlife

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 11


Protection Act, Forest Conservation Act, Issues involved in enforcement of environmental
legislation, Public awareness
7. Human Population and The Environment
Population growth, variation among nations, population explosion, Family Welfare
Program, environment and human health, human rights, Value education, HIV/AIDS,
Women and Child Welfare, Role of Information Technology in Environmental and
human health, Case studies
8. Field Work
Visit to a local area to document environmental assets (river/ forest/ grassland/ hill/
mountain), Visit to a local polluted site - Urban/Rural/Industrial/Agricultural, Study of
common plants, insects, birds, Study of simple ecosystems – pond, river, hill, slopes etc.

B. TEXT / REFERENCE BOOKS


1. Erach Bharucha Textbook of Environmental Studies; Second Edition, Universities Press:
Hyderabad, 2013
2. Rajagopalan, R. Environmental Studies; Oxford University Press: India, 2015
3. Varandani, N. S. Basics of Environmental studies; Lambert Academic Publishing:
Germany, 2013
4. Rao, C. S. Environmental Pollution Control Engineering; Wiley publishers: New Delhi,
2006
5. Clark, R. S. Marine Pollution; Clanderson Press Oxford: Bath, 2001
6. Cunningham, W.P.; Cooper; Gorhani, T. H. E.; Hepworth, M.T., Environmental
Encyclopedia; Jaico Publ. House: Mumbai, 2001
7. De, A. K. Environmental Chemistry; Wiley Eastern: New Delhi, 2006

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 12


B. TECH. – SEMESTER-I (CH)
WORKSHOP PRACTICE-I (ESC106a)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
0 0 2 2 1 0 0 25* 25 50
*TW Marks includes Viva based on TW

A. COURSE CONTENT
TOPICS
1. Introduction to Workshop, Basic Workshop types
2. Safety requirement in workshop, Safety rules
3. To Understand "5S" Concept for Workplace
4. Demonstration of Tin smithy Tools and it's exercise
5. To make job for Tin smithy shop
6. Demonstration of Plumbing tools, It's accessories.
7. To make job for Plumbing shop
8. Introduction to Fabrication shop, Welding Equipment
9. To make job for Fabrication shop
10. Introduction of Machine shop
11. Introduction and Demonstration of Lathe machine
12. Introduction and Demonstration of Milling and Radial Drilling m/c

B. TEXT / REFERENCE BOOKS


1. Erach Bharucha Textbook of Environmental Studies; Second Edition, Universities Press:
Hyderabad, 2013

BACK

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 13


SEMESTER-II
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
BSC104 Mathematics-II 3 1 0 60 40 0 0 100 4
ESC101 Engineering Graphics 3 0 3 60 40 25 25 150 4.5
BSC103 Chemistry 3 0 0 60 0 0 0 60 3
ESC103b Basic Electronics 3 0 2 60 40 25 25 150 4
BSC105b Mechanics of Solids 3 0 2 60 40 25 25 150 4
ESC106b Workshop Practice-II 0 0 3 0 0 25 25 50 1.5
TOTAL 15 1 10 300 160 100 100 660 21

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 14


B. TECH. – SEMESTER-II (CH)
MATHEMATICS-II (BSC104)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 1 0 4 4 60 40 0 0 100

A. COURSE CONTENT
TOPICS
1. First Order Ordinary Differential Equations and Introduction to Higher Order
Differential Equations
Exact, linear and Bernoulli’s equations, Introduction to second order linear differential
equations with variable coefficients, Method of variation of parameters, Cauchy-Euler
equation.
2. Series Solution of Ordinary Differential Equations By Power Series Method
Introduction, Validity of series solution of the equation, General Method, Forms of series
solution.
3. Partial Differential Equations
Basic Concepts, Classification and Solutions of partial differential equations: Lagrange’s
linear equation of first order, Non-linear equations of first order- Charpit's method,
Homogenous linear equations with constant coefficient to find the complementary
functions and the particular integral, Introduction to non-homogenous linear equations
with constant
coefficients, Method of separation of variables.
4. Multivariable Calculus (Integration)
Multiple Integration: Double integrals (Cartesian), Change of order of integration in
double integrals, Change of variables (Cartesian to polar), Introduction to Triple integrals
(Cartesian), Vector line integrals, Vector surface integrals, Theorems of Green, Gauss and
Stoke’s.
5. Laplace Transform
Laplace Transform, Properties of Laplace Transform, Laplace transform of periodic
functions, finding inverse Laplace transform by different methods, Convolution theorem,
Evaluation of integrals by Laplace transform, Solving ODE by Laplace Transform
method

B. TEXT / REFERENCE BOOKS


1. B. S. Grewal, Higher Engineering Mathematics, Khanna Publishers, 40th Edition, 2007
2. G.B. Thomas and R.L. Finney, Calculus and Analytic geometry, 9th Ed. Pearson, 2002
3. Erwin Kreyszig, Advanced Engineering Mathematics, 9th Edition, John Wiley & Sons,
2006
4. W. E. Boyce and R. C. DiPrima, Elementary Differential Equations and Boundary Value
Problems, 9th Edn., Wiley India, 2009
5. S. L. Ross, Differential Equations, 3rd Ed., Wiley India, 1984
6. E. A. Coddington, An Intro. to Ordinary Differential Equations, Prentice Hall India, 1995
7. J. W. Brown & R. V. Churchill, Complex Variables and Applications, 7th Ed., Mc-Graw
Hill, 2004
8. N.P. Bali and Manish Goyal, A text book of Engineering Mathematics, Laxmi Pub., 2008

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 15


B. TECH. – SEMESTER-II (CH)
ENGINEERING GRAPHICS (ESC101)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 3 6 4.5 60 40 25 25 150

A. COURSE CONTENT
TOPICS
1. Introduction to Engineering Drawing
Principles of Engineering Graphics and their significance, usage of Drawing instruments,
lettering, Conic section curves (Ellipse, Parabola, Hyperbola), Cycloidal Curves
(Cycloid, Epicycloid, Hypocycloid), Involutes; Archemedian Spiral
2. Solid Geometry
Projection of points, projection of lines and their applications. Projection of regular planes
such as square, rectangle, triangle, circle, pentagon, hexagon, rhombus. Projection of right
and regular solids inclined to both the planes (prisms, pyramids, cylinder and cone)
3. Orthographic Projections
First angle and third angle projection methods, conversion of pictorial views into
Orthographic projections with dimensioning, sectional orthographic projection, special
sections
4. Section of Solids and Development of Solids
Sections and Sectional Views of Right Angular Solids Covering, Prism, Cylinder,
Pyramid, Cone
5. Envelopment of Surfaces
Development of surfaces of Right Regular Solids - Prism, Pyramid, Cylinder and Cone
6. Isometric Projections
Principles of Isometric projection – Isometric Scale, Isometric projection and view,
Conversion of orthographic views to isometric projections and views
7. Working Environment of CAD Software
Menu bar, Quick access toolbar, Dashboard/Ribbon, Toolbars, drawing space, Navigation bar
(View controls: zoom, pan, orbit), Command prompt, Status bar, Drawing Area (Background,
Crosshairs, Coordinate System), Shortcut Menu, Properties manager
8. Drawing Customization
Setting up the drawing sheet (drawing sheet templates, drawing limits, drawing units etc.),
Coordinate system (User coordinate system, Absolute and relative coordinates, Cartesian
and Polar coordinates), Modes of drawing (Grid, Snap, Ortho, Osnap, Otrack, Polar
tracking, Iso draft, etc.) Formatting (colours, line type, line weight, point style etc.)
9. Preparing Computer Aided Drawing
Exploring various commands with exercises of Orthographic drawing views and Isometric
drawing views using different drawing tools, modifying tools, dimensioning tools etc.
10. Plotting and Exchanging Drawing
Printing/Plotting the drawing (page setup, plot area, plot scale, drawing orientation, plot
options etc.), Drawing standard (DXF), Generating PDF drawing documents, file
management

B. TEXT / REFERENCE BOOKS


1. Bhatt N.D., Panchal V.M. & Ingle P.R., (2014), Engineering Drawing, Charotar
Publishing House
2. Narayana, K.L. & P Kannaiah (2008), Text book on Engineering Drawing, Scitech
Publishers

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 16


3. Shah P. J., (2014) Engineering Graphics, S. Chand Publishing
4. Luzadder W., Duff J., (1992), Fundamentals of Engineering Drawing, Peachpit Press
5. Gill P. S., (2009), Engineering Drawing, S. K. Kataria & Sons
6. Agrawal B. & Agrawal C. M. (2012), Engineering Graphics, TMH Publication

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 17


B. TECH. – SEMESTER-II (CH)
CHEMISTRY (BSC103)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 0 3 3 60 0 0 0 60

A. COURSE CONTENT
TOPICS
1. Atomic and Molecular Structure
Schrodinger equation. Particle in a box solution and their applications for conjugated
molecules and nanoparticles. Forms of the hydrogen atom wave functions and the plots of
these functions to explore their spatial variations. Molecular orbitals of diatomic molecules
and plots of the multi centre orbitals. Equations for atomic and molecular orbitals. Energy
level diagrams of diatomics. Pi-molecular orbitals of butadiene and benzene and
aromaticity. Crystal field theory and the energy level diagrams for transition metal ions
and their magnetic properties. Band structure of solids and the role of doping on band
structures.
2. Spectroscopic Techniques and Applications
Principles of spectroscopy and selection rules. Electronic spectroscopy. Fluorescence and its
applications in medicine. Vibrational and rotational spectroscopy of diatomic molecules.
Applications. Nuclear magnetic resonance and magnetic resonance imaging, surface
characterization techniques. Diffraction and scattering.
3. Intermolecular Forces and Potential Energy Surfaces
Ionic, dipolar and van Der Waals interactions. Equations of state of real gases and critical
phenomena. Potential energy surfaces of H3, H2F and HCN and trajectories on these
surfaces.
4. Use of Free Energy in Chemical Equilibria
Thermodynamic functions: energy, entropy and free energy. Estimations of entropy and
free energies. Free energy and emf. Cell potentials, the Nernst equation and applications.
Acid base, oxidation reduction and solubility equilibria. Water chemistry. Corrosion. Use
of free energy considerations in metallurgy through Ellingham diagrams
5. Periodic Properties
Effective nuclear charge, penetration of orbitals, variations of s, p, d and f orbital energies
of atoms in the periodic table, electronic configurations, atomic and ionic sizes, ionization
energies, electron affinity and electronegativity, polarizability, oxidation states,
coordination numbers and geometries, hard soft acids and bases, molecular geometries
6. Stereochemistry
Representations of 3 dimensional structures, structural isomers and stereoisomers,
configurations and symmetry and chirality, enantiomers, diastereomers, optical activity,
absolute configurations and conformational analysis. Isomerism in transitional metal
compounds.
7. Organic Reactions and Synthesis of a Drug Molecule
Introduction to reactions involving substitution, addition, elimination, oxidation, reduction,
cyclization and ring openings. Synthesis of a commonly used drug molecules.

B. TEXT / REFERENCE BOOKS


1. University chemistry, by B. H. Mahan
2. Chemistry: Principles and Applications, by M. J. Sienko and R. A. Plane
3. Fundamentals of Molecular Spectroscopy, by C. N. Banwell
4. Engineering Chemistry (NPTEL Web-book), by B. L. Tembe, Kamaluddin and M.
S. Krishnan

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 18


5. Physical Chemistry, by P. W. Atkins
6. Organic Chemistry: Structure and Function by K. P. C. Volhardt and N. E. Schore,
5th Edition

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 19


B. TECH. – SEMESTER-II (CH)
BASIC ELECTRONICS (ESC103)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 2 5 4 60 40 25 25 150

A. COURSE CONTENT
TOPICS
1. Transistor & Characteristics
Bipolar Junction Transistor (BJT) – Construction, Operation, Amplifying Action,
Common Base, Common Emitter and Common Collector Configurations, Operating
Point, Voltage Divider Bias Configuration
2. Field Effect Transistor (FET)
Construction, Characteristics of Junction FET, Depletion and Enhancement type Metal
Oxide Semiconductor (MOS) FETs, Introduction to CMOS circuit
3. Transistor Amplifiers and Oscillators
Classification, Small Signal Amplifiers – Basic Features, Common Emitter Amplifier,
Coupling and Bypass Capacitors, Distortion, AC Equivalent Circuit; Feedback
Amplifiers – Principle, Advantages of Negative Feedback, Topologies, Current Series
Feedback Amplifiers; Oscillators – Classification, RC Phase Shift
4. Operational Amplifiers and Applications
Introduction to operational amplifiers, Op-amp input modes and parameters, Op-amp in
open loop configuration, op-amp with negative feedback, study of practical op-amp IC
741, and inverting and non-inverting amplifier applications: summing and difference
amplifier, unity gain buffer, comparator, integrator and differentiator, wein bridge
oscillator.
5. Digital Electronics Fundamentals
Difference between analogue and digital signals, Boolean algebra, Basic and Universal
Gates, Symbols, Truth tables, logic expressions, Logic simplification, Logic ICs,
Implementation of combinational logic - half and full adder/subtractor, multiplexers, de-
multiplexers
6. Sensors & Signal Conditioning Circuits
Types of sensors – pneumatic, electromagnetic, electronic, smart sensors. Diaphragm,
bellows and bourdon tube, Resistive, Capacitive, Inductive, ultrasonic, LVDT,
piezoelectric, optoelectronic transducers, thermocouple, RTD and thermistors,
Application of sensors for flow, level, temperature and stress measurement, Bridge
Circuit, Differential Amplifier, Instrumentation Amplifier
7. Transistor & Characteristics
Bipolar Junction Transistor (BJT) – Construction, Operation, Amplifying Action,
Common Base, Common Emitter and Common Collector Configurations, Operating
Point, Voltage Divider Bias Configuration

B. TEXT / REFERENCE BOOKS


1. Principles of Electronics, 11th Edition By V. K. Mehta & Rohit Mehta Publisher: Chand
& Company
2. Electrical & Electronic Measurement & Measuring Instruments, 17th Edition By A.K.
Sawhney Publisher: Dhanpat Rai
3. M. M. Mano, "Digital logic and Computer design", Publisher : Pearson Education India

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 20


B. TECH. – SEMESTER-II (CH)
MECHANICS OF SOLIDS (ESC105b)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 2 5 4 60 40 25 25 150

A. COURSE CONTENT
TOPICS
1. Concept of stress and strain, elasticity, generalized Hooke’s law for 3D, concept of
isotropy and homogeneity, plane stress and plane strain idealization, axial, volumetric and
thermal stresses and strains
2. Transformation of stress and strain at a point, Principal stresses and strains, Mohr’s Circle,
strain rossete
3. Mechanical properties of metals – elasticity, plasticity, strain hardening, hardness,
toughness, fatigue, strain energy
4. Force-strain-deformation analysis for axial load, flexure, shear and torsion

B. TEXT / REFERENCE BOOKS


1. Strength of Materials: Part– I and II, Stephen Timoshenko, 3rd Edition, CBS Publisher,
2002
2. Strength of Materials, Sadhu Singh, 1st Edition, Khanna Book Publishing Company,
2016
3. Advanced Mechanics of Solid, L. S. Srinath, 3rd Edition, McGraw Hill Publication, 2017
4. Engineering Mechanics of Solids, E P Popov, 2nd Edition, Prentice Hall India Learning
Pvt. Ltd, 2002

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 21


B. TECH. – SEMESTER-II (CH)
WORKSHOP PRACTICE-II (ESC106b)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
0 0 3 3 1.5 0 0 25 25 50

A. COURSE CONTENT
TOPICS
1. Introduction to Carpentry Shop, Application of various tools, demonstration & making
of Job 1 & 2, assignment.
2. Introduction to Black smithy shop, demonstration & making of job
3. Introduction to Fitting shop, application of various tools, demonstration & making of Job,
assignment

B. TEXT / REFERENCE BOOKS


1. Equipment Manuals

BACK

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 22


SEMESTER-III
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
Introduction to
PCCXXX 2 0 2 40 0 25 25 90 3
Chemical Engineering
BS107 Chemistry-II 3 0 3 60 40 25 25 150 4.5
General Chemical
PCC113 3 0 2 60 40 25 25 150 4
Technology
Material & Energy
PCC101 Balance 3 1 0 60 40 0 0 100 4
Computations
BS102 Physics 2 0 2 40 0 25 25 90 3
HSMC101 English 2 0 2 40 0 0 50 90 3
TOTAL 15 1 11 300 120 150 100 670 21.5

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 23


B. TECH. – SEMESTER-III (CH)
INTRODUCTION TO CHEMICAL ENGINEERING (PCC---)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
2 0 2 4 3 40 0 25 25 90

A. COURSE OVERVIEW
Motivation: Learn the basics and fundamentals of chemical engineering to entry level students
Objective: Objectives of this course is to understand Fundamental concepts of unit operations and
unit processes, interpret data as table versus plot, draw and read PBD and PFD diagrams, apply
suitable tools relevant to chemical engineering problems and calculations associated to the physio-
chemical properties

B. COURSE CONTENT
TOPICS COs
1. Introduction and fundamentals CO1
About the discipline of chemical engineering, concept of unit operations and unit
processes, operations in batch, semi-batch and continuous mode, flow pattern as co-
current, counter-current and cross-current, concept of fluid solid contacting using
fixed, moving and fluid beds.
2. Overview of Chemical Process Industries (CPI) CO2
Satisfactory definition of CPI/GCT, important chemical process industries, its
typical raw materials, products and end usages.
3. Role of Chemical Engineer CO2
Role of chemical engineer in various aspects such as research, process
development, process design & evaluation, plant design, construction (EPC firms),
process supervision, plant technical service, product sales, general aspects of
chemical engineering such as communication, human relations, professional
activities & technical reading. Environmental, safety and ethical aspects
associated with chemical engineering profession.
4. Flowsheet Drawing CO2
Symbols as per Indian Standards 3232, basics of PBD, PFD and P&ID, CO3
systematic analysis of chemical processes by flowsheet reading and drawing.
5. Useful Mathematical Methods CO4
Presentation of data as table and chart, basics of regression and correlation, linear
and polynomial curve fitting using graphical and numerical method, determining
goodness of fit (R2 calculation), graphical and numerical methods for
interpolation, integration and to find the root of an equation, graphical addition &
subtraction of mass (inverse lever arm rule) and calculation of mean values etc.
6. Physical and Chemical Principles CO5
Process variables like temperature, pressure, density, viscosity, composition and flow CO6
rate. Ideal and real gas calculations and associated laws like Dalton and Amagat.
Concept of vapor-liquid equilibria, laws like Raoult’s and Henry’s, dew and
bubble calculations.

C. TEXT BOOKS
1. Andersen, L. B.; Wenzel, L. A. Introduction to chemical engineering; McGraw Hill Book
Company, New York, 1961.

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 24


D. REFERENCE BOOKS
1. Ghosal, S. K.; Sanyal S. K.; Datta, S. Introduction to Chemical Engineering; McGraw
Hill Education, 1st Ed, 2007
2. Himmelblau, D. M.; Riggs, J. B. Basic Principles and Calculations in Chemical
Engineering; PHI Learning PVt Ltd, 7th Ed, 2013

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand the concepts of various unit operation, their mode of
CO1
operation and applications.
Define chemical process industries, the roles of chemical
CO2 Conceptual engineers and their ethical practices.
Evaluation
Systematically analyze the process flow diagrams and piping &
CO3 Designing
instrumentation diagrams of industry.
Analytical
Estimation of various physico-chemical properties using
CO4 Application
appropriate mathematical approaches.
Problem solving
Application of computational tools (excel/c programming) to solve
CO5
problems pertaining to process industries.
CO6 Evaluation of problems relevant to ideal and real gases.

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 2 3 3 2 3 2.7
PO2 3 2 3 2 2 3 2.5
PO3 2 3 2 3 3 3 2.7
PO4 2 2 3 3 3 2 2.5
PO5 2 2 3 2 3 3 2.5
PO6 2 3 2 3 2 3 2.5
PO7 3 3 2 2 2 3 2.5
PO8 3 3 2 3 2 2 2.5
PO9 2 3 2 2 3 3 2.5
PO10 2 3 3 2 3 2 2.5
PO11 2 3 3 2 3 2 2.5
PO12 3 3 3 2 3 3 2.8
PSO1 2 3 3 3 3 3 2.8
PSO2 2 3 3 3 3 3 2.8
PSO3 3 2 3 3 3 3 28
PSO4 3 2 3 3 3 3 2.8

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 25


B. TECH. – SEMESTER-III (CH)
CHEMISTRY-II (BSC107)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 3 6 4.5 60 40 25 25 150

A. COURSE OVERVIEW
The course of Organic chemistry will enable students in the fields of Purification Methods &
Detection of elements, Polymers, Dyes and Pigments which all are basics of Chemistry in
Academia and as well as in Chemical industries. The course of physical chemistry is introducing
the students to the fundamentals of adsorption, colloidal surfactant and catalysis. The course
aims to provide basic knowledge of surface and colloid chemistry from a physical-chemical
perspective. This course will also Introduces the student to principles and theory of important
instrument analysis techniques.

