OperatingManual FW95SL
OperatingManual FW95SL
OperatingManual FW95SL
160
80
240
40
F81-HL
T 1 2 3 F 0
°C
320
°C
4 5 6
ESC 7 8 9 0
SL
F83-HL
FP88-HL
F95-SL
FP88
water cooled
FW95-SL
Software-Version: V2.xx-xxxx
JULABO Labortechnik GmbH
Eisenbahnstraße 45
D-77960 Seelbach / Germany
( +49-7823 / 51-0
Printed in Germany 3 +49-7823 / 2491
Changes without prior notification reserved š info@julabo.de
1.951.2811 BE2 07/04 ü www.julabo.de
19512811.doc 29.07.04
Content Page
Congratulations!
You have made an excellent choice.
JULABO thanks you for the trust you have placed in us.
This operating manual has been designed to help you gain an understanding of the principles of operating and
possibilities of our circulators. For optimum utilization of all functions, we recommend that you thoroughly
study this manual prior to beginning operation.
2
Ultra-Low Refrigerated Circulators
TABLE OF CONTENTS
Operating manual...................................................................................................................5
Description.............................................................................................................................5
Operator responsibility – Safety recommendations ...............................................................6
EC Declaration of Conformity...............................................................................................8
Warranty conditions ...............................................................................................................9
Technical specifications .......................................................................................................10
Operating instructions......................................................................................................... 14
1. Operating controls and functional elements............................................................. 14
2. Safety notes for the user ............................................................................................. 17
3. Preparations .................................................................................................................. 17
3.1. Installation...................................................................................................................17
3.2. Bath fluids...................................................................................................................18
3.2.1. Tubing................................................................................................................19
3.3. Filling / draining..........................................................................................................20
3.4. Temperature application to external systems..............................................................22
3.4.1. External control.................................................................................................23
4. Operating procedures.................................................................................................. 24
4.1. Power connection........................................................................................................24
4.2. Switching on / Selecting the language ........................................................................24
5. Manual operation.......................................................................................................... 25
5.1. Start - Stop...................................................................................................................25
4
Ultra-Low Refrigerated Circulators
Operating manual
Description
JULABO circulators have been designed for temperature application to specific fluids in a bath tank.
The units provide pump nozzles for temperature application to an external system (loop circuit).
þ The circulators are operated via the splash-proof keypad. The implemented
microprocessor technology allows to set and to store different values that can be
indicated on the VFD COMFORT-DISPLAY and LCD DIALOG-DISPLAY. Three
menu keys facilitate adjusting setpoints, warning and safety functions and menu
functions.
þ The integrated programmer allows storing and running temperature and time-
dependent processes.
JULABO circulators are not conceived for direct temperature application to food and
luxury articles or pharmaceutical and medico-technical products. Direct temperature
application means: Unprotected contact of the object with the bath medium (bath fluid).
5
Operating manual
Persons:
The operator is responsible for the qualification of the personnel operating the units.
The operator should be constantly informed about the dangers involved with their job activities as well
as preventive actions.
Make sure all persons expected to carry out operation, installation and maintenance of the unit read and
understand the safety information and operating instructions.
When using hazardous materials, the circulator may only be operated by persons that are absolutely
familiar with these materials and the circulator. These persons must be fully aware of possible risks.
If you have any questions concerning the operation of your unit or the information in this manual,
please contact us!
Handling:
You received a product conceived for industrial use. Nevertheless, avoid strikes to the housing,
vibrations, damages to the keypad foil (keys, display) or contamination.
Make sure the product is regularly checked for proper condition. Regularly check (at least every
2 years) the proper condition of the mandatory, warning, prohibition and safety labels.
Take care that the mains supply features a low impedance to avoid any negative affects on the
instrument being operated in the same mains.
This unit is designed for operation in a controlled electromagnetic environment. This means that
transmitting devices (e.g. cellular phones) should not be used in the immediate vicinity.
Magnetic radiation may influence other units with components susceptible to magnetic fields
(e.g. a monitor). We recommend to keep a minimum distance of 1 m.
Permissible ambient temperature: max. 40 °C, min. 5 °C.
Permissible relative air humidity: 50 % (40 °C).
Do not store in an aggressive atmosphere. Protect from contaminations. Do not expose to sunlight.
Operation:
Only qualified personnel is authorized to perform configuration, installation, maintainance and repairs
of the circulator.
Routine operation can also be carried out by untrained personnel who should however be instructed by
trained personnel. The summarized user guidance (short manual) and the specification table with
information on individual parameters are sufficient for this.
6
Ultra-Low Refrigerated Circulators
Use:
The bath can be filled with flammable materials. Fire hazard!
There might be chemical dangers depending on the bath medium used.
Observe all warnings for the used materials (bath fluids) and the respective instructions (safety data
sheets).
Insufficient ventilation may result in the formation of explosive mixtures. Only use the unit in well
ventilated areas.
Only use recommended materials (bath fluids). Only use non-acid materials.
When using hazardous materials, the user must attach the enclosed safety labels to the front of the unit
so they are well visible: The yellow warning label W09 (danger area) and the blue mandatory label
M018 or Semi S1-0701 Table A1-2 #9 (Carefully read the user information prior to beginning
operation).
Warning label W09: Danger area.
Attention! Observe instructions.
Colours:
(operating manual, safety data sheet)
yellow, black
Mandatory label M018 Carefully read the user information prior to beginning
operation
Colours: blue, white
Scope: EU
Particular care and attention is necessary because of the wide operating range.
There are thermal dangers: Burn, scald, hot steam, hot parts and surfaces that can be touched.
Warning label W26:
Colours: Hot surface warning.
yellow, black (The label is put on by JULABO)
Observe the instructions in the manuals for instruments of a different make that you connect to the
circulator, particularly the respective safety recommendations. Also observe the pin assignment of plugs
and technical specifications of the products.
