X-ray

Diffraction
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Introduction to XRD
XRD basics
Interesting facts
Nobel prizes for research with X-rays
Background information
X-rays Overview
Properties of X-rays
Production of X-rays
The geometry of crystals
Crystal structure
Miller indices
Principles of diffraction
Wave structure
Interaction of X-rays with matter
Diffraction of X-rays by a crystal
Penetration depth
Diffraction measurements
XRD in practice
Anatomy of an X-ray diffractometer
Anatomy of an X-ray diffractometer - Intro
Source
Primary optics
Sample holder & stage
Secondary optics
Sample preparation
Types of samples
What is good data?
The importance of specimen height
Safety
Analysis of data
What the data tells you
Phase identification
Quantitative powder diffraction
Quantitative analysis
Factors affecting peak intensity
Factors affecting peak intensity - Intro
Structure Factor
Multiplicity factor
Lorentz polarisation factors
Temperature Factor
Summation of factors effecting peak intensity
Factors effecting peak width
Rietveld Refinement
What is Rietveld refinement?
Summary of analysis cues
Specialist techniques using XRD
Texture
What is texture?
Displaying texture
Measuring texture with X-rays
Normalisations

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 Residual stress
Glancing Angle XRD
Glancing angle XRD

Credits

www.myscope.training X-ray Diffraction 3

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 Credits

Microscopy Australia acknowledges the huge input of time and expertise by the many sta: members and associates
who have contributed to the development of MyScope over the years.

For the XRD module we thank: Nikki Stanford, Kevin Jack, Matt Foley, Ruth Williams, Aaron Dodd, Anya Yago, Philip
Francis.

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