B. COURSE CONTENT
TOPICS COs
1. Chemistry of Surfaces and Catalysis CO2
Adsorption, Langmuir adsorption isotherm, reactions at surfaces, colloidal
surfactants-classification anionic, cationic and non-inorganic surfactants, micelles,
structure, applications of colloidal surfactants, Catalysis, Homogeneous Lewis acid
base catalysts, organometallic catalysts and industrially examples. Heterogeneous
catalysts basic concepts and industrial examples.
2. Electrochemistry CO2
Theory, Principle and Application of the Electrolytic Dissociation. Osmotic Properties
of Electrolytes, Thermochemical effect & Chemical Equilibrium in Electrolytic
solution, Electrolytic Dissociation of Water, Buffer Capacity of Solution. Ionic
Activity and Activity co-efficient, Dissociation constant and pH in terms of Activity,
Ionic Strength, Ghosh’s Theory of electrolytes, Debye Huckel Theory of electrolytes,
Debye-Huckel Limiting Law, Theoretical Interpretation of the Electrical conductance
of electrolyte, Debye Onsager Theory of Conductance, Wine Effect and Debye
Falkenhagen effect.
3. Analytical Chemistry CO5
Theory, Instrumentation and applications of pH Metry, Potentiometry,
Conductometry, Polarography, Atomic absorption spectroscopy. Basics of
Chromatography, Thermal Gravimetric Analysis, Differential Scanning Calorimetry
and Calorimetry.
4. Purification, Detection & Estimation of Elements of Organic Compounds CO4
Organic Compounds are purified by Purification Methods (Crystallization
Sublimation & Different types of Distillation), Detection of elements (C, H, N, S, P
& halogens), Estimation of elements (C, H, S, P & halogens), Combustion estimation
of Nitrogen by Dumas method & Kjeldahl’s method, Combustion estimation of S, P
& halogens by Carius method.
5. Aromatic Compounds and Heterocyclic Compounds CO1
General nature of Aromatic reaction with their mechanism (Electrophilic Substitution
Reactions), Halogenation, Sulphonation, Nitration, Friedel Craft Alkylation, Friedel
Craft Acylation, Hydrogenation and reductive alkylation. Preparation, chemical
properties and uses of Furan, Furfural, Thiophene, Pyrrole, Pyridine.

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 26


6. Bio-Molecules CO3
Preparation, Constitution, Chemical reactions and uses of Glucose, Fructose,
Sucrose, Starch & Cellulose. Some typical conversions in Monosaccharide and
Disaccharides Isolation of proteins, General and physical characteristics of Proteins,
Analytical tests of Proteins.
7. Polymers CO3
Types of Polymerization reactions, Thermoplastic & Thermosetting plastics
Plasticizers, Classification of resins & plastics (polyethylene, polypropylene,
polyester and nylon, etc.) Synthetic & natural rubbers –Polychloroprene, Buna-S and
Buna-N.
8. Colour & Dyes CO3
Constitution & colour of Dyes & Dyeing process, Chromophore –Auxochrome
theory & Chromogen, Valence bond theory of colour Classification of dyes: Direct
dies, Mordant dyes, Vat dyes, Classification based on chemical structure: - Nitro&
Nitroso dyes, Triphenyl dyes

C. TEXT BOOKS
1. Mahan, Bruce H., University Chemistry 4th ed, Pearson Education India: Singapore, 2009
2. Soni, P. L.; Katyal, M., Textbook of Inorganic Chemistry; 20th ed.; Sultan Chand &
Sons: New Delhi, 2017
3. Antropov, L., Theoretical Electrochemistry; 2nd ed.; Mir Publishers: Moscow, 1977
4. Skoog, Douglas A, Holler, F. James, and Crouch, Stanley R. Principles of
Instrumental Analysis; 7th ed.; Cengage Learning India Pvt. Ltd: India, 2020
5. Bahl, A.; Bahl, B.S.; Tuli, G. D. A Textbook of Organic Chemistry; S.Chand New
Delhi, 2012

D. REFERENCE BOOKS
1. Carey, Francis A., Sundberg, Richard A., Advance Organic Chemistry; 5th
ed.; Charlottesville: Virginia, 2007
2. Morrison R.T.; Boyd R.N.; Bhattacharya S.K. Organic Chemistry; 7th ed; Pearson: New
York, 2011
3. Finar, I. L. Stereo Chemistry and the Chemistry of Natural Products (Volume -II); 5th ed;
Pearson: London, 2002
4. Finar, I. L. Organic Chemistry (Volume -I); 6th ed; Pearson: London, 2002
5. Hiemenz, P. C., and Rajagopalan, R., Principle of colloid and surface chemistry, 3rd
ed.; CRC Press, 2016
6. M. J. Rosen, Surfactants and Interfacial Phenomena, Wiley Publication, 2004

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Examine the various classes of Aromatic and Heterocyclic
CO1
Evaluate compounds, as well as their chemical properties and applications.
Comprehension Understand the fundamentals of Electrochemistry and Surface
CO2
Science.
Developing solutions for problems associated with synthetic
CO3 Application organic chemistry, dyes, soaps, detergents, Biomolecules and
polymers.
Students will learn to synthesize the chemical compounds by
CO4 Synthesis maneuvering the addition of reagents under optimum reaction
conditions.

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 27


Learn how to use various chromatographic techniques to separate
CO5 Analysis and identify chemicals. Gain hands on experience of the thermal
analysis technique, including its principles and instrumentation.

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 AVG.
PO1 2 3 2 1 2 2
PO2 2 1 2 2 1 1.6
PO3 1 3 1 2 1 1.6
PO4 2 1 1 3 2 1.8
PO5 2 3 2 1 1 1.8
PO6 2 2 1 2 1 1.6
PO7 1 2 2 1 2 1.6
PO8 2 1 2 1 1 1.4
PO9 1 2 1 2 1 1.4
PO10 2 1 2 1 2 1.6
PO11 2 1 2 1 1 1.4
PO12 1 2 1 2 2 1.6
PSO1 2 1 3 1 2 1.8
PSO2 1 2 1 2 2 1.6
PSO3 2 1 2 1 2 1.6
PSO4 1 2 2 3 1 1.8

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 28


B. TECH. – SEMESTER-III (CH)
GENERAL CHEMICAL TECHNOLOGY (PCC113)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 2 5 4 60 40 25 25 150

A. COURSE OVERVIEW
Motivation: To inculcate the knowledge of various processes and operations of the chemical
industries, among the undergraduate students of chemical engineering.
Objective:
• To study chemical manufacturing processes and their applications to specific chemical
Industries.
• Main focus is on the raw materials, flow sheet, synthesis and detailed analysis of the
processes.
• Enables the readers to integrate the fundamental knowledge of the basic disciplines & all
other courses you have read or reading
• To understand the most important chemical processes, and to apply this knowledge and
understanding to industrial processes.
• To familiarize the students with characteristics of Crude, its refining to get
commercially important fractions and products.
• To help the students in understanding the unit operations and unit processes in
manufacture of various petrochemicals and their downstream products like polymers, dyes,
synthetic fibers and pharmaceuticals.
• To familiarize with environmental issues and engineering problems involved.

B. COURSE CONTENT
TOPICS COs
1. Water and Water Treatment CO1
Industrial use of water, demineralization, deionization, RO system, water treatment, CO2
concept of water resources management.
2. Fuels & Energy CO1
Classification of fuels, Water gas, Producer Gas, Coke oven gas., Coal & coal chemicals, CO3
coking of coal, Various types of coal gasifiers.
3. Cement & Glass Manufacturing CO1
Lime stone beneficiation, types of cement, Manufacturing of cement. Types of glass, CO4
manufacturing of glass.
4. Sulphur and Electrolytic Manufacturing of Aluminum & Magnesium CO1
Manufacturing of elemental sulfur by Frasch process. Hydrogen sulfide conversion and CO3
from iron pyrites, CO4
5. Pulp & Paper Manufacturing CO1
Kraft process and sulfite process for manufacturing of pulp, chemical recovery system, CO3
types of paper, paper manufacturing process. CO4
6. Sugar & Starch Industry CO1
Manufacturing of sugar, starch, and dextrin CO3
CO4
CO5
7. Oils, Fats, Soaps & Detergents CO1
Vegetable oil Extraction method using Mechanical and Solvent extraction process. CO3
Hydrogenation of oil, cleaning mechanism of soaps and detergents, manufacturing CO4

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 29


of soaps and glycerine, manufacturing of detergents CO5
8. Overview of Petroleum and Petrochemical Industry Petroleum Refining CO4
Origin, formation and composition of petroleum, Petroleum reservoirs in India and World, CO6
Evaluation of petroleum, thermal properties of petroleum fractions, Important products- CO4
properties and test methods, Dehydration and desalting of crudes, Distillation of CO6
petroleum, Fractions-impurities, Gasoline Treatment, Treatment of Kerosene, Treatment
of Lubes, Wax and purification, Thermal and Catalytic cracking, Catalytic reforming,
Naphtha cracking, Coking, Hydrogen processes, Alkylation.
Petrochemical Industry: Overview of petrochemicals from petroleum feedstock.
9. Introduction to Polymers and Synthetic Fiber Industries CO1
Manufacture of phenol & urea formaldehyde resins, manufacture of PVC, polyethylene, CO3
CO4
etc, Manufacture of synthetic fibers (e.g. Industries nylon, polyester, acrylic, rayon etc)
CO6
10. Fine Chemicals, Drugs, Intermediates and Dyes CO1
Classification of pharmaceuticals, manufacture of important drugs and pharmaceuticals – CO3
salicylic acid, methyl salicylate, aspirin, antibiotics, & vitamins. CO4
CO6

C. PRACTICAL AND TERM WORK


• To determine Flash and Fire point of given sample using Able's apparatus.
• To determine Flash and Fire point of given sample using Pensky Martin apparatus.
• To determine Aniline point of given oil sample.
• To determine Smoke point of Kerosene sample.
• To determine viscosity of given oil sample.
• To determine Cloud and Pour point of given oil sample.
• To determine Softening Point of given sample.
• To do proximate analysis of coal.
• ASTM distillation Test.
• Carbon Residue Test.
• Synthesis of Soap
From the above list, selected experiments may be performed by students for better understanding
of theoretical concept.

D. TEXT BOOKS
1. Dryden’s Outlines of Chemical Technology, 2nd Ed. By M. Gopala Rao & Marshall
Sitting, East West Press Pvt. Ltd., New Delhi
2. Shreve’s Chemical Process Industries, 5th Ed. By, George F. Austin McGraw Hill
International Edition
3. George F. Austin, Shreve’s Chemical Process Industries, 5th Ed. McGraw Hill
International Edition, NY, 1984
4. Bhaskara Rao, B.K., Modern Petroleum Refining Processes, 6th Ed. Oxford & Ibh,
New Delhi, 2017
5. Bhaskara Rao, B.K., A Text On Petro Chemicals, 5th Ed, Khanna Publisher, New
Delhi, 2010

E. REFERENCE BOOKS
1. Chemical Process Industries, 4th Ed. by R. Norris Shreve & J. A. Brink, Jr. International
Student’s Edition
2. Pollution Control in Chemical Process Industries, 1st Ed. By S. P. Mahajan Tata McGraw
Hill Publications, New Delhi

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 30


F. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand the fundamentals of general chemical process technologies
CO1
and the importance of these technologies
Understand Develop an ability to identify and quantify, various process conditions
CO2
Develop associated with chemical processes and operations.
CO3 Explain Explaining the production processes of various chemical products.
Analyse Analyse the major engineering problems associated with production
CO4
Application units of various chemical industries.
CO5 Awareness and Application of the process drawing tools for process flow diagrams.
sustainability Create awareness among students for the research and innovation in the
CO6 field of chemical process industries for environmental issues and
sustainability.

G. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 2 3 3 3 3 2.8
PO2 3 2 3 3 3 3 2.8
PO3 2 2 3 3 3 3 2.7
PO4 3 2 2 3 2 3 2.5
PO5 3 3 3 2 2 2 2.5
PO6 3 3 3 3 2 3 2.8
PO7 3 2 3 3 2 3 2.7
PO8 3 2 3 3 2 3 2.7
PO9 3 3 3 3 2 2 2.7
PO10 3 2 3 3 3 2 2.7
PO11 3 2 2 3 3 3 2.7
PO12 3 3 3 3 2 2 2.7
PSO1 2 3 3 3 2 2 2.5
PSO2 2 3 3 3 2 2 2.5
PSO3 2 3 3 3 2 2 2.5
PSO4 2 3 3 3 2 2 2.5

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 31


B. TECH. – SEMESTER-III (CH)
MATERIAL AND ENERGY BALANCES (PCC101)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 1 0 4 4 60 40 0 0 100

A. COURSE OVERVIEW
The basics of units, dimensions, dimensional analysis, and engineering calculations related to
unit operations and unit processes. Analysis of chemical processes in steady-state and unsteady-
state domain along with mass and energy balance involving scenario of recycle bypass and purge.

B. COURSE CONTENT
TOPICS COs
1. Units, Dimensions and Dimensional Analysis CO1
System of units, fundamental & derived units, dimensional consistency, dimensional CO2
equations & empirical equations, different ways of expressing units of quantities and
physical constants. Conversion of empirical formula from one-unit system to another.
Dimensional analysis using Rayleigh and Buckingham method.
2. Basic Chemical Calculations CO1
Composition of gaseous mixtures, liquid mixtures and solutions. Determination of CO2
hardness, elements present in compound, acidity-alkalinity and concentration based
numerical. Behavior of real gas and determination of Van-der- Waals constants, and
saturation pressure based numerical.
3. Material Balance without Chemical Reaction CO3
Schematic representation of process, selection of key component and degree of freedom CO4
analysis. Material balance over unit operations like distillation, mixing unit, evaporator, CO5
absorber, stripper, extractors, crystallizers, dryer, humidifier and dehumidifier. Complex
mass balance involving recycle, bypass and purge stream. In
addition, mass balance in unsteady state domain over simple unit operation.
4. Material Balance with Chemical Reaction CO3
Concept of limiting & excess reactants, conversion, yield and selectivity, material balance CO4
involving reactions with special reference to fertilizers, chlor-alkali, petrochemicals, CO5
pharma and dyestuff industry.
5. Energy Balance CO3
Heat capacity of gas and gaseous mixtures, heat capacity of liquids and solids, sensible CO4
heat change in liquids and gases, enthalpy changes during phase change transformation, CO5
enthalpy changes accompanied by chemical reactions, thermo chemistry of mixing
process, dissolution of liquids and solids, energy balance at plant elevated conditions and
adiabatic temperature rise calculations.
6. Mass and Energy Balance over Flowsheet CO6
Mass and energy balance over connected equipment and complete mass and energy
balance over at least one process flow sheet from Dryden. Ethics and decision making
while performing mass and energy balance over flowsheet.
7. Fuels & Combustion CO1
Types of fuels, proximate and ultimate analysis of fuel, calorific value of fuels as gross CO2
and net, problems on combustion of coal, liquid fuels, gaseous fuels, sulphur and sulphur
pyrites.

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 32


C. TEXT BOOKS
1. Bhatt, B. I., Thakore, S. B.; Stoichiometry; 5th Ed.; Tata McGraw Hill Education Pvt.
Ltd., 2010.

D. REFERENCE BOOKS
1. Himmelblau, D. M., Riggs, J. B.; Basic Principles & Calculations in Chemical
Engineering; 7th Ed.; Prentice Hall India Learning Pvt. Ltd., 2013
2. Felder, R.M., Rousseau R.W.; Elementary Principles of Chemical Processes; 3rd Ed.;
John Wiley & Sons Inc., 2005
3. Watson, K.M., Hougen, O.A., Ragatz, R.A.; Chemical Process Principles Part-I
Material and Energy balances; 2nd Ed.; CBS Publishers & Distributors Pvt. Ltd., 2004

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand the basic principles and unit conversion-based
CO1
calculation techniques used in the chemical industries.
Define and develop analogy for chemical processes in steady-
CO2
state and unsteady-state domain.
Understand Apply the basics of mass and energy balances and their
CO3 Develop applications in chemical industries by using examples primarily
Apply based on chemical operations.
Discuss Discuss the possible ways of solving complex mass balance
CO4 Evaluate problems involving scenario of recycle, bypass and purge in
Analyse chemical industries.
Evaluate the energy consumption for both flow and non-flow
CO5
processes.
Analyse the complete mass and energy balance calculation for the
CO6
entire chemical process.

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 2 2 3 2.7
PO2 2 3 3 2 2 2 2.3
PO3 2 2 3 2 2 2 2.2
PO4 2 2 2.5 2 2 2 2.1
PO5 2 2 2 2.5 2 2 2.1
PO6 2 2.5 2 2 2 2 2.1
PO7 2 2 2 3 2 2 2.2
PO8 2 2 2 2 2 2.5 2.1
PO9 2 2 2.5 2 2 2 2.1
PO10 2 2.5 2 2 2 2 2.1
PO11 2 2 2 3 2 2 2.2
PO12 3 2 3 2 2 3 2.5
PSO1 2.5 2 2.5 2.5 2 2.5 2.3
PSO2 2.5 2.5 2 2.5 2.5 2.5 2.4
PSO3 2.5 2.5 2.5 2 2 2.5 2.3
PSO4 2.5 2 2.5 2 2.5 2.5 2.3

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 33


B. TECH. – SEMESTER-III (CH)
PHYSICS (BS102)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
2 0 2 4 3 40 0 25 25 90

A. COURSE OVERVIEW
To make a bridge between the physics in school and engineering courses.
Objective
To create general understanding regarding basic physical principles and orient themselves in
implementation involved in living systems. To familiarize the student with basic concepts in
physics as: classical optics used in microscopes. To familiarize students with concepts in digital
electronics, lasers, sound waves, electricity. To introduce them to concepts in modern physics
such as: production of X-ray, X-ray crystallography, quantum mechanics etc.

B. COURSE CONTENT
TOPICS COs
1. Optics CO1
• Interference: Introduction to optics, Principles of superposition, CO2
Constructive & Destructive Interference, Types of Interference, Conditions
for observing interference, interference due to thin films, wedge shaped films,
Newton’s rings, applications of interference
• Diffraction: Concept of diffraction, Types of diffraction (Fraunhofer and
Fresnel diffraction), difference between interference and diffraction,
Fraunhofer diffraction at single slit, double slit, and multiple slits; Diffraction
grating and its applications.
• Polarisation: Introduction, polarisation by reflection, polarisation by double
refraction, scattering of light, circular and elliptical polarisation, optical
activity, Polarization of light waves, Polaroid, Optical activity.
• Optical Microscopy: Basic principles and components, Different
examination modes, Stereomicroscopy, Photo-microscopy, Color
metallography, Specimen preparation, Applications.
2. Laser and Fibre Optics CO1
• Lasers: Introduction to interaction of radiation with matter, principles and CO3
working of laser, Characteristics of laser, Properties of lasers, laser types:
solid state Laser, Ruby laser, He-Ne laser, semiconductor laser, applications
of laser, Industrial applications, and Medical applications.
• Fibre Optics: Introduction, Principle and propagation of light in optical
fibres, Fermat’s principle and Snell’s law, structure of optical fibres,
numerical aperture, acceptance angle, types of optical fibres (material,
refractive index, mode), losses in fibres, optical fibre communication system,
fibre optic sensors (displacement and pressure sensors). Fabrication: Double
Crucible Technique, Vapour phase Oxidation Process, applications of optical
fibres.
3. Electromagnetism and Magnetic Properties of Materials CO1
• Electrostatics & Electrodynamics: Introduction to electrostatics, Coulomb’s CO4
law for distribution of charges, polarization and Gauss’s law electric current
and equation of continuity, magnetic induction, Electrostatic filed in matter:
dielectric polarization, polarizability and susceptibility, types of polarization,

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 34


and Claussius-Mosotti equation.
• Magnetostatics & Magnetism: Introduction to magnetostatics, Lorentz force,
Steady current and equation of continuity, Biot Savart Law-Ampere’s law,
magnetization and magnetic intensity, Magnetostatic field in matter: torques
and forces on magnetic dipoles, Magnetization: Faraday’s laws of
electromagnetic induction, Electromagnetic waves: wave equation,
Electromagnetic energy density, Poynting theorem, Maxwell’s equations,
Physical significance of Maxwell’s equations, propagation of EM waves in
free space, Lenz’s law, Displacement current
4. Quantum Mechanics CO5
• Introduction to Quantum Mechanics: Plank’s Quantum Theory, Properties of
Photon, Photoelectric effect, Inadequacy of classical mechanics (black body
radiation, photoelectric effect)
• Classical mechanics and its limitations, Planck’s radiation law, Wien’s law,
and Rayleigh Jean’s law, wave and particle duality of radiation, de Broglie
concept of matter waves, Davisson-Germer experiment, Heisenberg’s
uncertainty principle, Consequences of uncertainty principle
• Equation of motion of matter waves, Schrodinger time independent wave
equation
• Physical significance and properties of wave function, interpretation of wave
function, eigenvalues and Eigen functions, superposition principle, Particle
in one dimensional box and extension to three dimensions, Tunnelling effect
(qualitative) and Applications.

C. TEXT BOOKS
1. Bhatt, B. I., Thakore, S. B.; Stoichiometry; 5th Ed.; Tata McGraw Hill Education Pvt.
Ltd., 2010.

D. REFERENCE BOOKS
1. Himmelblau, D. M., Riggs, J. B.; Basic Principles & Calculations in Chemical
Engineering; 7th Ed.; Prentice Hall India Learning Pvt. Ltd., 2013
2. Felder, R.M., Rousseau R.W.; Elementary Principles of Chemical Processes; 3rd Ed.;
John Wiley & Sons Inc., 2005
3. Watson, K.M., Hougen, O.A., Ragatz, R.A.; Chemical Process Principles Part-I
Material and Energy balances; 2nd Ed.; CBS Publishers & Distributors Pvt. Ltd., 2004

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Able to understand the general scientific concepts of optics,
CO1
electromagnetism, microscopy, advance materials, and modern physics.
Students understand the concept of interference, diffraction which are
CO2 Understand very basic in the field of wave optics.
Develop
An ability to understand the basic concepts of optical fibers & their
CO3 Apply
properties and the Laser fundamentals.
Discuss
CO4 An ability to identify, formulate, and solve Electromagnetic problems.
Evaluate
Analyse Understand the importance of Nanomaterials along with their
CO5
Engineering applications and their Synthesis and analysis.
To become familiar with modern physics like black body radiation,
CO6
quantum mechanics and statistical physics.