Disposal:
The circulator contains a so-called back-up battery that supplies voltage to memory chips when the unit
is switched off. Do not dispose of the battery in domestic waste!
Depending on battery regulations in your country, you might be obliged to give back used or defect
batteries to gathering places.
The product may be used with oil as bath fluid. These oils fully or partially consist of mineral oil or
synthetic oil. For disposal, observe the instructions in the safety data sheets.
This unit contains the refrigerants R404A and R23 – at this time considered not to have any negative
effects on the ozone layer. However, during the long operating period of the unit, disposal prescriptions
may change. So only qualified personnel should take care of disposal.
7
Operating manual
EC Declaration of Conformity
Ultra-Low Refrigerated Circulators:
F81-HL, F83-HL, FP88-HL
F95-SL, FW95-SL
The products mentioned comply with the requirements outlined by the following European
guidelines:
Guideline 73/23/EEC of the Council of 19 February 1973 with respect to legal harmonization of the
member countries concerning electric devices for use within certain voltage
limits
Guideline 89/336/EEC of the Council of 3 May 1989 with respect to legal harmonization of the member
countries concerning electromagnetic compatibility
Guideline 98/37/EC of the European Parliament and the Council of 22 June 1998 for harmonization of
legal and administrative regulations of the member countries with respect to
machinery
Guideline 97/23/EG of the European Parliament and the Council of 29. May 1997 with respect to legal
harmonization of the member countries with respect to pressure equipment.
8
Ultra-Low Refrigerated Circulators
Warranty conditions
JULABO Labortechnik GmbH warrants its products against defects in material or in workmanship,
when used under appropriate conditions and in accordance with appropriate operating instructions
With the ‘1PLUS warranty’ the user receives a free of charge extension to the warranty of up to 24
months, limited to a maximum of 10 000 working hours.
To apply for this extended warranty the user must register the unit on the JULABO web site
www.julabo.de, indicating the serial no. The extended warranty will apply from the date of JULABO
Labortechnik GmbH’s original invoice.
JULABO Labortechnik GmbH reserves the right to decide the validity of any warranty claim. In case
of faults arising either due to faulty materials or workmanship, parts will be repaired or replaced free of
charge, or a new replacement unit will be supplied.
9
Operating manual
Technical specifications
F81-HL F83-HL
Working temperature range °C -81 ... 100 -83 ... 50
Temperature stability °C ±0,02 ±0,02
Temperature selection digital
via keypad indication on LCD DIALOG-DISPLAY (°C/°F)
remote control via personal computer indication on monitor
Temperature indication VFD COMFORT-DISPLAY (°C/°F)
Resolution °C 0.01
Absolute Temperature Calibration °C ±3
Temperature control ICC - Intelligent Cascade Control
Heater wattage (at 230 V) kW 1,3 1,3
Cooling capacity °C +20 0 -20 -40 -60 -80 +20 0 -20 -40 -60 -80
Medium ethanol W 450 380 360 320 270 70 820 780 720 600 380 120
Cooling compressor 2-stage 2-stage
Refrigerant R404A/R23 R404A/R23
Electronically adj. pump capacity stages 1 ... 4 1 ... 4
Flow rate l/min at 0 bar 22 ... 26 22 ... 26
Pressure max. bar at 0 liter 0.7 0.7
Suction max bar at 0 liter 0.4 0.4
Electrical connections:
External alarm device 24-0 V DC / max. 25 mA
Computer interface RS232 or RS485
External Pt100 sensor
Optional for HL and SL
(Order No. 8900100 Electronic module with analog connections)
Programmer input -100 °C to 400 °C = 0 - 10 V or 0 - 20 mA or 4 - 20 mA
Input for the signal of a flow meter or external manipulated variable
Temperature recorder outputs 0 - 10 V (0 V = -100 °C, 10 V = 400 °C)
0 - 20 mA (0 mA = -100 °C, 20 mA = 400 °C)
4 - 20 mA (4 mA = -100 °C, 20 mA = 400 °C)
Standby input for external emergency switch-off
Alarm output for external alarm signal
Overall dimensions (WxDxH) cm 50x58x89 55x60x92
Bath opening (WxL) cm 13x15 13x15
Bath depth cm 16 16
Filling volume liters 5 ... 6,5 5,5 ... 8
Weight kg 88 118
Ambient temperature °C 5 ... 40 5 ... 40
Mains power connection ±10 % V/Hz 208 ... 230 / 60 208 ... 230 / 60
Mains power connection ±10 % V/Hz 208 ... 230 / 50 208 ... 230 / 50
Total power consumption kW 3,6 3,7
All measurements have been carried out at: rated voltage and frequency ambient temperature: 20 °C
Technical changes without prior notification reserved.