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 35


F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 1 3 3 2 3 3 2.5
PO2 1 3 3 2 3 3 2.5
PO3 1 3 3 2 3 3 2.5
PO4 1 3 3 2 3 3 2.5
PO5 1 3 3 2 3 3 2.5
PO6 1 3 3 2 3 3 2.5
PO7 1 3 3 2 3 3 2.5
PO8 1 3 3 2 1 2 2
PO9 1 2 3 2 1 2 1.8
PO10 1 2 3 2 1 2 1.8
PO11 1 2 3 2 1 2 1.8
PO12 1 2 3 2 1 2 1.8
PSO1 1 2 2 2 1 1 1.5
PSO2 3 3 3 3 3 3 3
PSO3 3 3 3 3 3 3 3
PSO4 1 1 1 2 2 2 1.5

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 36


B. TECH. – SEMESTER-III (CH)
ENGLISH (HSM201)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
2 0 2 4 3 40 0 50* 0 90
*Marks include Viva based on TW

A. COURSE OVERVIEW
This course will help students of engineering develop their Linguistic skills. Beginning with
Vocabulary Building the course proceeds towards the Sentence Formation and Paragraph
Formation which will help them to enhance their Writing skills and Communicative skills as
well. Understanding the common errors, and nature and style of writing will mould students’'
Writing competency for their professional growth in the world of competition. Understanding
Paralinguistic features like stress, intonation, rhythm and so on will improve their Speaking
skills to be efficient and confident for academic and professional purposes.

B. COURSE CONTENT
TOPICS COs
1. Vocabulary Building CO1
The concept of Word Formation, Root words from foreign languages and their use in
English, Acquaintance with prefixes and suffixes from foreign languages in
English to form derivatives, Synonyms, antonyms, and standard abbreviations.
2. Basic Writing Skills CO1
Sentence Structures, use of phrases and clauses in sentences, Importance of proper CO2
punctuation, creating coherence, organizing principles of paragraphs in documents,
Techniques for writing precisely
3. Identifying Common Errors in Writing CO2
Subject-verb agreement, Noun-pronoun agreement, Misplaced modifiers, CO3
Articles, Prepositions, Redundancies, Clichés
4. Nature and Style of Sensible Writing CO3
Describing, Defining, Classifying, providing examples or evidence, Writing CO4
introduction and conclusion
5. Writing Practices CO4
Comprehension, Précis Writing, Essay Writing
6. Oral Communication CO5
(This unit involves interactive practice sessions in Language Lab) Listening CO6
Comprehension, Pronunciation, Intonation, Stress and Rhythm, Common,
Everyday Situations: Conversations and Dialogues, Communication at Workplace,
Interviews, Formal Presentations

C. TEXT / REFERNCE BOOKS


1. Practical English Usage. Michael Swan. OUP. 1995
2. Remedial English Grammar. F.T. Wood. Macmillan.2007
3. On Writing Well. William Zinsser. Harper Resource Book. 2001
4. Study Writing. Liz Hamp-Lyons and Ben Heasly. Cambridge University Press. 2006
5. Communication Skills. Sanjay Kumar and Pushp Lata. Oxford University Press. 2011
6. Exercises in Spoken English. Parts. I-III. CIEFL, Hyderabad. Oxford University Press

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 37


D. COURSE OUTCOMES
COs SKILLS STATEMENT
Reading and Understand the vocabulary and their root forms to enhance
CO1
Writing vocabulary level
CO2 Errorless Writing Enhance their Writing in effective way
Reading, Writing, Rectify common errors in their Speaking and Writing
CO3 and Speaking
Proficiently
Focused and Develop efficiency in writing
CO4 Organised
Writing
Speaking and Be competent at Public Speaking and Interviews
CO5
Listening
Specific Soft Acquire Proficiency in all four skills of Language
CO6
Skills

E. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1
PO2 1 1 1 1 1
PO3
PO4 1 1 1 1
PO5
PO6
PO7
PO8
PO9 1 1 1 1
PO10 3 3 3 3 3 3 3
PO11 1 1 1 1 1 1 1
PO12 1 1 1 1 1 1 1
PSO1 1 2 2 2 2 2 1.8
PSO2 1 2 2 2 2 2 1.8
PSO3 2 2 3 3 3 3 2.7
PSO4 1 2 2 2 2 3 2

BACK

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 38


SEMESTER-IV
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
PCC104 Heat Transfer 3 0 3 60 40 25 25 150 4.5
PCC105 Mass Transfer - I 3 1 0 60 40 0 0 100 4
PCC106 Fluid Mechanics 3 0 3 60 40 25 25 150 4.5
Particles and Fluid
PCC111 3 0 3 60 40 25 25 150 4.5
Particle Processing
PCC103 Thermodynamics -II 3 1 0 60 40 0 0 100 4
Effective Technical
HSMC201 3 0 0 40 0 0 0 40 3
Communication
TOTAL 18 2 9 340 200 75 75 690 24.5

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 39


B. TECH. – SEMESTER-IV (CH)
HEAT TRANSFER (PCC104)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 3 6 4.5 60 40 25 25 150

A. COURSE OVERVIEW
The course will introduce the fundamental concepts of various modes of heat transfer. It will
further elaborate these concepts with theories and applications to the solutions of practically
relevant chemical engineering problems. Some aspects of process design principles of various
heat transfer equipment will be taken up in the later part of this course.

B. COURSE CONTENT
TOPICS COs
1. Modes of heat transfer: Conduction, Convection, and Radiation. Material CO1
properties of importance in heat transfer: Thermal conductivity, Specific heat
capacity. Classification of heat transfer equipment’s and processes
2. Steady state conduction in one dimension. Basic law of heat conduction- Fourier’s CO2
law, Steady state heat conduction through composite wall, Steady state heat
conduction through a variable area: cylinder, sphere. Heat conduction in bodies
with heat source: plane wall, cylinder, sphere.
3. Newton’s law of cooling. Dimensionless numbers and their physical significance, CO2
empirical correlations for free and forced convection. Thermal and hydrodynamic CO1
boundary layer, heat and momentum analogy.
4. Definition, phenomena of boiling, boiling curve, regimes of boiling. Heat transfer CO3
to boiling liquids, the mechanism of nucleate boiling, correlation for pool boiling CO4
heat transfer: Nucleate boiling, critical heat flux, stable film boiling. Force
convection boiling.
5. Definition, phenomena of condensation, film type & drop wise condensation. Film CO2
condensation on vertical surface, condensation on horizontal tube or tube bank. CO6
6. Definition, basic principles, properties of solution. Performance of steam heated CO4
tubular evaporators: Capacity and economy, single and multiple effect CO6
evaporators, Boiling point elevation, heat transfer coefficient, enthalpy balance
calculation. Method of feeding: forward & backward feed systems, Types of
evaporators: natural circulation evaporator, forced circulation evaporator.
7. Classification, heat exchanger analysis, LMTD for parallel and counter flow CO4
exchanger. Condenser and evaporator, overall heat transfer coefficient, fouling CO5
factor, correction factors for Multipass heat exchanger. CO6
Effectiveness and number of transfer unit for parallel and counter flow heat
exchanger. Design of Double pipe heat exchanger and shell and tube heat
exchanger (kern’s method of heat Exchanger design, Bell Delaware method).
Introduction to compact heat exchanger and their design aspects. Importance of
Ethics in design of
heat exchanger and its importance in process industry.
8. Basic definition radiation: Absorptivity, reflectivity, and transmissivity. CO1
Blackbody radiation, laws of radiation: Planck’s law, Wien’s law, The Stefan- CO2
Boltzmann law for blackbody, Special characteristic of blackbody radiation,
Kirchhoff’s law, radiation between surfaces.

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 40


9. Types of fins, heat flow through rectangular fin, infinitely long fin, fin insulated CO2
at the tip and fin losing heat at the tip, efficiency and effectiveness of fin.

C. TEXT BOOKS
1. Kern, D. Q., Process Heat Transfer, McGraw Hill, 1997
2. Dutta, B. K., Heat Transfer – Principles and Applications, PHI, 2004

D. REFERENCE BOOKS
1. Holman, J. P., Heat Transfer, 9 ed., McGraw Hill, 2008
2. Sinnott, R. K., Coulson & Richardson’s Chemical Engineering Design, Vol. 6,
Elsevier Butterworth Heinemann,1996
3. Incropera Frank P., Dewitt David P., Bergman T. L., Lavine A. S., Seetharaman
K.N., Seetharaman T. R., Fundamentals of Heat and Mass Transfer, Wiley, 2014

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand and analyse basic knowledge of heat transfer with the
CO1
help of science and engineering fundamentals
CO2 Design and solve conduction, convection and radiation problems.
Understand Build a bridge between theoretical and practical concept used in
CO3
Design Apply industry.
Analysis Utilize heat transfer knowledge to design and analyse the
CO4
Evaluates performance of heat exchangers and evaporators.
Develop Use the techniques, skills, and modern engineering tools
CO5
necessary for engineering practice.
Analyse and calculate heat transfer in complex systems
CO6
involving several heat transfer mechanisms.

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 2 2 2 3 3 3 2.5
PO2 2 3 2 2 3 2 2.3
PO3 1 2 2 3 2 3 2.2
PO4 2 2 2 3 2 3 2.3
PO5 1 2 3 3 3 3 2.5
PO6 2 1 3 2 3 2 2.2
PO7 2 3 3 3 3 3 2.8
PO8 2 1 3 2 3 1 2
PO9 1 2 2 3 2 3 2.2
PO10 1 2 2 2 3 2 2
PO11 2 1 2 3 3 3 2.3
PO12 3 3 3 3 3 2 2.8
PSO1 3 2 2 3 2 3 2.5
PSO2 3 3 2 3 3 3 2.8
PSO3 2 3 3 2 3 2 2.5
PSO4 3 3 3 2 3 3 2.8

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 41


B. TECH. – SEMESTER-IV (CH)
MASS TRANSFER-I (PCC105)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 1 0 4 4 60 40 0 0 100

A. COURSE OVERVIEW
This course will provide an overview of mass transfer operation at basic to an intermediate level.
Objective: The purpose of this course is to introduce basic concepts of mass transfer and attain
ability to identify, formulate, and solve mass transfer problems. To introduce basic concepts of
mass transfer equipment and apply them for designing purpose. The goal is to provide students
with the theoretical/analytical background to understand mass transfer operations as well as
application and to tackle the sort of complex problems.

B. COURSE CONTENT
TOPICS COs
1. Introduction to Mass Transfer Operations (MTO): Classification, methods of CO1
conducting MTO
2. Molecular Diffusion in Fluids: Steady state molecular diffusion in fluids (both CO1
liquids & gases). Diffusivity of liquids & gases. CO2
3. Mass Transfer Coefficients: MT coefficients in laminar flow & turbulent flow. CO1
Theories of MT, heat, mass & momentum transfer in laminar & turbulent flow & CO3
their analogies. Simultaneous heat & mass transfer. Effect of chemical reaction on
mass transfer.
4. Diffusion in Solids: Fick’s law. Unsteady state diffusion. Types of solid diffusion CO1
CO2
5. Inter Phase Mass Transfer: Equilibrium, diffusion between phases. Local & CO1
overall diffusion. Various processes & material balance for each of them CO3
6. Equipment for Gas – Liquid Operations: Gas dispersion. Liquid dispersion CO4
equipment
7. Distillation: VLE data, flash distillation, simple distillation and continuous CO5
rectification. McCabe Thiele & Ponchon Savarit methods. Distillation in packed CO6
columns & vacuum distillation. Azeotropic distillation. Use of steam. Introduction
to multicomponent distillation. Moral issues and ethics

C. TEXT BOOKS
1. Treybal, R.E. Mass Transfer Operations,3rd Ed.; Tata McGraw Hill: New Delhi, 2012
2. McCabe, W.L.; Smith. J.C.; Harriot, P. Unit Operations in Chemical Engineering, 4th
Ed.; McGraw Hill Publications: NY, 1985

D. REFERENCE BOOKS
1. Dutta, B. K. Principles of Mass Transfer and Separation Processes, 2nd ed.; Prentice Hall
of India: New Delhi, 2007
2. Foust, S. Principles of Unit Operations, 2nd Ed.; Wiley: New York, 1980

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 42


E. COURSE OUTCOMES
COs SKILLS STATEMENT
Explain the basic mechanism of mass transfer including
CO1
diffusion and convective mass transfer
Estimation of steady state molecular diffusion in fluids (both
CO2
liquids and gases)
Explain Find the mass transfer coefficient and evaluate the problems
CO3
Analysis related to interphase mass transfer
Evaluates Identify the equipment for different gas-liquid operations and solve
CO4
Application related problems
Generate VLE data and estimate the problems related to design
CO5
calculation of distillation and absorption column
Develop analytical skill of the students that helps in to solve the
CO6
problems associated with real situation

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 3 3 3 3
PO2 3 3 3 2 3 2 2.7
PO3 3 3 3 2 3 2 2.7
PO4 3 3 3 2 2 2 2.5
PO5 2 2 3 2 3 2 2.3
PO6 2 2 2 2 2 3 2.2
PO7 3 2 2 3 3 2 2.5
PO8 3 2 2 2 3 3 2.5
PO9 3 3 3 2 3 3 2.8
PO10 2 3 3 3 3 3 2.8
PO11 3 3 3 3 3 2 2.8
PO12 3 3 3 3 3 3 3
PSO1 2 2 3 3 3 3 2.7
PSO2 2 2 3 3 3 3 2.7
PSO3 2 2 3 3 3 3 2.7
PSO4 2 2 3 3 3 3 2.7

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 43


B. TECH. – SEMESTER-IV (CH)
FLUID MECHANICS (PCC106)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 3 6 4.5 60 40 25 25 150

A. COURSE OVERVIEW
Fluids are an integral part of our day to day life. Fluid Mechanics occupies a privileged position
in the science. It is a field where multiple physical effects can be met and its knowledge is
necessary to understand the nature of flowing medium. The students will have creative thinking,
a deeper understanding and intuitive feel for fluid mechanics.

B. COURSE CONTENT
TOPICS COs
1. Introduction to Fluid mechanics, Definition of fluid, Types of fluids, Various Fluid CO1
Properties, Dimensional analysis in fluid flow phenomena, Simple numerical
examples related to fluid properties.
2. Fluid Statics CO2
Laws of fluid statics: Pascal’s law, Hydrostatic law, Barometric equation,
Hydrostatic equilibrium equation in a centrifugal field, Pressure and types of
pressure, Measurement of pressure using manometers and pressure gauges,
Selection criteria for pressure measuring devices, Simple numerical examples
related to hydrostatic law and pressure.
3. Fluid Kinematics CO2
Methods of describing fluid motion, Types of Flow- steady, unsteady, uniform,
non- uniform, laminar, turbulent, one, two and three dimensional, compressible,
incompressible, rotational, irrotational, Types of flow patterns - stream lines, path
lines, streak lines, Boundary layer concept.
4. Fluid Dynamics CO2
Concept of Control Volume, Laws affecting fluid motion, Conservation of mass,
linear momentum and energy, Basic equations derived using conservation
principles- Continuity equation in Cartesian coordinates, Momentum equations,
Bernoulli’s equation, Kinetic and momentum correction factor, Simple numerical
examples related to basic equations.
5. Fluid flow in pipes and ducts CO3
Introduction pipe and pipe fittings, Selection criteria for pipe, Concept of
equivalent length and pipe, pipes in series and parallel, Laminar flow through
circular pipe and between two parallel plates, Introduction to turbulent flow and
velocity distribution, Types of friction, Flow through non circular cross-section,
Energy losses through pipes, Minor losses in pipe lines, TEL, HGL, Moody
diagram. Simple numerical examples.
6. Flow around Immersed Bodies CO5
Concept of Drag and lift, Types of drag, Drag coefficient, Flow through bed of
solids, Fluidization- Conditions, Types and applications, Simple numerical
examples.
7. Fluid Flow Measurement CO4
Classification of flow-meter, Detailed study (Principle, construction and working)
of Venturi meter, orifice meter, Rotameter, Pitot-tube, Various types of notches,
Simple numerical examples.

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 44


8. Hydraulic pumps and Valves CO4
Classification of pumps, Detailed study (Principle, construction and working) of
Centrifugal pump, reciprocating pump, Characteristics curves for pump, Selection
of pumps, Classification of valve, Main parts of a valve, Various types of valves
like – Gate valve, Globe Valve, Ball Valve, Check valve

C. TEXT BOOKS
1. McCabe, W.L.; Smith. J.C.; Harriot, P. Unit Operations in Chemical Engineering, 7th
Ed.; Tata McGraw Hill Publications: NY, 2017
2. Dr R.K. Bansal, Fluid Mechanics and Hydraulic Machines; 9th ed.; Laxmi Publications,
New Delhi, 2010.

D. REFERENCE BOOKS
1. Dr. A. K. Jain, Fluid Mechanics including hydraulic machines; 12th ed., Khanna
Publishers, New Delhi, 2014.
2. K. A. Gavhane, Unit Operation -I, 12th ed., Nirali Prakashan, Pune, 2015
3. A.P. Kulkarni, Chemical Engineering Fluid Mechanics, 4th ed., Nirali Prakashan, Pune,
2019

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand the basic properties of fluids and classify their
CO1 behavior. Apply dimensional analysis to predict physical
parameters that influence the flow in process fluid mechanics.
Apply the concept of fluid statics and fluid kinematics in real life
Evaluate
engineering problems, create shell balance and ability to analyze
CO2 Comprehension
fluid flow problems in different configurations with the application
Application of continuity, momentum and energy equations.
Synthesis
Apply appropriate equations and principles to analyze pipe flow
CO3 Analysis
problems
Able to understand the functions and performances of various
CO4
equipments and flow measuring.
CO5 Analyse fluid behavior in fixed bed and fluidized bed system.

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6
PO1 2 3 3 3 2 2.6
PO2 1 3 3 3 2 2.4
PO3 1 2 2 2 1 1.6
PO4 1 2 2 2 2 1.8
PO5 2 2 2 1 2 1.8
PO6 1 2 2 2 2 1.8
PO7 1 2 2 2 2 1.8
PO8 2 2 2 2 2 2.4
PO9 2 2 2 2 2 2.4
PO10 2 2 2 2 2 2.4
PO11 3 2 2 3 2 2.4
PO12 3 3 3 3 2 2.8
PSO1 1 2 2 2 1 1.2
PSO2 1 2 2 2 1 1.6
PSO3 1 2 2 2 1 1.6
PSO4 1 2 2 2 1 1.6

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 45


B. TECH. – SEMESTER-IV (CH)
PARTICLES AND FLUID PARTICLE PROCESSING (PCC111)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 3 6 4.5 60 40 25 25 150

A. COURSE OVERVIEW
Motivation: Describe basic concept of Mechanical Operations and troubleshooting of Industrial
equipments for sustainable development of process industries.
Objectives: To develop basic concept of properties of particle and mixture along with its storage
and transportation. Students are able understand of various mechanical operations like
Screening, Size reduction & Enlargement, Filtration, Sedimentation, Agitation and Mixing used
in Chemical Process Industries. The students are exposed to fundamental theory, calculations,
and various types of equipment used in Chemical Process Industries related to Mechanical
Operations.

B. COURSE CONTENT
TOPICS COs
1. Solids CO1
• Introduction to solid particles CO2
• Characteristics of solid particles and Concept of Sphericity CO5
• Properties of mixture
• Introduction to nanoparticles properties & characterization
2. Size Reduction & Enlargement CO1
• Principle of comminution, Types of crushers, grinders & disintegrators for CO2
coarse and intermediate & fine grinding CO4
• Energy & power requirement for size reduction, laws of crushers & work
index, close & open circuit grinding, feed control, mill discharge and removal
& supply of heat in wet grinding
• Size enlargement– objectives, methods and equipment used in industries
3. Screening & Other Separation Methods CO2
• Screen Terminology and various screen series and Differential and CO3
cumulative method of screen analysis
• Types of Industrial screen, comparison of ideal & actual screens and capacity
& effectiveness of screens
• Principle of elutriation, floatation, jigging and electrostatic & magnetic
separation processes
4. Sedimentation CO2
• Concept of sedimentation, terminal settling velocity, batch settling test CO4
and free & hindered settling
• Flocculation, types of thickener & thickener area calculation, batch &
continuous settling chambers and sorting of classifiers
• Centrifugal settling process, cyclone and principle of centrifugal
sedimentation
5. Filtration CO2
• Types of filtration, requirements of filter media and filter aids CO3
• Principle of cake filtration, constant pressure filtration, batch & CO4
continuous filtration equipments – filter press, leaf filter, cartridge filter &
rotary drum filter

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 46


• Theories of filtration, washing of cake, principle of centrifugal filtration
and suspended basket centrifuge, etc.
6. Mixing & Agitation CO3
• Fundamentals of mixing & agitation, purpose of agitation and standard CO4
agitated vessel CO5
• Types of impellers, vortex formation in agitated vessel, power consumption
in agitated vessels, scale of agitated vessel and power consumption
• Characteristics of mixing equipment, mixing of pastes & paste masses, pony
mixers, beater mixer, mixing of dry powder, ribbon blender & tumbler mixer
etc
7. Storage and Conveying CO4
• Storage of solid, liquid and gases and types of storage vessels CO6
• Types of flow in solid discharge and various problems
• Types of Mechanical & pneumatic conveying system
8. Ethics CO1
Apply ethical principles and commit to professional ethics and responsibilities and CO5
norms of the engineering practice CO6

C. PRACTICAL AND TERM WORK


1. Experiments based on screening, screen efficiency, Size Reduction such as- Jaw crusher,
Roll crusher and Ball mill
2. Sedimentation, filtration, Agitated vessel and Terminal settling velocity etc

D. TEXT BOOKS
1. McCabe, L. W.;Smith, J.C.;Peter,H.Unit Operations of Chemical Engineering; 7th ed;
Tata Mc-Graw Hill Publication:New Delhi, 2017
2. Narayanan, C.M.;Bhattacharyya, B.C. Mechanical Operations for Chemical Engineers;
3rd ed; Khanna Publishers: New Delhi,2014

E. REFERENCE BOOKS
1. Harker, J.H.; Backhurst, J.R. Richardson, Coulson & Richardson’s Chemical
Engineering Volume 2; 5th ed; Butterworth-Heinemann: Oxford Woburn MA,2002
2. Badger, L.W.; Banchero, J. Introduction to Chemical Engineering; McGraw Hill:
Singapore,1984

F. COURSE OUTCOMES
COs SKILLS STATEMENT
Describe basic concept of Mechanical Operations used in chemical
CO1
process industries
CO2 Classify and Explain solid-solid, solid-fluid related operations
Understand
CO3 Identify methods for measuring performance of equipments
Analysing
Examine the factors affecting on solid handling related operations with
CO4 Synthesis
respects to the sustainable development of process industries
Evaluating
Applying Experiment related to various mechanical operations equipments during
CO5 Creating laboratory work including demonstration of advance instruments like
particle size analyser and XRD
Generating reports for selection, Design and troubleshooting of
CO6
Industrial equipments

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 47


G. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 3 3 3 3
PO2 3 3 3 3 2 3 2.8
PO3 3 3 3 2 3 2 2.7
PO4 3 3 3 2 2 2 2.5
PO5 2 1 2 2 3 2 2
PO6 2 2 2 3 3 3 2.5
PO7 2 2 3 3 3 3 2.7
PO8 3 2 2 2 3 3 2.5
PO9 2 2 2 2 3 3 2.3
PO10 2 2 2 3 3 3 2.5
PO11 3 3 2 3 3 3 2.8
PO12 3 3 3 3 3 3 3
PSO1 3 2 3 3 3 3 2.8
PSO2 2 3 3 3 2 3 2.7
PSO3 3 3 3 2 3 2 2.7
PSO4 2 2 3 3 3 3 2.7

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 48


B. TECH. – SEMESTER-IV (CH)
THERMODYNAMICS-II (PCC103)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 1 0 4 4 60 40 0 0 100

A. COURSE OVERVIEW
The subject aims to introduce the principles of Chemical Engineering Thermodynamics and
illustrate their applications in the design of equilibrium governed separation processes like
distillation, solvent extraction, etc. The course comprises the concept of chemical potential,
fugacity, activity & activity coefficient, vapour-liquid equilibrium (VLE), liquid-liquid
equilibrium (LLE) and reaction equilibrium. Introduction to molecular thermodynamics, the
laws of thermodynamics & their applications.

B. COURSE CONTENT
TOPICS COs
1. Systems of Variable Composition. Ideal behavior CO1
Review of first and second law of thermodynamics, concept of chemical potential, CO2
Concept of equilibrium, Chemical Potential as a Criterion of phase equilibrium,
Property changes for mixing of ideal gas mixtures and ideal solution, Raoult’s
law and its applications, Binary phase diagrams and problems.
2. Solution Thermodynamics CO2
Concept of partial properties, definition of fugacity and fugacity coefficient of
pure species and species in solution, Vapor Liquid Equilibrium (VLE), VLE by
modified Raoult’s law, VLE from K-value correlations, Flash Calculations,
Positive & negative deviations from Raoult’s law.
3. Phase Equilibria CO3
Phase rule, Duhem’s theorem, Gibb’s – Duhem equation, Definition of activity & CO4
activity coefficient, Lewis – Randall rule and Henry’s law, excess properties, CO5
Models for excess Gibbs energy (Activity models) such as Redlich-kister
equation, Wohl’s equation, Van Laar equation, Margule’s equation, Wilson
equation, NRTL, UNIQUAC & UNIFAC, Thermodynamic consistency test for
VLE data, Heat effects and property change of mixing processes, Liquid-Liquid
Equilibria; Vapor-Liquid- Liquid Equilibria; Solid-Liquid Equilibria; Solid-Gas
Equilibria, Ethics concern with VLE data.
4. Chemical Reaction Equilibria CO3
Equilibrium criterion for a chemical reaction, concept of Equilibrium conversion
(x), equilibrium constant (k), evaluation of equilibrium constants at different
temperatures, equilibrium conversion of single reactions and multi-reaction
equilibria, Phase rule for chemically reacting systems.
5. Introduction to Statistical Thermodynamics CO6
Probability theory, Different thermodynamic distributions- Boltzmann, Bose –
Einstein & Fermi-Dirac, Laws of thermodynamics & their applications, Properties
of elementary particles.

C. TEXT BOOKS
1. Smith, J. M.; Van Ness, H. C. Introduction to Chemical Engineering
Thermodynamics; Fourth Edition, McGraw Hill Book Company: Singapore, 1987

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 49


2. Sonntag, R. E. & Van Wylen, Gordon J. Fundamentals of Statistical Thermodynamics;
First Edition, John Wiley & Sons: United States of America, 1968

D. REFERENCE BOOKS
1. Narayan, K. V. A Textbook of Chemical Engineering Thermodynamics; Second Edition,
PHI Learning Private Limited: Delhi, 2013
2. Rao, Y.V.C. Chemical Engineering Thermodynamics; First Edition, Universities Press
India Private Limited: Hyderabad, 1997
3. S. Sandler, “Chemical, Biochemical and Engineering Thermodynamics”,4th edition,
Wiley, India
4. Elliot, J.E.; Lira C.T. Introductory Chemical Engineering Thermodynamics; Second
Edition, Pearson Education publishing as Prentice Hall: South Africa, 2012

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Recall the laws of thermodynamics & relationship between the
CO1
fundamental thermodynamic properties.
Discuss the thermodynamic properties for multiphase &
CO2 multicomponent mixtures for the equilibrium separation
Knowledge processes.
Comprehension
Compute numerical problems involving equilibria of different
Application
CO3 phases such as VLE, LLE, VLLE, SLE, SVE as well as reaction
Analysis
equilibria.
Synthesis
Analyze the experimental VLE data for binary mixtures and
CO4 Evaluation
estimate the VLE data using activity models.
CO5 Propose the appropriate classical models for a binary system.
Molecular interpretation of thermodynamic equilibrium &
CO6
compare the of laws of thermodynamics statistical point of view.

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 2 3 3 3 3 2 2.7
PO2 3 3 3 3 3 2 2.8
PO3 2 3 3 3 3 2 2.7
PO4 3 2 3 3 3 2 2.7
PO5 3 2 3 3 3 3 2.8
PO6 2 3 3 3 3 3 2.8
PO7 3 3 3 3 3 2 2.8
PO8 2 3 3 3 3 3 2.8
PO9 2 3 3 3 3 3 2.8
PO10 2 3 3 3 3 2 2.7
PO11 3 2 3 3 3 2 2.7
PO12 3 2 3 3 3 2 2.7
PSO1 2 3 3 3 3 2 2.7
PSO2 2 3 3 3 3 2 2.7
PSO3 2 3 3 3 3 2 2.7
PSO4 3 3 3 3 3 3 3

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 50


B. TECH. – SEMESTER-IV (CH)
EFFECTIVE TECHNICAL COMMUNICATION (HSMC201)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 0 3 3 40 0 0 0 40

A. COURSE OVERVIEW
This course will help students of engineering develop their Linguistic skills. Students will learn
the effective ways of writing technically. Errorless writing and presenting will be developed.
Understanding ways of self-development will make students competent to enhance their
professional and Personal growth. Learning and understanding Professional ethics will help them
be a better professional. Overall, the course is going to help student be competent and efficient
professional

B. COURSE CONTENT
TOPICS COs
1. Module 1: Information Design and Development Different kinds of technical CO1
documents, Information development life cycle, Organization structures, factors
affecting information and document design, Strategies for organization, Information
design and writing for print and for online media.
2. Module 2: Technical Writing, Grammar and Editing Technical writing process, CO1
forms of discourse, Writing drafts and revising, Collaborative writing, creating CO2
indexes, technical writing style and language. Basics of grammar, study of
advanced grammar, editing strategies to achieve appropriate technical style.
Introduction to advanced technical communication, Usability, Hunan factors,
Managing technical communication projects, time estimation, Single sourcing,
Localization.
3. Module 3: Self Development and Assessment Self-assessment, Awareness, CO3
Perception and Attitudes, Values and belief, Personal goal setting, career CO5
planning, Self-esteem. Managing Time; Personal memory, Rapid reading, taking
notes; Complex problem solving; Creativity.
4. Module 4: Communication and Technical Writing Public speaking, Group CO1
discussion, Oral; presentation, Interviews, Graphic presentation, Presentation aids, CO4
Personality Development. Writing reports, project proposals, brochures, CO6
newsletters, technical articles, manuals, official notes, business letters, memos,
progress reports, minutes of meetings, event report.
5. Module 5: Ethics Business ethics, Etiquettes in social and office settings, Email CO3
etiquettes, Telephone Etiquettes, engineering ethics, managing time, Role and
responsibility of engineer, Work culture in jobs, Personal memory, Rapid reading,
taking notes, Complex problem solving, Creativity.

C. TEXT / REFERENCE BOOKS


1. David F. Beer and David McMurrey, Guide to writing as an Engineer, John Willey.
New York, 2004
2. Diane Hacker, Pocket Style Manual, Bedford Publication, New York, 2003. (ISBN
0312406843)
3. Shiv Khera, You Can Win, Macmillan Books, New York, 2003

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 51


D. COURSE OUTCOMES
COs SKILLS STATEMENT
CO1 Speaking and Writing Enhance Professional way of Speaking and Writing,
CO2 Errorless Writing Understand basics of Grammar in Professional writing
Being professionally Understand the Business Ethics, Etiquettes and Values.
CO3
efficient
Focused, organised and Present himself/herself in the effective way at Public, Group
CO4
competent Speaking Discussion and Interview.
Understanding Oneself- Improve Self-awareness and Perception.
CO5 knowing one's
capabilities
Specific Soft Skills Enhance their soft skills required for their professional
CO6
development.

E. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 1 1 1 1
PO2
PO3
PO4
PO5
PO6 2 1 1.5
PO7
PO8 1 3 1 1.7
PO9 2 1 2 3 2 2 2
PO10 3 3 3 3 3 3 3
PO11 2 2 2 1 2 1.8
PO12 1 2 2 2 1 1.6
PSO1 1 1 2 2 1 2 1.5
PSO2 1 2 3 3 2 2 2.2
PSO3 3 2 2 3 3 3 2.7
PSO4 2 2 3 3 2 3 2.5

BACK

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 52


SEMESTER-V
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
Chemical Reaction
PCC108 3 0 3 60 40 25 25 150 4.5
Engineering-I
PCC109 Mass Transfer-II 3 1 3 60 40 25 25 150 5.5
PEC101 Core Elective-I 3 1 0 60 40 0 0 100 4
OEC101 Open Elective-I 3 0 0 60 0 0 0 60 3
Numerical Techniques
PCC107 in Chemical 3 0 2 60 40 25 25 150 4
Engineering
Financial and
HS103 Management 3 0 0 40 0 0 0 40 3
Accounting
TOTAL 18 2 8 340 160 75 75 650 24

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 53


B. TECH. – SEMESTER-V (CH)
CHEMICAL REACTION ENGINEERING-I (PCC108)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 3 6 4.5 60 40 25 25 150

A. COURSE OVERVIEW
Selection, Design, Operation and Troubleshoot Ideal Reactors for various type of chemical
reactions.
Objectives: Basic concepts of Kinetics and Rate law; Interpretation of rate of rate data; Design
and Rating of Ideal Reactors involving homogeneous single reactions; Arrangement of different
type and size of reactors for homogeneous reactions; Concept of Recycle Reactor for controlling
mixing inside the reactors

B. COURSE CONTENT
TOPICS COs
1. Introduction CO1
Introduction to chemical reaction engineering and Classification of chemical CO2
reactions Concept of Chemical kinetics. Role of Thermodynamics in chemical CO3
reaction engineering. Definition of Rate of reaction, Rate expression for various types
of reactions. Variables affecting the rate of reaction: Temperature, Pressure,
concentration, catalyst, inert, surface area etc.
2. Kinetics of Homogeneous Reactions CO1
Effect of concentration on rate of reaction. Terminology in calculation of rate of CO2
reaction: Elementary vs non elementary reactions, Molecularity of reactions, order CO3
and rate constant of reaction, Irreversible vs Reversible reactions, concept of CO4
equilibrium constant. Effect of temperature on rate of reaction: Arrhenius theory,
Collision theory & Transition state theory, comparisons of the theories. Kinetic of
non-elementary reactions: matching reaction mechanism with rate law equation, Rule
based derivation of rate law equation for given reaction mechanism and comparing
with experimental rate law equation.
3. Interpretation of Batch Reactor Data of Homogeneous Reactions CO1
Conversion in terms of concentration and pressure. Using Integral and Differential CO2
method of analysis to obtain kinetics of chemical reaction from obtained experimental CO3
data. Constant and variable volume reaction: irreversible, reversible, series, parallel, CO4
catalytic, autocatalytic reactions, Concept of variable volume reaction. Differential
method of analysis: partial analysis of rate of reaction. Reactions with shifting order:
Reactions with shifting of order from Higher to lower and lower to higher.
4. Introduction to Reactor Design CO5
Introduction to concept of macro and micro mixing. Concept of ideal mixing in CO6
reactors. Definition and characteristics of various ideal reactors: Batch, CSTR,
PFR, Selection of Batch or continuous mode of reactor operation.
5. Single Ideal Reactors CO4
Reactor terminology - space time, space velocity, steady state condition, local CO5
conversion, global conversion, uniform vs. constant T, P and Concentration, Extent CO6
of reaction. Derive equation for Ideal Reactors from first principal model. Apply
design equations of Ideal reactors to real system for single reactions and reactor.
6. Design for Single Reactions CO3
Comparison of various type of reactors for same order. Comparison of same type CO4

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 54


of reactors for various feed ratios for order more than one, comparison of MFR CO5
with that of PFR for same order for constant volume and variable volume CO6
reactors. Comparison of ideal reactors using graphical and analytical method.
Multiple reactor system in series and/or parallel, Equal/unequal size reactors in
series, Reactors of different types in series. Introduction to recycle reactor,
Design of recycle reactor, Solution using graphical method, application of recycle
reactor to autocatalytic reaction
7. Design for Multiple Reactions CO5
Maximizing desired product for parallel and series reactions. Mixed complex CO6
reactions

C. PRACTICAL AND TERM WORK


Experiment pertaining to determination of order and rate constant of reaction using integral &
differential methods of analysis, effect of temperature on rate of reaction, study of pilot scale
reactor. Application of computer by solving ordinary differential equation using numerical
methods to compare the result predicted by numerical method with that of experimental data

D. TEXT BOOKS
1. Levenspiel, O. Chemical Reaction Engineering; 3rd ed.; John Wiley & Sons (Asia) Pvt.
Ltd : Singapore, 2014

E. REFERENCE BOOKS
1. Scott, F. H. Elements of Chemical Reaction Engineering; 5th ed.; Prentice Hall India (p)
Ltd.: New Delhi, 2016
2. Smith, J. M. Chemical Engineering Kinetics; 3rd ed.; McGraw Hill Incorporation:
New York, 2000

F. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand and State the fundamentals of chemical reactions
CO1
(Classification, Definitions) and chemical kinetics
Discuss the thermodynamic properties for multiphase &
CO2 Understanding multicomponent mixtures for the equilibrium separation
Analysing processes.
Applying Explain the concept of Rate of Reaction, Evaluate Kinetic
CO3
Remembering Expression, Examine effect of various parameters on it
Creating Apply Kinetic Expression to experimental data and compare the
CO4
Evaluating results
Define the concept of Ideal Reactor and classify the type of ideal
CO5
reactors
CO6 Select, Design, Operate and Sketch different type of reactors

G. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 2 2 3 2 3 3 2.5
PO2 2 2 3 2 3 3 2.5
PO3 2 2 3 2 3 3 2.3
PO4 2 2 2 2 3 3 2.33
PO5 1 1 2 2 3 3 2
PO6 1 2 2 2 3 2 2
PO7 2 2 3 2 3 2 2.3

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 55


PO8 1 1 2 2 3 3 2
PO9 1 2 2 2 3 2 2
PO10 1 1 2 2 3 3 2
PO11 1 2 2 2 3 3 2.16
PO12 1 2 3 2 3 3 2.3
PSO1 2 3 3 3 2 3 2.67
PSO2 3 3 3 2 3 2 2.67
PSO3 2 3 2 2 2 2 2.17
PSO4 3 3 3 3 3 3 3

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 56


B. TECH. – SEMESTER-V (CH)
MASS TRANSFER-II (PCC109)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 1 3 7 5.5 60 40 25 25 150

A. COURSE OVERVIEW
Motivation: Study, Design, Operation and Application of various Mass transfer operation and
equipments in Chemical Process Industry.

B. COURSE CONTENT
TOPICS COs
1. Gas Absorption CO1
Equilibrium solubility of gases in liquids. Concept of idea and non-ideal solution. CO3
Material balance for single component transfer in absorption and stripping. CO5
Minimum Liquid-gas ratio and its significance. Counter current multi stage
operation. Absorption factor and Stripping factor with significance. Solvent
Selection Criteria for absorption. Multistage & packed tower operation. Concept of
HETP and transfer units.
2. Humidification CO2
VLE and Enthalpy for pure substances. Saturated & Unsaturated vapour–gas CO6
mixture and related terminologies such as dry bulb temperature, dew point, wet
bulb temperature, percentage & relative saturation, adiabatic saturation
temperature, humid heat, humid volume etc. Psychometric Chart in
Humidification & dehumidification. Adiabatic saturation curves, wet bulb
temperature theory, Lewis’s relation Adiabatic & non-adiabatic operations. Types
of cooling tower & design.
3. Liquid-Liquid Extraction CO2
Equilibrium in extraction. Ternary diagram & tie line data. System of three CO4
liquids-one pair & two pairs partially soluble. Single stage & multistage CO5
extraction, Co-current and cross current extraction, Continuous counter current
multistage extraction with and without reflux, Theory & performance of
continuous contact equipments, Single stage & multistage equipments
4. Adsorption & Ion Exchange CO2
Adsorption, Definition and industrial application. Types of adsorption & most
commonly used adsorbents. Adsorption Equilibria & hysteresis, Effect of
temperature on adsorption & Heat of adsorption. Adsorption of solute from dilute
liquid Material balance and Freundlich’s equation for single stage operation and
multistage cross-current operation, counter current operation, Equipments for
adsorption. Ion-Exchange Principles, Applications, Equilibria and Rate of ion-
exchange
5. Drying CO5
Equilibrium in drying. Batch drying & its mechanism, Continuous drying. CO6
Various types of moisture in drying. Rate of drying & time of drying. Cross-
circulation drying. Batch & continuous drying equipments-Tray dryer, Tunnel
dryer, Rotary dryers, Spray dryers, Fluidized bed dryer, etc
6. Leaching CO6
Steady state and unsteady state leaching operations. Single stage leaching.
Multistage cross current and counter current leaching. Rate of leaching.

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 57


Application of leaching. Leaching equipments
7. Crystallization CO1
Principle of crystallization. Saturation & methods of saturation. Nucleation & CO2
Crystal Growth. Crystallization rate, Equilibria and yields. Caking of crystals,
Application of crystallization, Crystallization equipments, Crystallization from
melts
8. Introduction to Novel Separation Techniques CO1
Types of Novell Séparation techniques. Membrane Séparation processes like
Ultra filtration, Nano filtration, Reverse Osmosis etc.

C. TEXT BOOKS
1. Treybal, R.E. Mass Transfer Operations,3rdEd.; Tata McGraw Hill:New Delhi, 2012
2. McCabe, W.L.;Smith. J.C.; Harriot, P. Unit Operations in Chemical Engineering, 4th
Ed.; McGraw Hill Publications: NY, 1985

D. REFERENCE BOOKS
1. Dutta, B.K. Principles of Mass Transfer and Separation Processes, 2nd Ed.; Prentice Hall
of India: 2007
2. Foust, S. Principles of Unit Operations, 2nd Ed.; Wiley: New York, 1980

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand how to use the basic fundamentals of Mass transfer in
CO1
designing the unit operation equipments.
Understand Relate the theoretical fundamentals with practical aspects to improve
CO2
Relate the performance.
CO3 Design Design (process) all Mass transfer equipments.
Optimize Optimize the process and design parameters related to mass transfer
CO4
Application equipments.
CO5 Develop Apply the design simulation tools to optimize the real process.
Develop analytical skill of the students that helps in to solve the
CO6
problems associated with real situation.

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 3 3 2 2.8
PO2 3 3 3 3 2 2 2.5
PO3 3 2 3 2 2 2 2.3
PO4 2 2 2 2 2 2 2
PO5 2 2 2 2 2 2 2
PO6 2 2 2 2 2 2 2
PO7 2 2 2 2 2 2 2
PO8 3 2 3 2 3 3 2.7
PO9 2 2 2 2 2 2 2
PO10 3 3 3 2 2 2 2.5
PO11 2 2 2 2 2 2 2
PO12 3 3 3 2 2 2 2.5
PSO1 3 3 3 2 3 3 2.8
PSO2 3 3 3 3 3 3 3
PSO3 3 3 3 3 3 3 3
PSO4 3 3 3 3 3 2 2.8

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 58


B. TECH. – SEMESTER-V (CH)
NUMERICAL TECHNIQUES IN CHEMICAL ENGINEERING (PCC107)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 2 5 4 60 40 25 25 150

A. COURSE OVERVIEW
Numerical solutions of various mathematical models describing steady state and dynamic
behaviours of Chemical Process Systems and parameter estimation using numerical methods
in Chemical Engineering.
Objectives: To introduce students to numerical methods used for solving engineering problems,
in particular chemical engineering problems, using numerical methods and computer
programming. Fundamentals of numerical methods/algorithms to solve systems of different
mathematical equations (e.g. linear/nonlinear algebraic equations, ordinary / partial differential
equations) will be introduced. The course would enable students to write their own computer
programs using programming languages like C/C++ and commercial software like MATLAB.
Hands-on experience will be provided to apply these computer programs to solve problems in
different areas of chemical engineering, e.g. fluid flow, heat and mass transfer, chemical
reaction engineering etc. Practical are involved for solving actual chemical engineering
problems through computer programming and coding.