10
Ultra-Low Refrigerated Circulators
FP88-HL
Working temperature range °C -88 ... 100
Temperature stability °C ±0.02
Temperature selection digital
via keypad indication on LCD DIALOG-DISPLAY (°C/°F)
remote control via personal computer indication on monitor
Temperature indication VFD COMFORT-DISPLAY (°C/°F)
Resolution °C 0.01
Absolute Temperature Calibration °C ±3
Temperature control ICC - Intelligent Cascade Control
Heater wattage (at 230 V) kW 1,3
Cooling capacity °C +20 0 -20 -40 -60 -80
Medium ethanol W 960 960 920 730 590 150
Cooling compressor 2-stage
Refrigerant R404A/R23
Electronically adj. pump capacity stages 1 ... 4
Flow rate l/min at 0 bar 22 ... 26
Pressure max. bar at 0 liter 0.7
Suction max bar at 0 liter 0.4
Electrical connections:
External alarm device 24-0 V DC / max. 25 mA
Computer interface RS232 or RS485
External Pt100 sensor
Optional for HL and SL
(Order No. 8900100 Electronic module with analog connections)
Programmer input -100 °C to 400 °C = 0 - 10 V or 0 - 20 mA or 4 - 20 mA
Input for the signal of a flow meter or external manipulated variable
Temperature recorder outputs 0 - 10 V (0 V = -100 °C, 10 V = 400 °C)
0 - 20 mA (0 mA = -100 °C, 20 mA = 400 °C)
4 - 20 mA (4 mA = -100 °C, 20 mA = 400 °C)
Standby input for external emergency switch-off
Alarm output for external alarm signal
Overall dimensions (WxDxH) cm 55x60x92
Bath opening (WxL) cm 13x15
Bath depth cm 16
Filling volume liters 5,5 ... 8
Weight kg 121
Ambient temperature °C 5 ... 40
Mains power connection ±10 % V/Hz 208 ... 230 / 60
Mains power connection ±10 % V/Hz 208 ... 230 / 50
Total power consumption (at 230V) kW 2,82
All measurements have been carried out at: rated voltage and frequency ambient temperature: 20 °C
Technical changes without prior notification reserved.
11
Operating manual
12
Ultra-Low Refrigerated Circulators
13
Operating instructions
Operating instructions
1. Operating controls and functional elements
Front view Rear view
7 8 9a10 11 12
2 Sollwert
ExternIst:
165.5°C
Leistung:
124.7°C
Regelung:
%
50 1a ext
Pt10
SERIA ALAR STAND- REG
E-
intern 0 PROG
3
6 13
160
0
8 240
T 1 2 3 F
40
0
°C
320
°C
4 4 5 6
16a T16A
ES
C
7 8 9 0
HL
14
5 T16A
T1.25 15
17a A
21 22 9
1b 9b
19
18
FP88
FPW
24
17b
20
2 VFD-COMFORT-DISPLAY
Header: Control indicators see sections 2.1 and 2.2
Line 1: Actual value internal or external
The display is depending on the selected control mode in the
menu > Control < (internal or external).
Line 2: Working temp. setpoint, constantly S xxx.xx
Line 3: Actual value (E = external or I = internal)
Alternating with the display in line 1
15
Operating controls and functional elements
ALARM
11 Standby input (for external emergency switch-off)
STAND-BY
12 Programmer input and temperature recorder output
REG+E-PROG
13 Connector for supplementary pump or solenoid valve
230 V / max. 1.25 A
No control voltage in the -OFF- condition
14 Connector solenoid valve
1. No control voltage in the -OFF- condition
2. Configurable for controlled countercooling via solenoid valve
(only used with Heating Circulators)
21
22 Pump connectors suction pump pressure pump
OUT IN
24 Only for water cooled models: Cooling water OUTLET and INLET
16
Ultra-Low Refrigerated Circulators
Warning :
Describes a possibly highly dangerous situation.. If this is not avoided, serious injury and
danger to life could result.
Caution:
Describes a possibly dangerous situation. If this is not avoided, slight or minor injuries
could result. A warning of possible damage can also be contained in the text.
Notice:
Describes a possibly harmful situation. If this is not avoided, the product or anything in its
surroundings can be damaged.
3. Preparations
3.1. Installation
• Place the unit on an even surface on a pad made of non-flammable material.
• Keep at least 20 cm of open space on the front and rear venting grids.
• Do not set up the unit in the immediate vicinity of heat sources and do not
expose to sun light
• Before operating the unit after transport, wait about one hour after setting it up.
This will allow any oil that has accumulated laterally during transport to flow
back down thus ensuring maximum cooling performance of the compressor.
17
Preparations
Notice:
Please contact JULABO before using other than recommended bath fluids.
JULABO takes no responsibility for damages caused by the selection of an unsuitable
bath fluid.
Unsuitable bath fluids are liquids which e.g.
• are very highly viscous
(much higher than 70 mm2 /s at the respective working temperature)
• have corrosive characteristics or
• tend to cracking.
ATTENTION: The maximum permissible viscosity is 70 mm2 /s.
18
Ultra-Low Refrigerated Circulators
Caution:
The temperature controlling i.e. of fluids in a reactor constitutes normal circulator
practise.
We do not know which substances are contained within these vessels.
Many substances are:
• inflammable, easily ignited or explosive
• hazardous to health
• environmentally unsafe
i.e.: dangerous
The user alone is responsible for the handling of these substances!
The following questions shall help to recognize possible dangers and to reduce the risks
to a minimum.
• Are all tubes and electrical cables connected and installed?
Note:
sharp edges, hot surfaces in operation, moving machine parts, etc.
• Do dangerous steams or gases arise when heating?
Is an exhaust needed when working?
• What to do when a dangerous substance was spilled on or in the unit?
Before starting to work, obtain information concerning the substance and determine
the method of decontamination.
3.2.1. Tubing
Recommended tubing:
Order No. Length Temperature range
8930008 2m CR® tubing 8 mm inner dia. -20 °C to 120 °C
8930012 2m CR®- tubing 12 mm inner dia. -20 °C bis 120 °C
8930108 1m Viton tubing 8 mm inner dia. -50 °C to 200 °C
8930112 1m Viton tubing 12 mm inner dia. -50 °C bis 200 °C
8930410 2m Insulation for tubing 8 mm inner dia. -50 °C bis 100 °C
8930412 2m Insulation for tubing 12 mm inner dia. -50 °C bis 100 °C
8 930 209 0.5 m Metal tubing, triple insulated, M16x1 -100 °C to +350 °C
8 930 210 1.0 m
8 930 211 1.5 m
8 930 214 3.0 m
8 930 220 0.5 m Metal tubing, insulated, M16x1 -50 °C to +200 °C
8 930 221 1.0 m
8 930 222 1.5 m
8 930 223 3.0 m
Warning: Tubing:
At high working temperatures the tubing used for temperature application and cooling
water supply represents a danger source.