B. COURSE CONTENT
TOPICS COs
1. Basics of Vectors, Scalars and matrix algebra CO1
Addition/subtraction, multiplication/division of vectors, matrix multiplication, CO3
inverse of matrix, determinant and rank of matrix, eigen values, sparse matrices,
Use of MATLAB for matrix algebra, approximation and concept of error and
error analysis
2. Numerical methods for linear algebraic equations CO1
Gauss elimination method, Gauss-Jordan method, Jacobi method, Successive – To
over relaxation method, tri-diagonal matrix, MATLAB programming CO3
3. Numerical methods for nonlinear algebraic equation CO1
Successive substitution method, Newton-Raphson method, Secant method, False To
position method, single variable and multivariable case studies, MATLAB CO5
functions for nonlinear algebraic equations
4. Eigen Value Problems CO1
Eigen value analysis of linear and nonlinear systems and solution of To
homogeneous equations using eigen values CO3
5. Regression, interpolation, curve fitting, numerical integration CO1
Simple interpolation, Lagrange’s interpolation, Newton’s interpolation, To
Simpson’s rule, trapezoid method, linear regression, polynomial regression, CO3
exponential and power regression, MATLAB routines and commands
6. Numerical methods for IVP and BVP ordinary differential equations CO1
Explicit and implicit ODEs, Euler’s explicit and implicit methods, explicit To
Adams- Bashforth methods, implicit Adams-Mouton methods, Predictor – CO6
corrector methods, Runge-Kutta methods, MATLAB solvers for ODEs, Finite
difference, Orthogonal collocation and Orthogonal collocation on finite-element
methods for ODE-BVP, Shooting Methods for solving BVP

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 59


7. Numerical methods for Partial differential equations CO1
Steady state and dynamic PDES, method of lines, Crank-Nicholson method, To
finite- difference, Orthogonal collocation and orthogonal collocation on finite CO6
element method

C. PRACTICAL AND TERM WORK


Simulation experiments are designed to use MATLAB software for solving linear/nonlinear
algebraic equations for steady state problems in Chemical Engineering and for solving dynamic
problems in Chemical Engineering. Simulation experiments for parameter estimation problems
in chemical engineering systems are also designed

D. TEXT BOOKS
1. Gupta, S. K. Numerical Methods for Engineers, 3rd ed.; New Age International
Publishers: New Delhi, 2015
2. Chapra, S. C. Applied Numerical Methods with MATLAB for Engineers and Scientist,
3rd ed.; McGraw-Hill: New York, 2012

E. REFERENCE BOOKS
1. Beers, K J. Numerical Methods for Chemical Engineering Applications in MATLAB,
Cambridge University Press: UK, 2006
2. Constantinides, A.; Mostoufi, N. Numerical Methods for Chemical Engineers with
MATLAB Applications, Prentice Hall International Series: New Jercy, 1999

F. COURSE OUTCOMES
COs SKILLS STATEMENT
Remember and understand the various numerical methods to solve
various linear and nonlinear steady state and dynamic problems in
CO1
chemical engineering systems described by ODE,
PDE, AE and NAE
Carry out the error analysis in the numerical solutions of chemical
CO2 Understanding engineering problems
Analysing Apply linear algebraic equation solution techniques and nonlinear
Applying
algebraic equation techniques for solving steady states of chemical
CO3 Evaluating
engineering systems. Use MATLAB to implement numerical
Creating
methods in simulations.
Remembering
Evaluating Do critical evaluation of the performance of various numerical
CO4 methods using simulations for solving chemical engineering
problems.
CO5 Develop MATLAB codes for various numerical methods
Generate a MATLAB program for industrial application to carry
CO6
out steady state and dynamics analysis.

G. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 2 2 2 3 2 3 2.3
PO2 1 1 3 3 3 3 2.3
PO3 1 2 3 3 3 3 2.5
PO4 1 1 2 3 2 3 2
PO5 0 0 2 3 3 3 1.8
PO6 2 2 3 3 3 3 2.7

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 60


PO7 2 3 3 3 3 3 2.8
PO8 1 1 2 2 2 3 1.8
PO9 2 2 3 2 3 3 2.5
PO10 1 2 3 2 2 3 2.2
PO11 2 3 3 2 2 3 2.5
PO12 3 3 3 2 3 3 2.8
PSO1 2 3 3 3 2 3 2.67
PSO2 3 3 3 2 3 2 2.67
PSO3 2 3 2 2 2 2 2.17
PSO4 3 3 3 3 3 3 3

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 61


B. TECH. – SEMESTER-V (CH)
FINANCIAL MANAGEMENT AND ACCOUNTING (HSMC103)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 0 3 0 40 0 0 0 40

A. COURSE OVERVIEW
Motivation: Analyze businesses’ financial position and performance, selection of appropriate
management accounting techniques to make informed decisions.
Objective: The need to understand concepts of accountancy is essential for better decision
making in personal and professional life, principles of accounting applied to make financial
statements which can be understood by the internal and external stakeholders. Management
accounting for understanding the concepts of marginal costing and absorption costing, and
Cost- Volume-Profit analysis. Concepts such as fundamental analysis, ratio analysis, and break-
even analysis are important to compare different companies of the same industry.

B. COURSE CONTENT
TOPICS COs
1. Financial Accounting – An Introduction CO1
Introduction. Meaning of Accountancy. Book-keeping and Accounting.
Accounting Process. Objectives for accounting. Differences between book-
keeping and accounting Users of accounting information. Limitations of
Accounting and basic terminologies
2. Accounting Concepts, Principles, Bases and Policies CO1
Introduction, Accounting Concepts, Principles, Policies and Standards, CO3
Types of accounting concepts - Business Separate entity concept, Going
concern concept, Money measurement concept, Periodicity concept, Accrual
concept,
Accounting Principles - Principle of Income recognition, Principle of expense,
Principle of matching cost and revenue, Principle of Historical costs, Principle of
full disclosure, Double aspect principle, Modifying Principle, Principle of
materiality, Principle of consistency, Principle of conservatism or prudence,
Accounting Policies - Changes in Accounting Policies, Disclosure in case of
changes in Accounting Policies,
Accounting Standards - Scope and functions of Accounting Standards Board,
International Financial Reporting System
3. Double Entry Accounting CO2
Introduction, meaning of double entry accounting, Classification of accounts
under Traditional approach, Classification of accounts under Accounting
Equation approach, Comparison of traditional approach with Modern approach
equal approach, Accounting Trail, Transactions and events, Meaning and roles
of debit and credit, Accounting equation
4. Secondary Books CO2
Introduction, Secondary books, Purchases Book/Purchases Day book, Cash
discount, Trade discount, Difference between cash discount and trade discount,
Sales Book or Sales Day book, Purchase Returns Book, Sales Returns Book,
bills receivable book, bills payable book, Cash book, Posting to Ledger
accounts, Posting to Ledger

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 62


5. Trial Balance CO2
Introduction, Meaning, Objectives of preparing a trial balance, Methods of
preparing a trial balance, Preparation of Trial balance, Adjusting Entries, Errors
and their rectification, Errors disclosed by Trial Balance, Errors not disclosed by
Trial Balance, Steps to locate the errors
6. Final Accounts CO2
Introduction, Adjustments before preparing final accounts, Depreciation, Bad CO3
Debts and accounting treatment of bad debts, Provision for doubtful debts,
Reserves for Discount on Debtors, Reserve for Discount on Creditors, Closing
Stock, Trading Account, Profit and Loss Account, Balance Sheet
7. Introduction to Management Accounting CO2
Introduction, Meaning of Management accounting, The Role of Management CO4
Accounting, Management Accounting Framework, Functions of Management
Accounting, Tools of Management Accounting, The Balanced Scorecard, Cost
Management System, Value Added Concept, Merits of Management
Accounting, Demerits of Management Accounting Distinction between
Management Accounting and Financial Accounting
8. Financial Statement Analysis CO3
Introduction, Meaning of Ratio, Steps in Ratio Analysis, Classification of
Ratios, Du Pont Chart, Solved Problems, Advantages of Ratio Analysis,
Limitation of Ratio analysis
9. Cash Flow Analysis CO2
Introduction, Meaning of Cash Flow Statement, Purpose of Cash Flow CO3
Statement, Preparation of Cash Flow Statement, Format of Cash Flow Statement
(AS3: Revised Method), Cash Flow from Operating Activities, Cash Flow
Statement under Direct Method, Different between Cash Flow Analysis and
Fund Flow Analysis, Uses of Cash Flow Statement
10. Marginal Costing and Break-Even Analysis CO2
Introduction, Concept of Marginal Costing, Characteristics of Marginal Costing, CO4
Difference between Absorption Costing and Marginal Costing, Marginal Cost, CO5
Contribution, Cost Volume Profit (CVP) Analysis, Break Even Chart, Break
Even Point, Profit Volume ratio or MCSR, Target profit, Margin of Safety,
Application of Marginal cost, Limitations of Marginal cost, Solved Problems
11. Basics of Financial Management CO2
Introduction of Financial Management, Objectives of financial management, CO4
Role of finance manager, Functions of financial management, Concept of time CO6
value of money, Present value, Future value, Annuity concept, Solved problems

C. TEXT BOOKS
1. S.K. Bhattacharya, John Dearden, Financial Accounting for Managers – Text book &
cases, Vikash Publishing House Private Limited, 2009
2. Ravi M. Kishore, Management Accounting, Taxman, 2018

D. REFERENCE BOOKS
1. M.N. Arora, A Text Book of Cost Accountancy, Vikas Publishing, 2010
2. B.K. Bhar, Cost Accounting: Method & Problems, Academic Publishers, 2012
3. Horngren, Foster & Datar, Cost Accounting – A Managerial Emphasis, Prentice Hall,
1997
4. N.K. Prasad & A.K. Prasad, Cost Accounting, Book Syndicate, 2016
5. Edmonds, Edmonds and Tsay, Fundamental Managerial Accounting Concept, Irwin
McGraw Hill, 2013
6. Asish Bhattacharya, Principles and Practice of Cost Accounting, Sultan Chand, 2004
7. R.S.N. Pillai & Bhagavati, Management Accounting, S. Chand, 2010

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 63


8. Moriarty and Allen, Cost Accounting, John Wiley, 1991
9. Bhabatosh Banerjee, Cost Accounting – Theory & Practices, Sultan Chand & Sons, 2014
10. V.K. Saxena & C.D. Vashist, Advanced Cost & Management Accounting – Problems
& Solutions, Prentice Hall of India (P) Ltd., 2015
11. R.S.N. Pillai & Bhagavati, Cost Accounting, S. Chand, 2010
12. S.N. Maheshwari, Studies in Cost Management, Sultan Chand & Sons, 2013
13. M.E. Thukaram Rao, Cost and Management Accounting, New Age International, 2004
14. M.E. Thukaram Rao, Management Accounting, New Age International, 2003

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand the concepts and principles of accounting, double- entry
CO1
book-keeping, limitations and objectives of accounting
Analyse the accounting cycle and process involved in financial and
CO2
Comprehension management accounting
Analysis Evaluate financial statements given in annual reports of listed
CO3
Evaluate companies and apply the same knowledge in real life.
Comprehension Understand the objectives of management accounting and apply
CO4
Application the techniques utilized in management accounting
CO5 Utilize the concepts of break-even analysis and marginal costing
Outline time value of money concepts and implement them to analyse
CO6
real life situations

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 1 2 2 3 3 3 2.33
PO2 2 2 2 3 3 3 2.5
PO3 1 2 2 2 3 3 2.16
PO4 1 1 3 3 2 3 2.16
PO5 2 2 3 3 3 3 2.67
PO6 3 1 2 3 2 2 2.16
PO7 1 2 3 2 2 1 1.83
PO8 3 3 3 3 1 2 2.5
PO9 2 2 3 3 2 2 2.33
PO10 2 2 3 2 3 3 2.5
PO11 3 3 3 3 3 3 3
PO12 3 2 3 3 3 3 2.8
PSO1 2 2 2 2 2 3 2.17
PSO2 2 2 2 3 2 3 2.33
PSO3 2 3 3 3 3 3 2.83
PSO4 3 3 3 3 3 3 3

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 64


B. TECH. – SEMESTER-V (CH)
ENVIRONMENTAL ENGINEERING (PEC101)
(CORE ELECTIVE-I)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 1 0 4 4 60 40 0 0 100

A. COURSE OVERVIEW
Environmental engineering deals with the application of engineering principles to the control,
modification and adaption of the physical, chemical and biological factors of the environment
in the interest of human’s health, comfort and social wellbeing. The student will identify and
troubleshoot for environmental pollution problems.

B. COURSE CONTENT
TOPICS COs
1. Introduction to Environmental Pollution CO1
Introduction to environment, Biosphere, Hydrological and nutrient Cycles, Types
of pollution and Pollutant
2. Air Pollution CO2
Sources and Effects: Air pollution – Definition and concentrations, classification
and properties of air pollutants, criteria air pollutants, Photochemical smog,
emission sources for air pollutants, Air pollution laws and standards in India,
behaviour and fate of various air pollutants in atmosphere, Effects of air pollution
on health, impact on vegetation and materials.
Meteorological aspects of air pollutant dispersion: Meteorology – definition
and parameters, Temperature lapse rate, Inversion and atmospheric stability,
Plume behaviour, Dispersion of air pollutants – The Gaussian plume model
Air pollution sampling and measurement: Ambient air sampling and stack
sampling, Collection of gaseous air pollutants and Particulate pollutants,
Analysis of air pollutants
Air pollution control methods and Equipments: Control methods, Principle
and design of particulate matter control devices- gravitational settling chambers,
cyclone separators, bag house filters, electrostatic precipitators, wet and dry
scrubbers. Control of specific gaseous pollutants: Control of specific gaseous
pollutants: Modification of operating conditions, modification of design
conditions, effluent gas treatment methods.
3. Waste water engineering CO3
Origin of waste water and waste water flow rates: Introduction to waste CO4
pollution, Reasons for waste water treatment, Introduction to treatment
operations, process and concepts, Components of waste water flow rates, Waste
water sources and flow rates, Variation in wastewater flow, Analysis of waste
water flow rate data, Reduction of waste water flows.
Waste water characteristics: Physical, Chemical and Biological characteristics
of wastewater
Waste water treatment: Objective and classification of waste water treatment,
Major factors for selection of system, Design parameters for waste water
treatment, Reactor used in waste water treatment
Physical unit operation and their design: Objective and Application of Physical
unit operations in waste water treatment, Various unit operations – Screening,

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 65


Grit chambers, Flow equalization, Flocculation, Flotation., Sedimentation,
Design of various units- Screening, Flow equalization, Flotation, Sedimentation.
Chemical Unit processes: Objective and Application of Chemical unit processes
in waste water treatment, Various chemical unit processes – Chemical
Precipitation, Disinfection
Biological Unit processes: Objective of Biological unit processes in waste
water treatment, Important definition, Classification of biological unit processes,
Bacterial growth and Kinetics of Bacterial growth, Suspended growth treatment
process – Activated sludge process- Modification, Design, Aerated lagoons,
Aerobic attached growth treatment processes – trickling filters & its design,
rotating biological contractors, Introduction to anaerobic suspended growth
treatment processes attached growth treatment process, sludge treatment &
disposal,
Introduction to advanced waste water treatment
4. Solid waste management CO5

C. TEXT BOOKS
1. Metcalf and Eddy, Wastewater Engineering, Treatment and Reuse,15th ed.; Tata
McGraw Hill, New Delhi, 2003
2. C. S. Rao., Environmental Pollution Control Engineering,3rd ed., New Age International
Publishers, Delhi, 2018

D. REFERENCE BOOKS
1. Scott, F. H. Elements of Chemical Reaction Engineering; 5th ed.; Prentice Hall India (p)
Ltd.: New Delhi, 2016
2. Smith, J. M. Chemical Engineering Kinetics; 3rd ed.; McGraw Hill Incorporation:
New York, 2000
3. Peavy, H.S., Rowe, D.R., Tchobanoglous, G. Environmental Engineering, Indian
editon, Tata McGraw Hills
4. Martin Crawford, Air pollution control theory, Tata McGraw-Hill
5. G. L. Karia and R. A. Christian, Waste water treatment – Concepts and Design
approach,2nd ed.; East Economy Edition

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand the sources, effects and control measure of different
CO1
types of pollution. (Air, Water, Land etc.)
Analyse general air pollution problems, meteorological aspects, control
CO2
and measure of particulate pollutants and gaseous pollutants.
Apply the basic knowledge on water pollutants and waste water
CO3 Evaluate characteristics and build expertise in analysis and testing of water
Comprehension
samples.
Application
Evaluate the significance of various unit operations and unit
Synthesis
Analysis processes involved in waste water treatment, Create design of specific
CO4
treatment methods for effluents of various chemical
process industries
Understand about solid waste, remember problems associated with
CO5 solid waste disposal, evaluating various methods for solid waste
treatment.

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 66


F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 AVG.
PO1 2 3 3 3 2 2.6
PO2 2 3 3 2 1 2
PO3 1 2 2 3 2 2
PO4 2 2 2 2 1 2.8
PO5 2 2 2 2 1 2.8
PO6 2 2 2 2 1 2.8
PO7 3 2 2 2 2 2.2
PO8 1 2 2 2 2 2.8
PO9 2 2 2 2 2 2
PO10 1 2 2 2 2 2.8
PO11 1 2 2 2 2 2.8
PO12 2 2 2 2 2 2
PSO1 1 2 2 1 1 2.4
PSO2 1 1 2 2 1 2.4
PSO3 1 1 1 2 1 2.1
PSO4 1 1 1 1 2 2.1

BACK

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 67


SEMESTER-VI
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
Chemical Reaction
PCC112 3 0 3 60 40 25 25 150 4.5
Engineering-II
Chemical System
PCCXXX 3 1 0 60 40 0 0 100 4
Modeling
Instrumentation and
PCC117 3 1 3 60 40 25 25 150 5.5
Process Control
Process Equipment
PCCXXX 3 0 3 60 40 25 25 150 4.5
Design and Drawing
Core Elective-II (1),
PEC102 3 0 0 60 0 0 0 60 3
(2), (3)
OEC102 Open Elective-II 3 0 0 60 0 0 0 60 3
TOTAL 18 2 9 360 160 75 75 670 24.5

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 68


B. TECH. – SEMESTER-VI (CH)
CHEMICAL REACTION ENGINEERING-II (PCC112)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 3 6 4.5 60 40 25 25 150

A. COURSE OVERVIEW
Motivation: Analysis, design, selection and operation of chemical reactors for non-ideal, non-
isothermal and heterogeneous reactions in chemical process industries
Objectives: Fundamentals of non-ideality in reactors and change in conversion, Basic concepts
of non-isothermal operations and design, Fundamentals of catalysis, mechanisms and kinetics
of catalytic reactions, Basic analysis and design of fixed bed, fluidized bed, trickle bed and slurry
reactors, Fundamentals and design of non-catalytic multiphase reactors (fluid-fluid, fluid-solid)

B. COURSE CONTENT
TOPICS COs
1. Non-ideal Reactors CO1
RTD theory, understanding RTD curves and moments, Finding out RTD by CO6
experiments – Pulse and Step Input, Models for non-ideal flow – zero (segregation
& maximum mixedness), one (Dispersion and TIS) and two parameter models
2. Non-isothermal Operations and Design CO2
Material and Energy balances for CSTR and PFR/PBR, Design Algorithms for CO6
CSTR and PFR/PBR, Adiabatic and non-adiabatic design Procedures, Unsteady-
state Batch reactor design Procedures, Concept of Multiple Steady states in CSTR
3. Fundamentals of Catalytic Reactions CO3
Mechanism of solid catalyzed reaction, Experimental Methods for studying kinetics CO6
of catalytic reactions and data analysis, Design of Fixed bed catalytic reactors,
Design of Fluidized bed catalytic reactors, Design of Trickle bed catalytic reactors
4. Fundamentals of Fluid-Fluid Reactors and Reactor Design CO4
Kinetic regimes for mass transfer & reaction, Enhancement factor in gas-liquid CO6
reactions, Design of towers/tanks for fast & slow reactions
5. Fundamentals of Fluid-Solid Reactors and Reactor Design CO5
Rate equation for heterogeneous reactions, the concept of rate controlling step, CO6
Design of Plug flow, Fluidized bed reactors
6. Professional Ethics in Chemical Reaction Engineering
Discussion on engineering ethical considerations, focusing on problems
following best practices, Discussion of social and environmental considerations,
the importance of considering engineering ethics

C. PRACTICAL AND TERM WORK


Experiments to determine RTD & conversion form RTD for various geometries under laminar
& turbulent flows, heterogeneous reaction system, and application of tank in series & dispersion
models, RTD in a pilot scale batch reactor

D. TEXT BOOKS
1. Levenspiel, O. Chemical Reaction Engineering; 3rd ed.; John Wiley & Sons (Asia)
Pvt. Ltd : Singapore, 2014
2. Scott, Fogler. H. Elements of Chemical Reaction Engineering; 5th ed.; Prentice Hall India

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 69


(p) Ltd.: New Delhi, 2016

E. REFERENCE BOOKS
1. Smith, J. M. Chemical Engineering Kinetics; 3rd ed.; McGraw Hill Incorporation:
New York, 2000

F. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand and Analyse the non-ideality in the reactors and Evaluate
CO1
its performance
Apply energy balance, Analyse and Design PFR, CSTR and Batch
CO2
Understand type non-isothermal reactors
Analysis Develop Kinetic Expression from heterogeneous reaction experimental
CO3
Evaluate data and analyze the reaction mechanism involved
Application Analyse different control regimes and design fluid-fluid contactors
CO4
Create accordingly
CO5 Analyse and Design of non-catalytic fluid-solid reactors
Critiquing Industrial Reactor and Implement solution Methodology for
CO6
optimum Design of actual reactors

G. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 3 3 3 3
PO2 3 3 3 3 3 3 3
PO3 3 3 3 3 3 3 3
PO4 3 3 3 3 3 3 3
PO5 3 3 3 3 3 3 3
PO6 3 3 3 3 3 3 3
PO7 3 3 3 3 3 2 2.8
PO8 3 3 3 3 3 3 3
PO9 3 3 3 3 2 2 2.7
PO10 3 3 3 3 2 2 2.7
PO11 3 3 3 3 3 3 3
PO12 3 3 3 3 2 2 2.7
PSO1 3 3 3 3 2 2 2.7
PSO2 3 3 3 3 2 2 2.7
PSO3 3 3 3 3 2 2 2.7
PSO4 3 3 3 2 2 3 2.7

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 70


B. TECH. – SEMESTER-VI (CH)
CHEMICAL SYSTEM MODELING (PCCxxx)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 1 0 4 4 60 40 0 0 100

A. COURSE OVERVIEW
Motivation: To have a good grasp of mathematical modelling and its basic classification of various
process, such as deterministic and stochastic processes. Students are made aware with specific
applications of mathematical modelling in chemical engineering, which is generally referred to
as chemical systems modelling
Objectives: The basic objective of this subject to give general approach for the model formulation
of various chemical engineering systems, Applying the basic principles of chemical engineering to
the various systems

B. COURSE CONTENT
TOPICS COs
1. Modeling Overview CO1
Physical modelling, mathematical modelling and its classification, principles of
similarity in physical modelling, concepts of independent variables, dependent
variables, boundary conditions partial Differential Equations & finite Difference
2. Mathematical Modelling in Mass Transfer CO2
Single stage, 2 stage & N stage extraction of steady state mass transfer process, CO6
unsteady state formulation of single stage extraction, unsteady state mass transfer
(Fick’s second law), gas absorption accompanied by chemical reaction
(mathematical model formulation), finite difference – solvent extraction in N
stage process, gas absorption in N stages (Kremser – Brown), N stirred tanks
reactors in series, etc.
3. Mathematical Modelling in Heat Transfer CO3
Steady state heat conduction through hollow cylindrical pipe using various CO6
boundary conditions, unsteady state process of steam heating of liquid, heat
transfer through extended surfaces (triangle & rectangle), steady state counter
current cooling of tanks, unsteady state heat loss through maturing tank, unsteady
state heat conduction, gas pre-heater, heat loss through circular flanges
4. Mathematical Modeling in Reaction Engineering CO4
The model of the chemical reaction with diffusion in a tubular reactor, chemical CO6
reaction with heat transfer in a packed bed reactor, gas absorption accompanied by
chemical reaction and reactors in series.
5. Mathematical Modelling in Fluid Mechanics CO5
Continuity equation, model formulation of flow through a packed bed column, CO6
models on momentum transfer such as laminar flow in a narrow slit, model of flow
between concentric cylinders and concentric spheres
6. Professional Ethics in Chemical System Modeling
Ethical considerations for Modeling approach. Motivating the students to
consider socio-environmental issues in a serious manner. Best practices to be
followed with engineering ethics

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 71


C. TEXT BOOKS
1. B.V. Babu, Process Plant simulation, Oxford University Published in India
2. Jensen V. G.; Jeffreys G. V., Mathematical Methods in Chemical Engineering,
Academic Press, New York
3. Mickley H S; Sherwood T S; Reed C E, Applied Mathematics in Chemical
Engineering 2nd Ed. Tata McGraw Hill Publishing Co. Ltd., New Delhi

D. COURSE OUTCOMES
COs SKILLS STATEMENT
Understanding Understand and State the fundamentals of general approach on the
CO1
modeling of chemical systems
Application Explanation of the concept of mathematical modeling of mass transfer
CO2
Analysis unit operations
Application Conceptual modeling of heat transfer unit operations
CO3
Analysis
Application Fundamentals of mathematical modeling in reaction engineering
CO4
Analysis
Application Explain the concept of mathematical modeling of fluid flow unit
CO5
Analysis operations
CO6 Create Discussion on the modelling approach of real industrial problems

E. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 3 3 3 3
PO2 3 3 3 3 2 3 2.8
PO3 3 3 3 3 3 2 2.8
PO4 3 3 3 3 3 3 3
PO5 3 3 3 3 3 3 3
PO6 3 3 3 3 3 3 3
PO7 3 3 3 3 3 2 2.8
PO8 3 3 3 3 3 3 3
PO9 3 3 3 3 2 2 2.7
PO10 3 3 3 3 2 2 2.7
PO11 3 3 3 3 3 3 3
PO12 3 3 3 3 2 2 2.7
PSO1 3 3 3 3 3 2 2.8
PSO2 3 3 3 3 2 2 2.7
PSO3 3 3 3 3 2 3 2.8
PSO4 3 3 3 2 2 3 2.7

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 72


B. TECH. – SEMESTER-VI (CH)
INSTRUMENTATION AND PROCESS CONTROL (PCC117)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 1 3 7 5.5 60 40 25 25 150

A. COURSE OVERVIEW
Design of feedback, feedforward and other control structures and its application to process
industries.

B. COURSE CONTENT
TOPICS COs
1. Introductory Concepts: Need for control and automation, control logic, servo and CO1
regulatory control-block diagrams, control structures (feedback vs. feedforward), CO2
process and instrumentation diagrams. Laplace transforms, solution of ODEs
using Laplace transform. Temperature measuring devices
2. Transfer function approach, response of first order systems: step, impulse and CO1
sinusoidal response, first order systems in series. Level measurement CO6
3. Second order systems, higher order systems, transportation lag and dead time. CO1
Flow measuring instruments
4. Linear closed loop systems, development of block diagrams, classical feedback CO2
controllers. Final control element (control valves), block diagram reduction CO1
Closed loop response, servo and regulatory problems Pressure measuring
instruments/sensors
5. Stability analysis, Routh stability criterion, Root locus diagrams (rule based). CO3
Introduction to frequency response, notion of stability. Bode diagrams, Nyquist CO5
plots, Bode and Nyquist stability criterion CO6
6. Controller tuning: Ziegler-Nichol’s method, Cohen-Coon method. Introduction CO4
to advanced controllers: cascade control, feed forward control, ratio control, CO6
Smith- predictor, IMC, MPC, dead-time compensation. Introduction to digital
control

C. TEXT BOOKS
1. Coughanowr D R; LeBlanc S E, Process System Analysis & Control,3rd Edition,
Chemical Engineering series, McGraw Hill Publishing Co.: Newyork,2009
2. Eckman D, Industrial Instrumentation, Wiley & Sons: 1950

D. REFERENCE BOOKS
1. Stephanopoulos G, Chemical Process Control: An introduction to theory and practice, P
T R Prentice Hall: New Jersey, 2003

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand Understand the system and analyse the same with the help of science
CO1
Design and engineering fundamentals
Troubleshoot Design and draw Piping and instrumentation diagram for given
CO2
Application process

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 73


CO3 Analysis Modify and trouble shoot the control systems and loops
Develop Build a bridge between theoretical and practical concepts while
CO4
implementing systems engineering concepts
Utilize the process knowledge and existing simulation tools while
CO5
analysing loops.
Develop analytical thinking to overcome simple system engineering
CO6
related problems

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 3 3 3 3
PO2 3 3 3 3 3 3 3
PO3 3 3 3 3 3 3 3
PO4 2 3 2 3 3 2 2.5
PO5 3 3 3 3 3 2 2.8
PO6 3 3 3 2 3 2 2.7
PO7 2 3 3 2 2 2 2.3
PO8 3 3 2 2 2 2 2.3
PO9 2 3 2 2 2 2 2.2
PO10 1 1 2 1 2 2 1.5
PO11 1 2 2 2 2 2 1.8
PO12 3 3 3 3 3 2 2.8
PSO1 3 2 3 3 2 3 2.7
PSO2 3 3 2 3 3 3 2.8
PSO3 3 3 3 2 2 3 2.7
PSO4 3 2 3 2 3 3 2.7

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 74


B. TECH. – SEMESTER-VI (CH)
PROCESS EQUIPMENT DESIGN AND DRAWING (PCC---)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 3 6 4.5 60 40 25 25 150

A. COURSE OVERVIEW
Design and fabrication of components of Industrial Chemical Vessels under various operating
conditions
Objectives: The main objective of the course is to carry out mechanical design of Process
Equipment in chemical process industries. The subject deals with introduction to Mechanical
properties of Material of constructions and its selection for fabrication of vessels. The design of
process vessel is done for Unfired Pressure vessels. The course focuses on designing main
components of pressure vessel. It also deals with designing special components of pressure vessel
for particular vessel as per their functions.

B. COURSE CONTENT
TOPICS COs
1. Introduction CO1
• Introduction to design and drawing. CO3
• Basic considerations in mechanical design of process equipment.
• Concept of pressure vessel, definition and type, selection of type of vessel.
• Methods of fabrication of vessel, economic consideration.
2. Vessel Design CO1
• Selection Criteria for vessel design. CO2
• Design Preliminaries like excessive allowable stress, design stress, factor CO3
of safety, Poisson’s ratio, elastic deformation, plastic instability, brittle
rupture, creep, thickness of vessel wall.
• Introduction to vessel codes and standards.
3. Vessels under Internal Pressure CO2
• Design of pressure vessels under internal pressure CO3
• Design of wall thickness based on Lame theorem and membrane stress CO4
theory CO5
• Types of closers for pressure vessel, design thickness of closer
• Selection and Design of nozzles and reinforcement pads
• Introduction to flanges and gasket, types and selection, design of flanges
for pressure vessels.
4. Vessels under External Pressure CO2
• Industrial pressure vessels under external pressure CO3
• Design of vessel wall in presence and absence of stiffeners using CO4
analytical & graphical methods CO5
• Design of circumferential stiffeners CO6
• Design of closers subjected to external pressure.
5. Reaction vessels CO3
• Introduction to various components of reaction vessel CO4
• Selection and design of various jackets and Coil CO5
Selection and design of Agitators based on torque, moment and critical speed. CO6
6. Storage Vessels CO3
• Identification for storage for non-volatile & volatile liquids, storage of gases CO4

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 75


• Types & constructional features of storage vessels CO5
• Rectangular storage tank design CO6
• Design of cylindrical storage tank, course to course calculation of wall
thickness, bottom design, roof design
7. Design of Tall Columns CO3
• Industrial requirement of tall vessels CO4
• Construction & features in column stress & determination of shell thickness CO5
CO6
8. High Pressure Vessel CO3
• Types of high-pressure vessel CO4
• Design of high-pressure vessel CO5
• Construction features, materials for high pressure shell design, vessel CO6
closures
9. Design of Heat Exchanger CO3
• Basic introduction to heat exchanger and selection of heat exchanger, CO4
• Fluid allocation in heat exchanger, CO5
• process design of various components like tube, baffles, shell etc and CO6
• Mechanical design of shell and tube heat exchanger based on TEMA class.
Pressure drop on shell side and tube side in heat exchanger.
10. Supports for Vessels CO3
Selection and design of different types – bracket or lug support, skirt support & CO4
saddle support, design calculations CO5
CO6

C. PRACTICAL AND TERM WORK


Students are Divided in to two groups, one of the groups will go to computer centre, where they
will use excel to carry out design of pressure vessel and its components based on theory class,
whereas second group will go to drawing hall, where they will draw the pressure vessel
components, they designed in computer centre with dimensions. They will be judged based
on both design and drawing, as the title of subject emphasis on both.

D. TEXT BOOKS
1. Umarji, S. B.; Mahajani, V.V. Joshi’s Process Equipment Design; 5th ed.; Trinity
Press: New Delhi, 2016
2. Brownel, L. E.; Young, E. H. Process Equipment Design & Drawing; 2nd ed.;
Wiley Eastern Ltd.: New Delhi, 2005

E. REFERENCE BOOKS
1. Bhattacharya, B.C. Process Equipment Design: Mechanical Aspect; 1st ed.; CBS
Publisher and Distributors Pvt. Ltd.: New Delhi, 2014
2. Bhattacharya, B.C.; Narayanan, C.M. Computer Aided Process Equipment Design;
1st ed.; New Central Book agency (p) ltd.: Kolkata, 1992

F. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand and state the process condition and Interpret Process
CO1 Understanding Flow Diagram
CO2 Analysing
Classify the type of Pressure Vessels along with all its components
Applying
Implementing Codes and Standards to Design of Pressure Vessels and
CO3 Evaluating
its components
Creating
CO4 Critiquing Real life Industrial Problem and Implement solution

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 76


Remembering Methodology for optimum Design
Evaluating Organize a trouble shoot path using various tools for betterment of
CO5
society
Generate a detail design report along with drawing to plan the
CO6
fabrication of pressure vessel

G. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 2 2 2 3 2 3 2.3
PO2 1 1 3 3 3 3 2.3
PO3 1 2 3 3 3 3 2.5
PO4 1 1 2 3 2 3 2
PO5 0 0 2 3 3 3 1.8
PO6 2 2 3 3 3 3 2.7
PO7 2 3 3 3 3 3 2.8
PO8 1 1 2 2 2 3 1.8
PO9 2 2 3 2 3 3 2.5
PO10 1 2 3 2 2 3 2.2
PO11 2 3 3 2 2 3 2.5
PO12 3 3 3 2 3 3 2.8
PSO1 2 3 3 3 2 3 2.67
PSO2 3 3 3 2 3 2 2.67
PSO3 2 3 2 2 2 2 2.17
PSO4 3 3 3 3 3 3 3

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 77


B. TECH. – SEMESTER-VI (CH)
ENERGY TECHNOLOGY (PEC102)
(CORE ELECTIVE-II)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 0 3 3 60 0 0 0 60

A. COURSE OVERVIEW
The motivation of the course is students shall understand current practices of fuel usages and future
prospectus of new and non-conventional energy resources exploration. Moreover, they shall
understand various energy sources including conventional and non-conventional including solar
thermal, geothermal, wind, Ocean, biomass, etc. and also demonstrate knowledge of various energy
technologies and learn present energy scenario and the need for energy conservation.

B. COURSE CONTENT
TOPICS COs
1. An Introduction to Energy Sources CO1
energy sources (conventional & non-conventional), renewable energy resources, CO2
primary & secondary energy sources, energy chain, energy demand, national
energy strategy & plan, energy management, energy audit & conservation
Definitions, Units & Measures
proximate & ultimate analysis, calorific values, rank of coal, coking & caking,
gasification, basis for reporting results of analysis, units & conversion factors
2. Solid Fuels CO1
wood & charcoal, peat, lignite, sub-bituminous & bituminous coals, semi- CO2
anthracite and anthracite coals, cannel & boghead coal, origin of coal, CO3
composition of coal, analysis & properties of coal, problems
3. Processing of Solid Fuels CO1
coal preparation, washability curve, dry & wet washing methods of coal, washer CO2
efficiency, gasification & liquefaction of solid fuels, problems CO7
4. Solar Energy CO1
solar constant, solar radiation & related terms, measurement of solar radiation, CO3
solar energy collectors – flat plate collector, air collector, collectors with porous CO7
absorbers, concentrating collectors, applications & advantages of various
collectors, selective absorber coatings, solar energy storage systems (thermal,
electrical, chemical & mechanical), solar pond, applications of solar energy
5. Wind Energy CO1
basic principles, power in wind, force on blades & turbines, wind energy conversion, CO3
site selection, basic components of wind energy conversion systems (WECS), CO7
classification of WECS, wind energy collectors, applications of wind energy
6. Energy from Biomass CO1
introduction, energy plantation, biomass conversion technologies, photosynthesis, CO3
biogas generation, factors affecting biogas generation, classification of biogas CO4
plants & their comparisons, types of biogas plants (including those used in India), CO7
biogas from plant wastes, community plants & site selection, digester design
considerations, design calculations, methods of maintaining & starting biogas
plants, properties & utilization of biogas, thermal gasification of biomass,
pyrolysis, alternative liquid fuels

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 78


7. Geothermal Energy CO1
Geothermal resources, hydrothermal resources, liquid dominated systems, CO3
geopressured resources, petrothermal systems, magma resources, energy CO7
conservation & comparison with other resources, applications of geothermal energy
8. Energy from Oceans CO1
OTEC, methods (open cycle & close cycle) energy from tides, components of CO5
tidal power plants, operation, methods of utilization of tidal energy, storage, ocean CO7
waves, wave energy conversion devices
9. Fuel Cell CO1
introduction, hydrogen – oxygen fuel cell, ion exchange membrane cell, fossil CO6
fuel cell, molten carbonate cell, advantages & disadvantages, conversion CO7
efficiency, polarization, type of electrodes, applications of fuel cells
10. Hydrogen & Methanol CO1
properties of Hydrogen, production of hydrogen, thermochemical methods, fossil CO6
fuel methods, solar methods, storage & transportation, safety & management CO7
11. Magneto Hydro-Dynamic (MHD) Power Generation CO1
principle, MHD system, open cycle system, closed cycle system, design problems CO6
& developments, advantages, materials for MHD generators, magnetic field & CO7
super conductivity
12. Nuclear Energy CO1
fission, fusion, fuel for nuclear fission reactor (exploration, mining, milling, CO6
concentrating, refining, enrichment, fuel fabrication, fuel use, reprocessing, waste CO7
disposal), storage & transportation, fast & slow neutrons, multiplication factors &
reactor control, uranium enrichment process, nuclear reactor power plant, fast
breeder reactor, boiling water reactor, pressurized heavy & light water reactor

C. TEXT BOOKS
1. Energy Sources 2nd Ed. by G. D. Rai, Khanna Publications, New Delhi
2. Fuels & combustion by Samir Sarkar, Orient Longmans (1974)

D. REFERENCE BOOKS
1. Solar Energy by Sukatame. Tata McGraw Hill, New Delhi
2. Energy Technology by Rao & Parulaker

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand the types of energy sources, forms of energies basic
CO1
definition and terminology.
Explain the origin of solid fuel coal and its characteristic, analysis
CO2 and properties of coal and various coal washing
process.
Comprehension Classify the non-conventional energy resources like solar energy,
CO3
Application WECS and biomass conversion techniques.
Analysis Design the biogas plant and analyses the factors affecting the
CO4
biochemical biomass conversions.
Demonstrate the basic knowledge of renewable energy resources
CO5
like geothermal energy and OTEC systems for electricity generation.
Apply the use of chemical energy sources like hydrogen, fuel cell and
CO6
MHD for satisfy the energy need at various sectors.
Analyse the National energy strategies and policies for energy
CO7
conservation, energy Audit and causes of increase in energy demand.

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 79


F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 CO7 AVG.
PO1 3 2 3 3 3 2 2 2.6
PO2 1 2 3 2 2 2 1 1.9
PO3 1 2 3 1 3 1 3 2
PO4 1 1 2 1 3 1 3 1.7
PO5 2 2 3 2 3 1 3 2.3
PO6 3 1 2 3 3 2 2 2.3
PO7 2 1 2 2 2 3 2 2
PO8 2 2 1 2 2 2 2 1.9
PO9 2 2 2 3 1 2 2 2
PO10 2 2 2 3 1 3 2 2.1
PO11 1 2 1 2 1 2 1 1.4
PO12 3 2 1 3 2 2 3 2.3
PSO1 1 2 3 2 3 2 1 2
PSO2 2 3 3 2 2 3 1 2.3
PSO3 1 2 2 3 2 3 2 2.1
PSO4 3 3 2 2 2 2 3 2.4

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 80


B. TECH. – SEMESTER-VI (CH)
CHEMICAL PROCESS SAFETY (PEC102)
(CORE ELECTIVE-II)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 0 3 3 60 0 0 0 60

A. COURSE OVERVIEW
To inculcate the safety culture among the undergraduate students of chemical engineering. To
teach fundamentals of safety in process industries, current safety practices in industry by using
various tools. To study industrial case studies and standards approved/recommended by CCPS,
NFPA and Directorate of Industrial Safety and Health (DISH).

B. COURSE CONTENT
TOPICS COs
1. Introduction to Process Safety CO1
Define: safety, hazard, risk, accident, incident, likelihood, consequence, loss
prevention, domino effect, first aid, incident rate, lost workdays, occupational
injury and illness, frequency rate, severity rate, fatality rate and fatal accident
rate. Theory of accident causation, nature of accident process.
2. Process Safety Strategies and Case Studies CO1
Concept of Active, Passive, Inherent and Procedural Strategies. Case Studies: CO3
Analysis of mistakes made and lessons to learn from four significant chemical
industry disasters: Flixborough (England), Pasadena (Texas), Seveso (Italy) and
Bhopal (India).
3. Toxicological Studies CO4
Entry routes of toxicants into biological system and appropriate control strategy.
Elimination of toxicants from biological system by various ways, target organ,
acute and chronic toxicity and its toxicological studies, chemical and physical
asphyxiates, TLV-TWA, TLV-STEL and TLV-C, LD 50 and LC 50. Detection
of possible hazard through senses.
4. Industrial Hygiene CO2
Laws and regulations in Indian context and US context, role of OSHA, NIOSH, CO4
ACGIH, EPA, PSM vs. RMP. Safety work permits, Pre-start up and shut down
procedures, emergency planning and response, mock drill, safety audit. Role of
industrial hygienist: Identification using MSDS and NFPA diamond, Evaluation
(quantification methods) and Control methods like Dyke and Enclosures, dilute
and local ventilation, wet methods, good housekeeping and Personal Protective
Equipment (PPE).
5. Fire and Explosion CO1
Basic definitions like fire, combustion, explosion, fire and flash point, auto-ignition CO2
etc., concept of fire triangle, flammability limits (LFL and UFL). Classification CO3
of fires, various extinguishing medium and its selection, mobile and stationary
fire- fighting methods. Explosion types like mechanical explosion, detonation and
deflagration, deflagration to detonation transition (DtoD transition), confined and
unconfined explosion, dust explosions, vapor cloud explosion. BLEVE their
causes and prevention, Numerical on fire & explosion.
6. Source Models CO1
Concept of source models, flow of liquids and vapors through various geometries, CO5

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 81


flashing liquids, liquid pool evaporation, Realistic and worst-case releases.
7. Chemical Reactivity Hazard
Concept of chemical reactive hazard, thermal run-away models and parametric
sensitivity. Use of calorimeters and its types like DSC, ARC, ARRST, APTAC,
VSP2 etc. Characterization of reactive chemical hazard using calorimeters.
Strategies to control reactive hazard, case study of T2 laboratory for reactive
hazard.
8. Introduction to Reliefs and Relief Devices CO1
Need for relief devices, few terminologies like set pressure, max. Allowable working CO2
pressure, operating pressure, accumulation, overpressure, backpressure, blow
down, max. allowable accumulated pressure etc., Location of reliefs, various
relief devices like spring loaded (relief valve, safety valve and safety relief valve),
mechanical, buckling pin and rupture dick. Selection criteria and combination
criteria, effluent system, knock-out drum, cyclone, condenser, quench tank,
scrubber, flare and incinerator. Concept of Basic process control systems (BPCS)
and Safety instrumented system (SIS), sensor location criteria and redundancy of
system, safety interlocks and alarm systems.
9. Hazard Identification and Hazard Analysis CO1
HAZID tools like hazard checklist, job safety assessment, hazard survey CO5
(Calculation of Dow and Mond Index). Hazard Operability (HAZOP case study), CO6
safety reviews, ALARP and Risk Management (RM). HAZAN using probabilistic
methods, revealed and unrevealed failures, common failure modes and reliability
calculations. Use of tools like FTA, ETA and LOPA analysis.
10. Safety Guidelines and Standards CO4
Safety in laboratory of academic institute and R&D houses, safety during loading CO6
and unloading of chemicals, safety while operating positive pressure and negative
pressure systems, safety in tank farm, plant lay outing for safer operations, piping
and electrical color code. Brief discussion on coverage of factories act (1948), Boiler
act (1923), hazardous waste (management and handling) rules (1989), OISD
guidelines and ISO-14000 (EMS), 18000 (OHSAS) and 31000 (RM).