A damaged tubing line may cause hot bath fluid to be pumped out within a short time.
This may result in:
• Burning of skin
19
Preparations
• Difficulties in breathing due to hot atmosphere
Safety recommendations
• Employ suitable connecting tubing.
• Make sure that the tubing is securely attached.
• Avoid sharp bends in the tubing, and maintain a sufficient distance from
surrounding walls.
• Regularly check the tubing for material defects (e.g. for cracks).
• Preventive maintenance: Replace the tubing from time to time.
i After filling, immerse the samples in the bath or place the lid on the
bath, in case the opening is not to be used.
i The circulator provides an early warning system for low level
(description – please refer to page 30) that may be triggered when
changing samples in the bath.
Notice:
Pay attention to the thermal expansion of bath oil during heating to avoid overflowing
of the liquid.
Exercise caution when emptying hot bath fluids!
Check the temperature of the bath fluid prior to draining (by switching the unit on for
a short moment, for example).
Store and dispose the used bath fluid according to the laws for environmental
protection.
20
Ultra-Low Refrigerated Circulators
Draining:
• The drain plug is located behind the venting grid on the front of
the unit, which can be taken off by removing 4 screws.
• Slide a short piece of tube onto the drain port and hold it into a
pail.
• Unscrew the drain tap and empty the unit completely.
• Tighten the drain tap.
21
Preparations
Important:
i The liquid level should be equal in the internal and external
baths (absolute height).
S = Suction pump connection i If you take out samples (for example Erlenmeyer flasks) from
D = Pressure pump connection the external bath, turn the circulator off with the Start/Stop key.
K = Float
H = Height adjustment
i When working at temperatures below 0 °C and using the "D+S"
Level Adapter do not use oil as the bath liquid. Condensing air
will result in the formation of ice and thus affects the function
of the float.
Caution:
Fasten tubing to prevent slipping.
22
Ultra-Low Refrigerated Circulators
T16A
14
T1.25A
Flood hazard!
For this reason, solenoid valves for loop circuit or shut-off
valves can be integrated in the loop circuit.
i Connect the valve to the connector (13).
i If socket (14) is used:
In menu >Inputs/Outputs< set the
menu item >SV-Out< to >Backflow<.
Order No. Description
8 980 701 Set of solenoid valves
Inputs/Outputs for loop circuit up to +100 °C
>SV-Out : Backflow
Chan.1 : xxxxxxx 8 970 456 Shut-off valve (suitable up to +90 °C)
Chan.2 : xxxxxxx 8 970 457 Shut-off valve (suitable up to +250 °C)
(see page 48)
Pt100 M+R
23
Operating procedures
4. Operating procedures
4.1. Power connection
Caution:
Connect the unit only to a grounded mains power socket!
We disclaim all liability for damage caused by incorrect line voltages!
Check to make sure that the line voltage matches the supply voltage
specified on the identification plate. Deviations of ±10 % are permissible.
• Connect the circulator with mains power cable (17a) to the mains
outlet (18).
• Connect the control cable (9) between the connectors T (9a, 9b).
• Connect the refrigerated circulator with mains power cable (17b) to
the mains socket.
-OFF-
S 150.00
I 24.60
Configuration Selecting the language:
Off-Mode : pump off
>Language : english There are two options for the language of the LCD DIALOG-DISPLAY:
Reset : no German or English. Select the desired language in the menu
>Configuration< under the submenu >Language/Sprache<.
24
Ultra-Low Refrigerated Circulators
5. Manual operation
5.1. Start - Stop
Start: Press the start/stop key .
The actual bath temperature is displayed on the VFD COMFORT-
24.60 DISPLAY.
S 150.00 The LCD DIALOG-DISPLAY informs about adjustments and
E ----- conditions on the circulator (see example on the left).
Setpoint1: 150.00°C
IntAct : 24.60°C Stop: Press the start/stop key .
Power : 80 % The VFD COMFORT-DISPLAY indicates the message „OFF“.
Control : intern
i To save energy, turn off the cooling machine with the mains switch
(1b) whenever cooling is not required.
25
Manual operation
Setpoints
1. Press the key.
Setpoint1: 20.00°C The LCD DIALOG-DISPLAY indicates the valid settings.
Setpoint2: 37.00°C
>Setpoint3: 70.00°C 2. Use the keys to select Setpoint 3.
(One segment of the line blinks)
Change the value to 85 °C.
3. Use the numeral keypad to enter 8 and 5.
Then press enter to store the value.
Setpoints
The value remains visible on the LCD DIALOG-DISPLAY for about 10
Setpoint1: 20.00°C
Setpoint2: 37.00°C
seconds, or press to update the display immediately.
>Setpoint3: 85.00°C
i In the >Start< condition this value is immediately used for controlling
the working temperature.
The indication on the VFD COMFORT-DISPLAY is updated.
The heater control indicator blinks.
25.83
S 85.00
E -----
F
Notice: See SetMax: and SetMin:
in chapter 6.6. Limits on page 54
26
Ultra-Low Refrigerated Circulators
ESC
Safety-Values
>Warn-Type: Warning /Alarm
OverTemp: 85.00°C
SubTemp : -99.99°C 1
SafeTemp : 100.00°C 160
80 240
SafeSens : xx.xx°C 40
0 320
°C°C
Legend:
Select parameter
SafeTemp: Set the new cut-out value using a screwdriver via the LCD
DIALOG-DISPLAY. (Example: 50 °C)
27
Manual operation
Warning:
The excess temperature protection >SafeTemp< should be set at least 25 °C below the
fire point of the bath fluid used.
In the event of wrong setting there is a fire hazard!
We disclaim all liability for damage caused by wrong settings!
Actual temperature
below low tempera-
ture value.
28
Ultra-Low Refrigerated Circulators
Setpoint3 85.0°C
OverTemp 87.0°C
SubTemp 83.0°C
i The warning functions are only triggered when the actual bath temperature,
after start from the „OFF“ or „rOFF“ mode, lies within the set limits for 3
seconds.
29
Manual operation
Insuffient liquid
XXXXX level or float is
ALARM defective.
CODE 01 è
Press
Turn off the unit with the mains switch, refill bath fluid and
turn the unit on again!
3. Float
4. Circulating pump
5. Heater
Warning:
For refill always use the same bath fluid type that is already in the bath.
Bath oils must not contain any water contaminants and should be pre-heated to the
actual bath temperature! Explosion hazard at higher temperatures!
30
Ultra-Low Refrigerated Circulators
6. Menu functions
The term „menu functions“ refers to adjustments such as
Ø Configuration of the circulator
Ø Internal and external control with adjustable control parameters
Ø Start menu for the integrated programmer
Ø Integrated programmer; 6 profiles with 60 sections each
Ø Configurable inputs and outputs; analog recorder outputs, input for external
programmer or manipulated variable or flow rate
Ø Determination of limits for all important setting ranges and capacity
variables
Ø Online communication, with adjustable interface parameters
Ø Absolute temperature calibration; sensor calibration
Ø Electronically adjustable pump capacity
>Configuration
ESC
Control
Profile Start
Int.Programmer
Inputs/Outputs
Limits
Interface serial
ATCalibration
Pump
Select parameter
31
Menu functions
6.1. Configuration
>Configuration
Control ESC
Profile Start
Int.Programmer
Configuration
>Setpoint : keypad /RS232/ext.Pt100/eprog
ESC Autostart: off /on
OFF-Mode : pump off /pump on
Language : German /Englisch
Reset : no /yes
Variable : control /serial/eprog
Unit : °C /°F
Setpoint
The circulator provides four possibilities for setpoint setting. The selected mode
is indicated in line 1 on the LCD DIALOG-DISPLAY.
Possible parameters:
Setpoint1: 150.00°C Keypad – Setpoint setting via keypad or via the integrated programmer.
IntAct : 148.53°C
Power : 80 % (factory setting)
Control : intern
RS232 or RS485 - Setpoint setting via the serial RS232/RS485 interface (20)
RS232 : 150.00°C
ExtAct : 145.30°C through a PC or superordinated data system.
Power : 80 %
Control : extern In the header of the VFD COMFORT-DISPLAY an „R“ illuminates. It
indicates that remote control mode is set.
R
Important:
-OFF- Connect the circulator to a PC using an interface cable.
S xxxx
Check the interface parameters of both interfaces (on circulator and PC) and
I xxxx
make sure they match.
(see 10.1. Setup for remote control on page 69 )
Pt100 : 150.00°C ext.Pt100 – Setpoint setting via the analog socket „ext. Pt100“ using an external
ExtAct : 145.30°C
Power : 80 % temperature sensor or an appropriate voltage/current source.
Control : extern
32
Ultra-Low Refrigerated Circulators
eprog : 50.0°C eprog – Can only be adjusted when an electronic module with analog
IntAct
Power
:
:
24.7°C
80 %
connections is used (option).
Control : intern Setpoint setting via the analog interface REG+E-PROG through an external
programmer.
Important:
Connect the external programmer to the circulator via the socket REG+E-
PROG.
In the menu >Inputs/Outputs< set the parameter >EPROG< and the input
variables (see page 50).
The E-Prog input can only be used either under menu item >Setpoint< or
under menu item > Variable < (page 34).
Autostart
Possible parameters:
on - AUTOSTART on
off - AUTOSTART off (Factory setting)
Note:
The temperature system has been configured and supplied by JULABO
according to N.A.M.U.R. recommendations. This means for the start mode, that
the unit must enter a safe operating state after a power failure (non-automatic
start mode). This safe operating state is indicated by „ OFF „, resp. R OFF on
the VFD-COMFORT-DISPLAY. A complete shutdown of the main functional
elements such as heater and circulating pump is effected simultaneously.
The values set on the circulator remain stored, and the unit is returned to
operation by pressing the start/stop key (in manual control mode).
In remote control mode, the values need to be resent by the PC via the interface.
Should such a safety standard not be required, the AUTOSTART function
(automatic start mode) may be activated, thus allowing the start of the
instrument directly by pressing the mains power switch or using a timer.
i The AUTOSTART function can only be used, if setpoint setting is carried
out via >keyboard< or >eprog< or >ext. Pt100<.
Warning:
For supervised or unsupervised operation with the AUTOSTART function, avoid any
hazardous situation to persons or property.
The instrument does no longer conform to N.A.M.U.R. recommendations.
The safety and warning functions of the instrument should always be used to their
fullest capacity.
33
Menu functions
OFF-Mode
Normally the circulating pump is switched via the start/stop signal. However, if
circulation should be maintained also for the -OFF- condition, the parameter
>pump on< needs to be set.
Possible parameters:
pump off (factory setting)
pump on
Language
There are two options for the language of the LCD DIALOG-DISPLAY:
German or English.
Possible parameters:
deutsch / englisch German / English
Reset
Use this to reset all values to factory setting (except date and time).
Possible parameters:
yes
no (factory setting)
Possible parameters:
control – The internal control electronics of the circulator controls the heater.
(factory setting)
serial – The heater receives the control signal via the serial interface.
eprog – The heater receives the control signal via the E-Prog input. – Only
adjustable when an electronic module with analog connections is used
(option).
Important:
Set the parameter >EPROG< and the input variables also in the menu
>Inputs/Outputs< (see page 50).
Note:
The E-Prog input can only be used either under menu item >Setpoint<
(page 32) or under menu item > Variable <.