C. TEXT BOOKS
1. Crawl, D. A.; Louvar, J. F. Chemical Process Safety (fundamentals with applications);
3rd Ed.; Prentice Hall International Series, 2011

D. REFERENCE BOOKS
1. Lees, F. P. Loss Prevention in the Process Industries (Hazard Identification, Assessment
and Control); 2nd Ed.; Butterworth-Heinemann, 1980
2. Kletz, T. Learning from Accidents; 3rd Ed.; Gulf Professional Publishing, 2001
3. Stoessel, F. Thermal Safety of Chemical Processes (Risk Assessment and Process
Design); Wiley-VCH, 2008
4. Banerjee, S. Industrial Hazards and Plant Safety; 1st Ed.; CRC Press, 2002

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand the fundamentals of chemical process safety and the
CO1 Understand importance of process safety.
Development Develop an ability to identify and quantify the potential hazards
CO2 Determine
associated with chemical processes.
Analyse
Determining the issues pertaining to occupational safety and ethical
CO3 Evaluate
aspects associated with process safety.
Awareness
CO4 Analyse the major industrial safety related regulations and

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 82


guidelines.
Evaluate the process system through mathematical modelling and
CO5 implementation of the outcomes for the mitigation and prevention of
accidents.
Create awareness among students for the research and innovation
CO6
in the field of process safety for sustainable future

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 2.5 2.5 2.5 2.8
PO2 3 3 2.5 2.5 2.5 2.5 2.7
PO3 2.5 2.5 2.5 2.5 2.5 2.5 2.5
PO4 2.5 2.5 2.5 3 2.5 2.5 2.6
PO5 2.5 2.5 2.5 2.5 2.5 2.5 2.5
PO6 3 3 2.5 2.5 2.5 2.5 2.7
PO7 3 3 3 2.5 2.5 2.5 2.8
PO8 3 3 3 2.5 2.5 2.5 2.8
PO9 2.5 2.5 2.5 2.5 2.5 2.5 2.5
PO10 2.5 3 2.5 2.5 2.5 2.5 2.6
PO11 2.5 2.5 2.5 2.5 2.5 2.5 2.5
PO12 3 3 3 3 3 2.5 2.9
PSO1 2 3 3 3 2 2 2.5
PSO2 2 3 3 3 2 2 2.5
PSO3 2 3 3 3 2 2 2.5
PSO4 2 3 3 3 2 2 2.5

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 83


B. TECH. – SEMESTER-VI (CH)
OPTIMIZATION TECHNIQUES (PEC102)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 0 3 3 60 0 0 0 60

A. COURSE OVERVIEW
Motivation: Study, Understand and Utilize the appropriate mathematical models and tools to
optimize and solve the process and problems associated with any field and industry

B. COURSE CONTENT
TOPICS COs
1. Introduction to Operational Research CO1
• Introduction, CO3
• Engineering Application, CO4
• Methods of Operation Research,
• Formulation,
• Graphical method of Solution
2. Linear Programming CO2
• Simplex method CO3
• Degeneracy CO4
• Big-M method
• Revised Simplex method
3. Transportation Model CO3
• North-West Corner rule, CO4
• Row and Column Minima method, CO5
• Least-cost method,
• Vogel’s approximation method,
• Degeneracy in transportation problem,
• stepping stone method,
• modified distribution method,
• unbalanced supply and demand,
• profit maximization problem,
• trans-shipment problems
4. Assignment Model CO2
• Hungarian method for solution CO3
• Variation of the assignment problem - non-square matrix, restriction on CO4
assignments.
• Maximization problem
• Travelling salesman problem
• Travelling salesman problem (shortest cyclic route models)
5. Scheduling Optimization and Related Models on Sequencing CO5
• Batch Scheduling CO6
• Formulation of sequencing models and its applications.
• Introduction to Gantt Chart and its Application to Different types of
Transfer policies.
6. Advanced topics in Linear Programming CO2
• Duality in Linear Programming CO3

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 84


• Primal to Dual conversion CO4
• Duality Theorem and Dual Simplex method
7. Dynamic programming CO4
• Bellman’s principle of optimality, CO5
• Examples on the application of routing problem, inventory problem, CO6
marketing problem.
8. Non-Linear Programming CO1
• Elimination Methods — Unrestricted Search, Exhaustive Search, CO2
Dichotomous search, Fibonacci method, Golden Section Method, CO3
• Kuhn tucker condition CO4

C. TEXT BOOKS
1. Gupta P., Hira D.S., “Operation Research”, S. Chand & Company Ltd
2. Rao S.S., “Engineering Optimization: Theory and Practice”, Willey Publication
3. Vohra N D, Quantitative Techniques in Management, Tata McGraw Hill, New Delhi

D. REFERENCE BOOKS
1. Sharma S D & Sharma H, Operations Research: Theory, methods & applications
2. K. Nath R. Nath Arora J.S., “Introduction to Optimum Design”, Elsevier Academic
Press
3. Hiller & Libermann, Introduction to Operations Research, Tata McGraw Hill
4. Hamdy A. Taha, “Operation Research”, Pearson Education
5. Operation Research – V. K. Kapoor, S. Chand Publication

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Define the type of the problem in terms of Linear programming problem
CO1
or Non-linear programming problem
Define Describe the formulation of the problem into mathematical
CO2 Describe approach/model
Application
Apply the types of numerical/mathematical methods to be used in
CO3 Solution
industry to have optimal solution
Development
CO4 Use Solve the type of the problem using the appropriate method
CO5 Develop a skill to deal with type of problem to get best possible result
CO6 Use the mathematical tool to solve the trickiest problem

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 3 2 2 2.7
PO2 3 3 3 3 2 2 2.7
PO3 3 3 2 2 2 2 2.3
PO4 2 2 2 2 1 2 1.8
PO5 2 2 2 2 3 3 2.3
PO6 2 2 2 2 1 1 1.7
PO7 2 2 1 1 1 1 1.3
PO8 2 2 1 1 1 1 1.3
PO9 2 2 1 1 1 1 1.3
PO10 2 2 1 1 1 1 1.3
PO11 2 2 1 1 1 1 1.3
PO12 2 1 1 1 1 1 1.2

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 85


PSO1 3 3 3 2 3 3 2.8
PSO2 3 3 3 2 3 3 2.8
PSO3 3 3 3 2 2 2 2.5
PSO4 3 3 3 3 3 2 2.8

BACK

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 86


SEMESTER-VII
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
PCC116 Design and
2 0 4 60 40 25 25 150 4
Simulation Lab
PCC113 Process Technology
3 1 0 60 40 0 0 100 4
and Economics
PCC102 Transport Phenomena 3 0 3 60 40 25 25 150 4.5
ESC107 Material Science 3 0 0 40 0 0 0 40 3
PEC104 Core Elective-III (1),
3 0 0 40 0 0 0 40 3
(2)
OEC103 Open Elective-III 3 0 0 40 0 0 0 40 3
TOTAL 17 1 7 300 120 50 50 520 21.5

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 87


B. TECH. – SEMESTER-VII (CH)
DESIGN AND SIMULATION LAB (PCC116)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
2 0 4 6 4 60 40 25 25 150

A. COURSE OVERVIEW
Motivation: Use modern softwares to get an insight on various chemical processes and unit
operations, analyze and evaluate them qualitatively through modeling and simulations.
Objectives: Process Simulation – Operating Aspen Plus Basic unit operations; Developing
flowsheets and performing simulations; Parameter estimation and sensitivity study. CFD
Simulation – Operating ANSYS FLUENT; Developing geometry and perform meshing;
Performing simulations and analyzing the transport behavior of different systems

B. COURSE CONTENT
TOPICS COs
1. Process Simulation – Aspen Plus CO1
• Introduction to Aspen Plus, Setting up the model CO2
• Steady state and Unsteady state Simulation CO3
• Concept of Flowsheeting, sequential modular and EO approach CO6
• Parameter estimation of experimental data, Sensitivity study
2. CFD Simulations CO4
• Introduction to the concept of CFD CO5
• Introduction to ANSYS Workbench, FLUENT Environment CO6
• Developing geometry for the Simulations
• Meshing the geometry
• Setting up of model for simulations – boundary and initial conditions
• Solver strategies
3. Professional Ethics in Design and Simulation Lab
• Computer Ethics and Computer supported co-operative world, value sensitive
design
• Human welfare, confidentiality, data safety and management, trust,
accountability

C. PRACTICAL AND TERM WORK


Aspen Plus based simulations for basic unit operations such as – mixing tanks, distillation
columns, reactors, absorption columns, heat exchangers and process flowsheets
CFD simulations using FLUENT for different geometries – pipe flow, venturi/orifice meter,
annular flow, annular flow with heat transfer, CSTR

D. TEXT BOOKS
1. Aspen Plus Manuals
2. ANSYS FLUENT Manuals

E. REFERENCE BOOKS
1. Chemical Process Design and Simulation - Aspen Plus and Aspen HYSYS Applications
Juma Haydary, AIChE / John Wiley & sons
2. ASPEN PLUS - Chemical Engineering Applications, Kamal I.M. Al-Malah, John

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 88


Wiley & sons
3. Computational flow modeling for Chemical Reactor Engineering, V. V. Ranade,
Academic Press

F. COURSE OUTCOMES
COs SKILLS STATEMENT
Develop process flowsheet and understand to perform simulation by
CO1
using ASPEN PLUS
Solve various chemical engineering problems with unit operations
CO2
Understand such as mixing, mass transfer, heat transfer, reactions
CO3 Application Apply Sequential modular and EO approach to solve problems
Analysis Understand the concept of CFD, create geometry, mesh and set
CO4
Evaluate initial and boundary conditions using ANSYS FLUENT
Create Analyse the transport behavior in different geometries such as pipe
CO5
flow, Venturi/orifice meters, annular flow, heat transfer
Analyse the technical feasibility of Industrial scale chemical
CO6
manufacturing facility and Evaluate performance

G. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 3 3 3 3
PO2 3 3 3 3 3 3 3
PO3 3 3 3 3 3 3 3
PO4 3 3 3 3 3 3 3
PO5 3 3 3 3 3 3 3
PO6 3 3 3 3 3 3 3
PO7 3 3 3 3 2 2 2.7
PO8 3 3 3 3 3 3 3
PO9 3 3 3 3 2 2 2.7
PO10 3 3 3 3 2 2 2.7
PO11 3 3 3 3 3 3 3
PO12 3 3 3 3 2 2 2.7
PSO1 3 3 3 3 2 2 2.7
PSO2 3 3 3 3 2 2 2.7
PSO3 3 3 3 3 2 2 2.7
PSO4 3 3 3 2 2 3 2.7

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 89


B. TECH. – SEMESTER-VII (CH)
PROCESS TECHNOLOGY AND ECONOMICS (PCC113)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 1 0 4 4 60 40 0 0 100

A. COURSE OVERVIEW
Motivation: To equip the students with fundamental concepts and principles of manufacturing
of various industrially important chemical products through the economics.
Course Objectives:
• To familiarize students with manufacturing aspects of industrially relevant chemicals.
• Economics is introduced to fill the gap between technical knowledge & commercial
sustainability of any plant by imparting brief description of any plant from top to bottom
approach.

B. COURSE CONTENT
TOPICS COs
1. Introduction to Process Technology CO3
Description, raw material and energy sources and consumptions, operating CO6
conditions, catalysts, basic block diagram and simplified process flow diagram
for manufacture of inorganic chemicals, such as: inorganic acids, chlor-alkali,
ammonia, fertilizers, etc.
2. Introduction to Petrochemicals CO3
Description, raw material and energy sources and consumptions, operating CO6
conditions, catalysts, basic block diagram and simplified process flow diagram
for manufacture of Petrochemicals: C1, C2, C3, C4, etc., benzene, toluene, xylene
and other petrochemicals from these basic building blocks.
3. Industrial Fuels and Utilities CO3
Industrially relevant fuels, Common utilities such as electricity, cooling water, CO6
steam, hot oil, refrigeration and chilled water.
4. Cost Estimation CO1
Factors involved in project cost estimation, total capital investment, fixed capital CO2
investment, fixed capital & working capital, type & methods for estimation of CO4
total cost, investment, estimation of cost of equipment & cost of production. CO5
5. Estimation of Total Product Costs CO1
Factors involved in total cost of production, factors affecting investment & CO2
production cost, Direct Production cost, Plant overhead cost, Fixed Charges CO4
& General Expenses. CO5
6. Analysis of Projects CO1
Analysis of working results project: Balance sheets, Project financing, concept CO2
of interest, time value of money, depreciation. Profitability Analysis of Projects. CO4
Ethics to develop the moral conditions of professionalism. CO5

C. TEXT BOOKS
1. Shreve’s Chemical Process Industries, George T. Austin, McGraw-Hill International
Editions Series, 1984
2. Dryden’s Outlines of Chemical Technology, M. Gopala Rao, Marshall Sittig, East
West Press, 1997

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 90


3. Chemical Project Economics, Mahajani V. V. and Mokashi S M., MacMillan India
Ltd. 2005

D. REFERENCE BOOKS
1. Chemical Process Technology, Moulijn, M. and van Dippen, Wiley, 2013.

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand the basic economic concepts and apply them in the project
CO1
works undertaken.
Develop an ability to carry out the primary techno-economic feasibility
CO2 of project and to identify various process conditions associated with
chemical processes and operations.
CO3 Understand Explaining the production processes of various chemical products.
Development Analyse the project cost including capital investment, product cost,
CO4 Explanation time value, total project cost and the major engineering problems
Analysis associated with production units of various chemical industries.
Application Application of basics of depreciation, profitability and project finance
CO5 Awareness and process drawing tools for process flow diagrams.
Create awareness among students for the research and innovation in
CO6 the field of process technology and economics for environmental issues
and sustainability.

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 2 3 3 2.8
PO2 3 3 3 2 3 3 2.8
PO3 3 3 3 2 3 3 2.8
PO4 3 3 3 2 3 3 2.8
PO5 3 2 3 2 2 3 2.5
PO6 3 2 2 3 3 3 2.7
PO7 3 3 2 2 3 2 2.5
PO8 3 3 3 2 3 2 2.7
PO9 3 2 3 3 2 2 2.5
PO10 3 3 3 3 2 2 2.7
PO11 3 3 3 2 3 2 2.7
PO12 3 3 2 3 3 2 2.7
PSO1 2 3 3 3 2 2 2.5
PSO2 2 3 3 3 2 2 2.5
PSO3 2 3 3 3 2 2 2.5
PSO4 2 3 3 3 2 2 2.5

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 91


B. TECH. – SEMESTER-VII (CH)
TRANSPORT PHENOMENA (PEC102)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 3 6 4.5 60 40 25 25 150

A. COURSE OVERVIEW
The objective of this course is to make students aware and to teach them how to deal with the
movement of different physical quantities such as momentum, energy and mass in any chemical or
mechanical process and combination of the basic principles (conservation laws) and laws of various
types of transport.

B. COURSE CONTENT
TOPICS COs
1. Review of momentum, energy & mass transport by molecular motion, Vector CO1
and Tensor Analysis: Basic concepts, Euler/ Lagrangian viewpoint, laminar and
turbulent flows, boundary layers, stress tensor
2. Momentum Transport: shell momentum balances, velocity profiles in cases like CO2,
adjacent flow of two liquids. Energy Transport: shell energy balances, CO3
temperature profiles, heat conduction with an electrical heat source, heat CO4
conduction viscous heat source & heat conduction chemical heat source. Mass CO6
Transport: concentration distribution in solids & laminar flow, shell mass
balances, diffusion with heterogeneous chemical reaction, diffusion in falling
liquid film
3. Momentum Transport: equation of change for isothermal system, equation of CO2,
continuity & motion in rectangular, cylindrical & spherical co-ordinates. Energy CO3
Transport: non-isothermal systems, equation of energy of motion for forced & CO4
free convection in non-isothermal flow. Mass Transport: equation of continuity CO5
for binary mixtures, equation of change for multi-component systems, mass flux CO6
in terms of transport properties, use of equation of change
4. Momentum Transport: unsteady state viscous flow, two-dimensional viscous CO2
flow, boundary layer momentum transport. Energy Transport: heat conduction in CO3
viscous flow, boundary layer energy transport. Mass Transport: unsteady CO6
diffusion, diffusion in viscous flow, two-dimensional diffusion in solids, boundary
layer theory
5. Momentum Transport: time smoothing of equation of change for incompressible CO2
fluid & review of logarithmic law of viscosity. Energy Transport: temperature CO3
fluctuations & time smoothing of temperature & energy equation, semi-empirical CO4
equations for turbulent energy flux. Mass Transport: time smoothing of CO5
equation of change, turbulent concentration profiles CO6
6. Momentum transport: friction factors for flow in tubes, flow rate & pressure CO3
drop relations, friction factor for packed beds. Energy Transport: non- CO4
isothermal system, heat transfer coefficients, dimensionless correlations for CO6
forced & free convection in tubes & around submerged objects, heat transfer
coefficient for forced convection through packed bed. Mass Transport: mass
transport coefficient, correlations for binary systems in one phase & at low mass
transfer rates, definition & correlation for binary mass transfer coefficients in two
phases at low mass transfer rates, transfer coefficients for high mass transfer
rates, boundary layer theory

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 92


7. Microscopic mass balance & mechanical energy balances, estimation of CO3
friction losses, macroscopic energy balance in non-isothermal systems, use of CO4
balances to solve steady state & unsteady state problems. Ethical practices for CO6
designing of equipment’s using change equations

C. TEXT BOOKS
1. Bird R B; Stewart W E; Lightfoot F W,, Transport Phenomena, John Wiley & Sons
2. Gupta S K, Momentum Transfer Operations, Tata McGraw Hill Corp

D. REFERENCE BOOKS
1. Laddha G S; Degaleesan T E , Transport Phenomenon in Liquid Extraction , McGraw
Hill Publishing
2. Sherwood T K; Pigford R L, Absorption & Extraction, McGraw Hill Publishing
3. Holland D D, Multi-component Distillation, Prentice Hall, India

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Understand the system and analyse the same with the help of science
CO1
and engineering fundamentals
CO2 Understand Design momentum, heat and mass transfer systems
CO3 Design
Modify and trouble shoot the process equipment for better efficiency
Troubleshoot
CO4 Build a bridge between theoretical and practical concepts
Application
Analysis Utilize the process knowledge and existing simulation tools while
CO5
Develop analysing process using commercial solvers
Develop analytical thinking to overcome simple system engineering
CO6
related problems

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 3 3 3 3
PO2 3 3 3 3 3 3 3
PO3 3 3 3 3 3 3 3
PO4 3 3 2 3 3 2 2.7
PO5 2 3 3 2 3 2 2.5
PO6 2 3 3 2 3 2 2.5
PO7 2 3 3 2 3 2 2.5
PO8 3 2 2 2 2 2 2.2
PO9 2 2 2 2 2 2 2
PO10 1 1 2 2 2 1 1.5
PO11 2 2 2 2 2 2 2
PO12 3 3 3 3 3 2 2.8
PSO1 3 2 3 3 3 3 2.8
PSO2 3 3 2 3 3 3 2.8
PSO3 3 3 3 2 3 3 2.8
PSO4 3 3 2 2 3 3 2.7

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 93


B. TECH. – SEMESTER-VII (CH)
MATERIAL SCIENCE (ESC107)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 0 3 3 40 0 0 0 40

A. COURSE OVERVIEW
Motivation: Learning different classes of materials, their properties, processing and performance
characteristics relevant to chemical engineering. Objective of course is to learn different classes
of materials relevant to chemical industries, understand the performance characteristics of
materials, development of knowledge pertaining to the application of materials based upon
processing, evaluate the possible failures due to stress and corrosion and analyze and
understand experimental characterization techniques.