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Ultra-Low Refrigerated Circulators
Warning:
If set to >serial< or >eprog<, heat is applied to the bath without control. The user has to
take necessary precautions for temperature control by himself.
The safety and warning functions of the instrument should always be used to their
fullest capacity.
Unit
Temperature values can be displayed in the unit °C or °F.
With this change all adjusted temperature values are converted and displayed
Example: into the new unit.
Setpoints
>Setpoint1: 20.00°C
Setpoint2: 37.00°C
Sezpoint3: 70.00°C °F Possible parameters:
°C è °F ê -OFF- °C (factory setting)
Setpoints
>Setpoint1: 68.00°F
S xxxx
Setpoint2: 98.60°F I xxxx °F
Setpoint3: 158.00°F
6.2. Control
The circulator is conceived for internal and external temperature control.
Switching is carried out in this submenu. Depending on what is set, only the
respective set of parameters is indicated.
Configuration
>Control ESC
Profile Start
Int. Programmer
internal
Control
>ControlType: intern
ESC : Selftuning : once /always/off
Dynamic : aperio /normal
Xp : 1.0K
Tn : 100s
Tv : 5s 1
Control
>ControlType: extern
Selftuning: once /always/off
CoSpeed : 0.0
Xp : 0.7K
Tn : 720s
Tv : 55s
Xpu : 5.0K external
35
Menu functions
IMPORTANT:
Additional measures for external temperature control.
ext. i Connect a Pt100 sensor to the socket on the rear of the circulator.
Pt100
i Sensor calibration of the external Pt100 sensor is carried out in the menu
>ATCalibration<, with the > Status< set to >no< (see page 57).
i Suggested adjustments for external temperature control:
AreaUp/ AreaDown and IntMax / IntMin
see chapter >Limits< on page 54.
i External temperature control does not allow for setpoint setting via the
socket „ext. Pt100“ (see page 32).
Notice:
Place the external sensor into the bath medium and securely fix the sensor.
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Ultra-Low Refrigerated Circulators
Selftuning:
When performing an selftuning for the controlled system (temperature
application system), the control parameters Xp, Tn and Tv are automatically
determined and stored.
Possible parameters:
off - no selftuning.
The control parameters ascertained during the last identification are used
for control purposes.
Dynamic:
This parameter affects the temperature pattern only in case
of internal control.
normal
°C
temp. stability Possible parameters:
aperiodic normal –Allows for reaching the setpoint faster, but
setpoint overshooting of up to 5 % is possible.
Aperiodic – (factory setting)
t Target temperature is attained without overshooting.
temperature ramp
37
Menu functions
CoSpeed:
This parameter affects the temperature pattern only in case
of external control.
Possible parameters: 0 ... 5
During selftuning, the control parameters Xp, Tn
°C Int. temperature and Tv of a controlled system are automatically
determined and stored. Depending on the
controlled system, time for tuning can be
Ext. temperature
unequally longer. This controller layout allows
5
protection of sensitive objects requiring
3 temperature application.
0 As soon as a co-speed factor is set, it is
Setpoint considered for calculating the control parameters.
As shown in the diagram, tuning times become
t shorter the higher the co-speed factor is, but
overshooting can happen in the internal system.
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Ultra-Low Refrigerated Circulators
t t
t t
39
Menu functions
Configuration
ESC
Control
>Profile Start
Int. Programmer
>Start Profile 0
at Step 0 1
ESC Runs 1
Start no /yes/time
>hour.min 11:15
Day.Mon 11.12 1
Year 2003
Start no /yes
Possible parameters:
Start Profile 0 to 5
Select the profile that should be started.
at Step 0 bis 60.
Select the section with which the profile should be started.
Runs 0 to 99
Select the number of profile repetitions.
Starten no / yes ð (manual start)
or
time ð (via integrated timer)
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Ultra-Low Refrigerated Circulators
When selecting the parameter time, a new submenu is called up for entry of the
start time.
A flashing segment indicates that a start time needs to be entered.
hour.min Start time
Day.Mon day and month
Year year
Set each entry with enter .
Start no / yes
A flashing line indicates that the parameter „yes“ needs to be entered.
Press the key to select the parameter and press enter .
Starttime: 06:00 The temperature system switches to waiting mode and a flashing line
Date : 15:12 „wait“ appears on the LCD DIALOG-DISPLAY. The start time and
*** wait *** actual time are permanently indicated on the display.
Acttime 02:34:45
41
Menu functions
6.3.1. Status at the end of the profile
There are two possibilities for manually starting a program:
1. Starting a profile from the OFF state:
The temperature system switches back to the OFF state at the end of the
profile.
2. Starting a profile from the operating state.
The temperature system is started with the start key , and the bath is
heated to the desired temperature, for example 100 °C. At the end of the
profile, the programmer switches to the operating state and holds the bath
temperature stable at 100.00 °C.
Setp. : 125.80°C
i Press the start/stop key to interrupt or continue a profile.
IntAct: 124.70°C The setpoint and time period set for the corresponding section are
Prof. : 4 Step:12 thus stopped at the values presently achieved.
*** pause *** The instrument is put on hold and the message „pause“ flashes on the
LCD DIALOG DISPLAY.
Warning:
Following a power interruption, it would be possible in this condition for the
instrument to restart automatically. The safety and warning functions of the instrument
should always be used to their fullest capacity.
See Warning page 33.
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Ultra-Low Refrigerated Circulators
Setp : 125.80°C
i A profile can be terminated by pressing . The programmer
IntAct: 124.70°C switches back to the Start menu.
Prof. : 4 Step:12
Remain: 00:03:45 • Press again to quit the menu
ê or
use the keys to remain in the Start menu.
>Start Profile x
at Step x
Runs 1 The start of another temperature profile can now be prepared if
Start no necessary.
43
Menu functions
Profile Start
>Int. Programmer ESC
Inputs/Outputs
Limits
>Edit Profile: 0
Step: 0
Setp: °C 1
Time [hh:mm]
>Delete Prof. 0
from Step 0 1
to Step 60
delete no /yes
ESC
>Print Profile 0 1
Print yes /no
>hour.min 14:24
Day.Mon 07.12
Year 2003 1
09:27:36
1. Use the keys to select the desired menu item in menu level 2
on the LCD DIALOG-DISPLAY (>) and press enter to change to
menu level 3. An input window opens for each menu item.
2. In the input window, select the menu item with the keys .
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Ultra-Low Refrigerated Circulators
Example:
Step (No.) 1 3 5 6 9 11 14
Setpoint (°C) 50 50 100 100 80 80 20
Time (h.m) 00:08 00.02 00:10 01:05 00:10 00:05 00:30
45
Menu functions
Display sections (Step):
>Edit Profile: 1 1 Use the keys to select the submenu „Step“, enter the desired
Step: 3
Setp: 50.00°C number and press enter
Time [hh:mm] 00:02 or
2 If the submenu „Step“ is selected, section by section can be shown in
ascending order by the key .
i Each previously set value is displayed.
Example: Delete:
A flashing segment indicates that the respective profile number
>Delete Prof. 4
from Step 8 needs to be entered in which one or more consecutive sections are to
to Step 34 be deleted.
delete yes
Example:
ê Delete step 8 to step 34 in profile 4.
Example: Print:
>Print Profile 2
Each profile may be printed via the serial interface for control or
Print yes documentation.
A flashing segment indicates that the number of the profile to be
printed needs to be entered.
Example: Print profile 2
ê yes
>Print Profile 2
****** print ******* Printing is indicated in line 2.
46
Ultra-Low Refrigerated Circulators
Inputs/Outputs
ESC >SV-Out. : Backflow /C-Puls
Chan.1 : ActInt
Chan.2 : Power
Chan.3 : Setpoint
EPROG : Setpoint
Ext.StBy : inactive /active
AlarmOut : StdBy
AlarmOut
>Function: StdBy /Alarm/Al+StBy
Type : normal /invers
47
Menu functions
Menu level 2 1. Use the keys to select the desired (>) menu item in
Inputs/Outputs
menu level 2 on the LCD DIALOG-DISPLAY.
>SV-Out : Backflow /C-Puls
Chan.1 : ActInt 2. Use the keys and to store the desired parameter or
Chan.2 : ActInt
Chan.3 : Setpoint press enter to enter menu level 3. An input window
EPROG : Setpoint opens for each menu item.
Ext.StBy : inactiv /activ
AlarmOut : StdBy 3. In the input window in menu level 3 select the menu item with
the keys .
Menu level 2
SV-Output Control connector (14) 230 V max. 1.25 A
Channel 1 voltage output for recorder (V)
Channel 2 voltage output for recorder (V))
Channel 3 current output for recorder (mA)
EPROG external programmer input
External standby Standby input
(for external emergency switch-off)
Alarm output Output for external alarm signal
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Ultra-Low Refrigerated Circulators
REG+E-PROG (12):
Outputs of the connector
Examples:
>Chan.1 : ActInt
0V 0V = 10°C
10V = 210°C
10 °C 210 °C
∆ Τ = 200 K lowest temperature value: 10 °C
highest temperature value 210 °C
197 °C 202 °C Fig. shows 200 °C scaled to paper width
∆Τ=5 K rise: 50 mV/°C
49
Menu functions
i The E-Prog input can only be used either under menu item >Setpoint<
or under menu item > Variable <.
If the input is neither occupied by >Setpoint< or > Variable <, the
signal of a flow meter can be connected.
i First set menu >Configuration<, then menu >Inputs/Outputs<.
Example:
• Set a temperature of 50 °C on the external programmer!
i The value adjusted and set on the external programmer is displayed in
line 4 of the LCD DIALOG-DISPLAY for control purposes.
50
Ultra-Low Refrigerated Circulators
Eprog : 50.0°C
IntAct : 24.7°C i After returning the LCD display to standard display by pressing
Power : 80 % this value is displayed in line 1
Control : intern
(Example: Eprog 50.00 °C).
This EPROG input enables the use of different voltage and current values
as program parameters.
• „L Value“ - Setting the LOW value:
°C
1) Adjust and set the lowest desired value on the voltage or
300 current source resp. (Example A: 1 V).
250
2) Assign a lower temperature threshold value to this adjusted
B voltage/current value by pressing the appropriate buttons on the
200 keypad of the instrument (Example A: 20 °C ) and set by
A
150 pressing enter .
Notice:
If this adjustment is not correctly performed at two different points, the setpoint
setting will be incorrect.
51
Menu functions
52
Ultra-Low Refrigerated Circulators
53
Menu functions
6.6. Limits
The menu >Limits< allows for setting the minimum and maximum values for
all important setting ranges and capacity variables.
Inputs/Outputs ESC
>Limits
Interface serial
ATCalibration
Limits
ESC >SetMax :300.00°C
SetMin :-94.99°C
HeatingMax: 100%
CoolingMax: 0% 1
IntMax :300.00°C
IntMin :-94.99°C In case of external control
Upper band: 200K these menu items are
Lower band: 200K additionally indicated
54
Ultra-Low Refrigerated Circulators
100
75 AreaDown Using Upper band and Lower band, the
AreaUp
difference between the temperatures in the
50
internal bath and the external system can
25 be limited to any maximum value for the
heat-up or the cool-down phase.
10 20 30 40 50 60 10 20 30 40 50 60 10 [min] t
During the heat-up phase the difference value always adds to the actual external
temperature. During the cool-down phase, the difference value is subtracted.
Sense of a band limit:
þ Ensures gentle heating for the objects requiring temperature application.