B. COURSE CONTENT
TOPICS COs
1. Basic concepts of materials and material science CO1
Introduction to materials, bonding between atoms: metallic bonding, ionic bonding,
covalent bonding, Van der Waals bond, thermal expansion, elastic modulus and
melting point of materials, Role of materials selection in design, structure-property-
processing-performance relationships. Mechanical properties: Isotropy and
anisotropy, Stress and strain relation, Hooke’s law, Modulus of material,
Poisson’s ratio.
2. Fundamental Properties and failures CO3
Miller indices of directions and planes, packing of atoms inside solids, close- CO5
packed structures, structure of ceramics, ionic solids, glass and polymers, density
of various materials. Imperfections in solids: vacancies, equilibrium concentration
of vacancies, interstitial and substitutional impurities in solids, dislocations, types
and characteristics of dislocations, interfacial defects, stacking faults. Yield
strength, tensile strength and ductility of materials: stress strain behavior of
metals, ceramics and polymers, tensile test. Plastic deformation, necking, creep
behavior and fatigue and related knowledge of safety, and welfare of coworkers
due to failure.
3. Ferrous materials CO1
Ferrous metals, cast iron and its types, Steel, stainless steel, classification of CO3
steel, manufacturing process of steel. Alloy steels and its classification,
Advantages and Disadvantages of Alloy Steel, Purpose of Alloying, effect of
alloying elements on mechanical properties of steel, their safety and health
impacts.
4. Materials CO2
Semi-crystalline materials, their classification, structure and configuration of
ceramics, polymers, copolymers, liquid crystals and amphiphiles. Non-
crystalline/amorphous materials: Silicates, glass transition temperature,
viscoelasticity. Polymer nano-composite materials: Nanocomposites, role of
reinforcement-matrix interface strength on composite behavior. Biomaterials,
material related to catalyst such as zeolites, silica etc. and other selected materials
5. Corrosion, Degradation and Recycling CO5
Mechanism of corrosion, dry & wet corrosion, other forms of corrosion, Passivity, CO6
factors influencing corrosion, atmospheric corrosion. Control & prevention of

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 94


corrosion – cathodic & anodic control, inhibitors & other protective measures.
Protective coatings, metallic coating & metal cladding, physico-chemical principles
involved, chemical conversion coating, organic coating, enamels, ceramic
protective materials.
6. Experimental techniques CO6
Introduction to experimental techniques: XRD, NMR, PSA, etc. for material
characterization highlighting links between molecular structure and
macroscopic properties

C. TEXT BOOKS
1. Hajra Chaudhary, S.K. Material science and Processes; Indian Book Distributing Co.,
2009
2. Raghavan, V. Materials Science and Engineering, fifth edition, Prentice Hall of India
Private Limited: New Delhi, 2011

D. REFERENCE BOOKS
1. S. Upadhyaya and A. Upadhyaya, Material Science and Engineering, Anshan
Publications, 2007
2. Vijaya, M.S.; Rangarajan, G. Materials Science; Tata McGraw-Hill Education, 2004
3. Jastrzebski, Z.D. The Nature and Properties of Engineering Materials; (ed 2), Wiley &
Sons: New York, 1976
4. Van Vlack, L.H. Elements of Material Science and Engineering; Thomas Press: India,
1998
5. William, D.; Callister, Jr. Materials Science and Engineering – An introduction; sixth
edition, John Wiley & Sons, Inc., 2004
6. B. S. Mitchell An Introduction to Materials Engineering and Science for Chemical and
materials Engineers, John Wiley & Sons, 2004

E. COURSE OUTCOMES
COs SKILLS STATEMENT
CO1 Develop basic concepts of materials.
CO2 Comprehensive Classify various engineering materials.
CO3 Remembering
Understanding of performance characteristics of materials.
Understand
Application of materials in industries as per the safety, health and
CO4 Application
welfare of co-workers.
Evaluate
CO5 Analysis Evaluation of possible failures due to stress and corrosion.
CO6 Analyse various experimental characterization techniques.

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 2 3 3 3 2.8
PO2 3 2 3 3 3 3 2.8
PO3 3 3 3 3 3 2 2.8
PO4 2 2 3 2 3 3 2.5
PO5 2 2 2 3 3 3 2.5
PO6 2 2 3 3 3 2 2.5
PO7 2 2 2 3 3 3 2.5
PO8 2 2 3 3 3 2 2.5
PO9 2 2 3 2 3 3 2.5
PO10 2 2 3 3 3 3 2.7

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 95


PO11 2 2 2 3 3 3 2.5
PO12 3 3 3 3 3 2 2.8
PSO1 3 3 3 3 2 3 2.8
PSO2 3 3 3 3 3 2 2.8
PSO3 2 2 3 3 3 3 2.7
PSO4 2 3 3 3 3 3 2.8

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 96


B. TECH. – SEMESTER-VII (CH)
CHEMICAL PROCESS OPTIMIZATION (PEC104)
CORE ELECTIVE-III

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 0 3 3 40 0 0 0 40

A. COURSE OVERVIEW
Motivation: Examine the different optimization techniques associated with the field of Chemical
engineering and other fields
Objectives: Formulate the objective functions for constrained and unconstrained optimization
problems; Implement different optimization techniques; solve problems using non-traditional
techniques; use of different optimization techniques for integrated planning, scheduling and
control in the process industries

B. COURSE CONTENT
TOPICS COs
1. Introduction CO1
• Process optimization CO2
• Nature and Organization of Optimization Problems
• Formulation of various process optimization problems and their
classification
• Formulation of the Objective Function
2. Optimization Theory and Methods CO1
• NLP Problem Statement CO2
• Convexity and Its Applications CO3
• Optimality conditions for a single-variable and multi-variable function
• Structure of a single-variable and multi-variable optimization problems
with and without constraints (qualitative treatment)
3. Optimization programming with applications CO2
• Linear programming (LP) & Nonlinear programming (NLP) with CO3
applications CO5
• Mixed-Integer Programming- MILP & MINLP
• Global Optimization for Problems with Continuous and Discrete Variables
4. Chemical engineering optimization problems CO4
• Part 1: Pipe diameter, Optimization of a Multi-Effect Evaporator, CO5
Optimal Shell-and-Tube Heat Exchanger Design, Reflux ratio of CO6
distillation column.
• Part 2: Thermal cracker, Alkylation reactor, Optimal Design of an
Ammonia Reactor.
• Integrated Planning, Scheduling and Control in the Process Industries

C. TEXT BOOKS
1. Edgar, T. F., Himmelblau, D. M. and Lasdon, L.S. Optimization of Chemical
Processes, McGraw-Hill,2001
2. Babu, B.V., Process Plant Simulation, Oxford University Press ,2004

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 97


D. REFERENCE BOOKS
1. Kalyanmoy, D., Optimization for Engineering Design, Prentice Hall,1998
2. Reklaitis, G. V., Ravindran, A., and Ragsdell, K. M., Engineering Optimization -
Methods and Applications, John Wiley,1983
3. Reklaitis, G. V., Ravindran, A., and Ragsdell, K. M., Engineering Optimization -
Methods and Applications, John Wiley,1983
4. Box, G. E. P., Hunter, W. G., Hunter, J. S., Statistics for Experimenters – An
Introduction to Design, Data Analysis, and Model Building, John Wiley,1978

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Describe the basic concept of optimization techniques in the chemical
CO1
process industry.
Identify the different solving methods with containing the different
CO2 Understand Linear Programing Models (LP Models & NLP Models)
Synthesis Apply the basic knowledge on real-time problems related to chemical
CO3 Applying
engineering or other fields of engineering.
Evaluating
Evaluate the economical aspect of the chemical process or design
CO4 Creating
engineering
Planning
Applying Generating reports for selection, Design and troubleshooting of
CO5
Industrial optimization.
Integrated Planning, Scheduling and Control in the Process
CO6
Industries by considering environmental & safety constraints.

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 3 3 3 3
PO2 3 3 3 3 3 3 3
PO3 3 3 3 2 3 3 2.8
PO4 3 3 3 2 2 2 2.5
PO5 2 3 3 2 3 2 2.5
PO6 2 2 2 3 3 3 2.5
PO7 2 3 3 3 3 3 2.8
PO8 3 2 2 2 3 3 2.5
PO9 2 2 2 2 3 3 2.3
PO10 2 2 2 2 3 3 2.3
PO11 3 3 2 3 3 3 2.8
PO12 3 3 3 3 3 3 3
PSO1 3 2 3 2 3 3 2.7
PSO2 2 3 2 3 2 3 2.5
PSO3 3 3 3 2 3 2 2.7
PSO4 2 2 3 3 3 3 2.7

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 98


B. TECH. – SEMESTER-VII (CH)
ADVANCE PROCESS CONTROL (PEC104)
CORE ELECTIVE-III

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
3 0 0 3 3 40 0 0 0 40

A. COURSE OVERVIEW
Expose students to the advanced control methods used in industries and research. Students will
be able to analyse, design and tune the advanced controller used for solving the critical problems
in the industries related to safety, economy and optimization.

B. COURSE CONTENT
TOPICS COs
1. Review of Single Input Single Output (SISO) Control. CO3
2. Linearization of Mechanistic models . Introduction to z-transform. Development CO1
of grey-box models CO3
3. Development of output error models. Introduction to stochastic processes CO2
Development of ARX and ARMAX models. Model structure selection and CO3
issues in model development
4. Stability analysis of discrete time systems. Lyapunov Functions and interaction CO3
analysis. Multi-loop control. Multivariable-decoupling control CO4
Soft sensing and state estimation
5. Development of Luenberger observer. Introduction to Kalman filtering CO2
CO5
6. State feedback control design. Introduction to Linear Quadratic Gaussian control CO4
(LQG). Design of Linear Quadratic Gaussian regulator and controller. Design of CO5
DMC and Model Predictive control CO6

C. TEXT BOOKS
1. B. Wayne Bequette, Process Control Modeling, Design & Simulation, PHI
2. L.Ljung, "System Identification - Theory for the User", Prentice Hall, 1987
3. E. Camacho and C. Bordons, "Model Predictive Control in the Process Industry", 1995

D. REFERENCE BOOKS
1. Process Dynamics and Control, D. E. Seborg, T. F. Edgar, D.A. Mellichamp, Wiley,
2003
2. Control System Design, by Graham C. Goodwin, Stefan F. Graebe, Mario E.
Salgado, Prentice Hall, 2000
3. Franklin, G. F., Powell, J. D., and M. L. Workman, Digital Control Systems, Addison
Wesley, 1990
4. Astrom, K. J., and B. Wittenmark, Computer Controlled Systems, Prentice Hall
India (1994)

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 99


E. COURSE OUTCOMES
COs SKILLS STATEMENT
CO1 Analyze and design advanced control systems.
CO2 Understand Understand industrial applications of control theory.
Synthesis Apply the knowledge of process control to design the control
CO3
Applying algorithms and its tuning.
Evaluating Evaluate and judge the comparative performance of the different
CO4 Creating control strategies.
CO5 Planning Design of digital control systems.
Applying Optimization and safety evaluation of the overall process control
CO6
system of an industry.

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 3 3 3 3
PO2 3 3 3 3 3 3 3
PO3 3 3 3 3 3 3 3
PO4 3 3 2 3 3 2 2.7
PO5 2 3 3 2 3 2 2.5
PO6 2 3 3 2 3 2 2.5
PO7 2 3 3 2 3 2 2.5
PO8 3 2 2 2 2 2 2.2
PO9 2 2 2 2 2 2 2
PO10 1 1 2 2 2 1 1.5
PO11 3 3 3 3 3 3 3
PO12 3 3 3 3 3 3 3
PSO1 3 2 3 3 2 3 2.7
PSO2 3 3 2 3 3 3 2.8
PSO3 3 3 3 2 2 3 2.7
PSO4 3 2 3 2 3 3 2.7

BACK

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 100


SEMESTER-VIII
Teaching
Subject Scheme Exam Scheme (Marks)
Subject Name Credit
Code (hr/w)
L T P Th. S P TW Total
HS104 Universal Human
2 1 0 40 0 0 0 40 3
Value-II
PEC103 Core Elective-IV 2 0 2 40 0 25 25 90 3
PROJ Industrial Internship 0 3 12 0 0 150 100 250 9
PROJ Working Project 1 0 4 0 0 50 50 100 3
TOTAL 5 4 18 80 0 175 225 480 18

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 101


B. TECH. – SEMESTER-VIII (CH)
UNIVERSAL HUMAN VALUES-II (PEC104)

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
2 1 0 3 3 40 0 0 0 40

A. COURSE OVERVIEW
Motivation: Development of holistic perspective based on self-exploration. Discussion about individual
role in the society and nature.
Course objective is to understand the general perspective based on self-exploration about themselves,
family and nature. The harmony in the human being, family, society and nature. Strengths of self-
reflection. Importance of commitment and courage to act

B. COURSE CONTENT
TOPICS COs
1. Course Introduction - Need, Basic Guidelines, Content and Process for Value
Education
Purpose and motivation for the course, recapitulation from Universal Human Values-I.
Self-Exploration–what is it? - Its content and process; ‘Natural Acceptance’ and
Experiential Validation- as the process for self-exploration. Continuous Happiness and
Prosperity- A look at basic Human Aspirations. Right understanding, Relationship and
Physical Facility- the basic requirements for fulfilment of aspirations of every human
being with their correct priority. Understanding Happiness and Prosperity correctly- A
critical appraisal of the current scenario. Method to fulfil the above human aspirations:
understanding and living in harmony at various levels.
2. Understanding Harmony in the Human Being - Harmony in Myself
Understanding human being as a co-existence of the sentient ‘I’ and the material ‘Body’.
Understanding the needs of Self (‘I’) and ‘Body’ - happiness and physical facility.
Understanding the Body as an instrument of ‘I’ (I being the doer, seer and enjoyer).
Understanding the characteristics and activities of ‘I’ and harmony in ‘I’. Understanding
the harmony of I with the Body: Sanyam and Health; correct appraisal of Physical needs,
meaning of Prosperity in detail. Programs to ensure Sanyam and Health.
3. Understanding Harmony in the Family and Society- Harmony in Human-Human
Relationship
Understanding values in human-human relationship; meaning of Justice (nine universal
values in relationships) and program for its fulfilment to ensure mutual happiness; Trust
and Respect as the foundational values of relationship. Understanding the meaning of
Trust; Difference between intention and competence. Understanding the meaning of
Respect, Difference between respect and differentiation; the other salient values in
relationship. Understanding the harmony in the society (society being an extension of
family): Resolution, Prosperity, fearlessness (trust) and co-existence as comprehensive
Human Goals. Visualizing a universal harmonious order in society- Undivided Society,
Universal Order- from family to world family.
4. Understanding Harmony in the Nature and Existence - Whole existence as
Coexistence
Understanding the harmony in the Nature. Interconnectedness and mutual fulfilment
among the four orders of nature- recyclability and self- regulation in nature.
Understanding Existence as Co-existence of mutually interacting units in all-pervasive
space. Holistic perception of harmony at all levels of existence

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 102


5. Implications of the above Holistic Understanding of Harmony on Professional
Ethics
Natural acceptance of human values. Definitiveness of Ethical Human Conduct. Basis
for Humanistic Education, Humanistic Constitution and Humanistic Universal Order.
Competence in professional ethics: a. Ability to utilize the professional competence for
augmenting universal human order b. Ability to identify the scope and characteristics of
people- friendly and eco-friendly production systems, c. Ability to identify and develop
appropriate technologies and management patterns for above production systems.
Case studies of typical holistic technologies, management models and production
systems. Strategy for transition from the present state to Universal Human Order: a. At
the level of individual: as socially and ecologically responsible engineers, technologists
and managers b. At the level of society: as mutually enriching institutions and
organizations

C. TEXT BOOKS
1. Human Values and Professional Ethics by R R Gaur, R Sangal, G P Bagaria, Excel Books, New
Delhi, 2010

D. REFERENCE BOOKS
1. Jeevan Vidya: Ek Parichaya, A Nagaraj, Jeevan Vidya Prakashan, Amarkantak, 1999
2. Human Values, A.N. Tripathi, New Age Intl. Publishers, New Delhi, 2004
3. The Story of Stuff (Book)
4. The Story of My Experiments with Truth - by Mohandas Karamchand Gandhi
5. Small is Beautiful - E. F Schumacher
6. Slow is Beautiful - Cecile Andrews
7. Economy of Permanence - J C Kumarappa
8. Bharat Mein Angreji Raj - PanditSunderlal
9. Rediscovering India - by Dharampal
10. Hind Swaraj or Indian Home Rule - by Mohandas K. Gandhi
11. India Wins Freedom - Maulana Abdul Kalam Azad
12. Vivekananda - Romain Rolland (English); Gandhi - Romain Rolland (English)

E. COURSE OUTCOMES
COs SKILLS STATEMENT
Development of a holistic perspective based on self-exploration about
CO1 Development
human being and surrounding.
Understanding
Understanding of the harmony in the human being, family, society and
CO2 Comprehensive nature/existence.
CO3 Creation Defining and strengthening of self-reflection.
CO4 Analysing Development of commitment and courage to act.
CO5 Problem Analysing issues/problems and their role in society.
CO6 solving Improving human values and humanities.

F. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 3 3 3 3 3 3 3
PO2 2 3 3 2 3 3 2.7
PO3 3 3 2 3 3 3 2.8
PO4 2 3 3 3 3 3 2.8
PO5 3 3 3 2 3 3 2.8

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 103


PO6 3 3 3 3 3 3 3
PO7 3 3 2 3 3 3 2.8
PO8 3 3 3 3 3 3 3
PO9 3 3 2 2 3 3 2.7
PO10 3 3 3 3 3 3 3
PO11 2 2 3 3 3 3 2.7
PO12 3 3 3 3 3 3 3
PSO1 3 3 3 3 3 3 3
PSO2 3 3 2 3 3 3 2.8
PSO3 2 3 2 3 3 3 2.7
PSO4 3 2 3 3 3 3 2.8

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 104


B. TECH. – SEMESTER-VIII (CH)
COMPUTER AIDED DESIGN IN CHEMICAL ENGINEERING (PEC104)
CORE ELECTIVE-IV

Teaching Scheme (Hours/Week) Examination Scheme


Credits
L T P Total Ext S TW P Total
2 0 2 4 3 40 0 25 25 90

A. COURSE OVERVIEW
Development of customized solution of chemical engineering design / optimization problems using
various CAD tools. Use of computer for solving complex problems reduces human error, improves
efficiency, removes redundancy and cost-effective optimal solutions can be obtained
Objectives:
To study applications of computer aided tools in design, optimization and control of chemical engineering
systems. Emphasis is to develop CAD modules using MATLAB for solving various design problems,
dynamic problems and optimization problems in chemical engineering

B. COURSE CONTENT
TOPICS COs
1. Introduction to Computer Aided Design CO1
Motivation for using CAD in chemical engineering, Preliminaries of CAD, Tools of CO3
CAD, Onion model of process design
2. Computer aided design of process equipment CO1
Computer aided design of pressure vessel and algorithm development, Computer aided CO2
Nozzle design, Computer aided Head design, CAD module generation for Pressure CO3
Vessel using MATLAB
3. Computer aided optimization in Chemical engineering CO1
Introduction of Optimization, Linear Programming, Simplex and Big M method and its TO
variants, Application of MATLAB for solving linear programming optimization CO6
problems, Nonlinear optimization in chemical engineering, Convexity and its
determination, Unconstraint and constraint nonlinear optimization methods, Newton’s
method, Nelder-Mead method, Steepest descent method, Nonlinear optimization using
MATLAB, CAD module generation for Optimization
4. Process Synthesis and Pinch Technology CO1
Optimal Distillation column sequencing, Direct and indirect sequencing, side-rectifier, TO
side-stripper columns, Prefractionator with heat integration, Petluyk column, Simulation CO6
studies of column sequencing, Heat Exchanger network design, energy target, computer
aided design of HENS
5. Process Flow-sheeting and simulation CO1
Flow sheet simulation algorithms, sequential modular and simultaneous modular TO
approaches, Equation Oriented approach, tearing of recycle streams, Simulation CO6
examples using process simulators

C. PRACTICAL AND TERM WORK


Simulation experiments are designed to use various CAD tools such as MATLAB, ASPEN PLUS
software for solving developing CAD modules for solving design problems, dynamic problems and
optimization problems

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 105


D. TEXT BOOKS
1. Bhattacharya, C. M.; Narayanan, C. M. Computer Aided Design of Chemical Equipment; New
Central Book Agency (P) Ltd.: Calcutta, India, 1992
2. Husain, A. Chemical Process Simulation, Wiley Eastern Limited: New Delhi, 1986
3. Smith, R. Chemical Process Design and Integration, John Wiley & Sons Ltd.: England, 2005
4. Seborg, D. E.; Edger, T. F.; Mellichamp, D. A. Process Dynamics and Control, 2nd ed.; Wiley
India, New Delhi, 2004

E. REFERENCE BOOKS
1. Edger, T. F.; Himmelblau, D. M.; Lasdon, L. S. Optimization of Chemical Processes; 2 nd ed.
McGraw-Hill: New York, 2001
2. B. V. Babu, Process Plant Simulations; Oxford Press, 2004

F. COURSE OUTCOMES
COs SKILLS STATEMENT
Formulate standard single/multivariable optimization Problem, Understand
and Apply various optimization techniques to solve problems in Chemical
CO1
Engineering using MATLAB. Understand distillation sequences using
process simulation software
Develop and Analyse energy target-based heat exchanger network using
Understanding process simulation software. Analyse steady state and dynamic problems
Analysing and create simulation modules for chemical processes using process
CO2
Applying simulation software.
Evaluating Understand the ethics and morality in the context of CAD in Chemical
Creating Engineering
Remembering Apply various CAD tools for solving design problems, Steady state and
CO3
evaluating dynamic Analysis problem, optimal control problems
Do critical evaluation of the performance of various CAD tools simulations
CO4
for solving chemical engineering problems.
CO5 Create CAD modules for design of process equipment
Generate a matlab program for industrial application to carry out steady
CO6
state and dynamics analysis.

G. COURSE MATRIX
CO1 CO2 CO3 CO4 CO5 CO6 AVG.
PO1 2 2 2 3 2 3 2.3
PO2 1 1 3 3 3 3 2.3
PO3 1 2 3 3 3 3 2.5
PO4 1 1 2 3 2 3 2
PO5 0 0 2 3 3 3 1.8
PO6 2 2 3 3 3 3 2.7
PO7 2 3 3 3 3 3 2.8
PO8 1 1 2 2 2 3 1.8
PO9 2 2 3 2 3 3 2.5
PO10 1 2 3 2 2 3 2.2
PO11 2 3 3 2 2 3 2.5
PO12 3 3 3 2 3 3 2.8
PSO1 2 3 3 3 2 3 2.67
PSO2 3 3 3 2 3 2 2.67
PSO3 2 3 2 2 2 2 2.17
PSO4 3 3 3 3 3 3 3

DEPARTMENT OF CHEMICAL ENGINEERING, DDU, NADIAD 106

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