þ Protects glass reactors, for example, from thermal shock.
i The IntMax: and IntMin: values are superordinated to this band limit.
55
Menu functions
Inputs/Out ESC
Limits
>Interface serial
ATCalibration
RS232
Interface
ESC >Type RS232 /RS485/PROFI
Baudrate 4800 /9600/19200/38400
Parity even /no/odd
Handshake hardw / softw
RS485
Interface
>Type RS485 /PROFI/RS232
Baudrate 4800 /9600/19200/38400
Parity even /no/odd
Address 0
1
Address 0 to 127
Factory settings:
4800 Bauds
even
hardware handshake
56
Ultra-Low Refrigerated Circulators
Limits ESC
Interface serial
>ATCalibration
Pump
internal
ATCalibration
ESC >Sensor : intern
Status : no /yes
Type : 3-point /1-point/2-point
TmpValue1: xx.xx°C
CalValue1: xx.xx°C
TmpValue2: xx.xx°C
CalValue2: xx.xx°C 1
TmpValue3: xx.xx°C
CalValue3: xx.xx°C
ATCalibration
ESC >Sensor : extern
Status : no /yes
Type : 3-point /1-point/2-point
TmpValue1: xx.xx°C
CalValue1: xx.xx°C
TmpValue2: xx.xx°C
CalValue2: xx.xx°C external
1
TmpValue3: xx.xx°C
CalValue3: xx.xx°C
Status:
>no< The controller of the circulator uses the original curve of
the temperature sensor.
Important: During the calibration process >no< needs to be set.
57
Menu functions
Type:
A >1-point<, >2-point < or >3-point < calibration can be carried
out.
First geometrically define the location for calibration (measuring
point TM), then determine the temperature values of of the calibration
points.
The calibration type also determines the number of pairs of values
indicated on the LCD DIALOG-DISPLAY.
TmpValue: 1 or 2 or 3
Defined temperature value of the calibration point. This value is
automatically stored with >CalValue< and can be indicated for
control purposes.
CalValue: 1 or 2 or 3
The „Calibration value“ is determined with a temperature measuring
device and stored under menu item >CalValue<.
Example: Principle :
1-point calibration For ATC calibration, in steady state the bath temperature at the location of
°C the temperature sensor (T M) is determined at the respective adjusted
working temperature. This value is then set on the circulator in the menu
>ATCalibration< under menu item >Calwert X<.
This can be a 1-point, 2-point or 3-point calibration.
TT1
°C
3-point calibration
°C
58
Ultra-Low Refrigerated Circulators
Examples: Example:
TT = 80.00 °C 3-point calibration for internal control.
TM = 79.73 °C In the temperature range of 80 °C to 160 °C the calibration curve of the
TT = 120.00 °C temperature sensor (TT ) should be assimilated to the actual temperatures
TM = 119.51 °C on the measuring point (TM).
TT = 160.00 °C
TM = 159.34 °C
• Press the button. Under the menu >Control< set >ControlType<
Control to >intern< and press enter .
>ControlType: intern
Selftuning: once (ControlType: Can only be adjusted in the –OFF– condition)
Dynamic
nein : aperio
• Press start/stop .
Calibration procedure:
ATCalibration
>Sensor : intern 4. Set the following:
Status : no Menu item >Sensor< to >intern< ,
Type : 3.point
TmpValue1: 80.00°C Menu item >Status< to >no< ,
CalValue1: 79.73°C Menu item >Type< to >3-point<.
TmpValue2: xx.xx°C
CalValue2: xx.xx°C
TmpValue3: xx.xx°C
CalValue3: xx.xx°C 5. Read the value of TM on the temperature measuring device and enter
the value under menu item >CalValue 1< (79.73 °C) using the
numeral keypad.
Press enter and the circulator also stores the value of TT as
value for >TmpValue 1< (80.00 °C) .
The first of the 3 points is now calibrated.
59
Menu functions
Limits ESC
Interface serial
ATCalibration
>Pump
Pump
ESC >Pump level: 1 /2/3/4
60
Ultra-Low Refrigerated Circulators
ALARM • The circulator is operated without bath fluid, or the liquid level is
insufficient. Replenish the bath tank with the bath fluid.
CODE 01
• Tube breakage has occured (insufficient filling level due to excessive
Insuffient liquid
level or float is bath fluid pumped out). Replace the tubing and replenish the bath tank
defective. with the bath fluid.
• The float is defect (e. g., because damaged in transit). Repair by
authorized JULABO service personnel.
61
Troubleshooting guide / Error messages
ALARM
• Other errors (I2 C-BUS errors)
CODE 07
The internal I2C
bus-system shows
a failure.
62
Ultra-Low Refrigerated Circulators
ALARM • External control selected, but external Pt100 sensor not connected or
defect.
CODE 15
External control
selected, but ext.
sensor not connected
or defective.
ALARM • Ext. Pt100 sensor input without signal, but setpoint programming set
to external Pt100.
CODE 38
Ext. Sensor input
without signal but
setpoint programming
set to ext. Pt100.
63
Troubleshooting guide / Error messages
WARNING • The early warning system for low level signals a critical fluid level.
CODE 40 Replenish the bath tank with the bath fluid.
After eliminating the malfunction, press the mains power switch off and
on again to cancel the alarm state.
If the unit cannot be returned to operation, contact an authorized JULABO
service station.
Fuses:
The mains fuses on the rear of the unit may easily be exchanged as shown
on the left.
Circulator: Fine fuses (15)– T 1.25 A, 250 V~ , D 5 x 20 mm
Circulator: Fine fuses (16a)– T 16 A, 250 V~ , D5 x 20 mm
Warning:
Before exchanging the fuses, turn off the mains power switch and disconnect the
power plug from the mains socket!
Only use fine fuses with a nominal value as specified.
Example:
Manufacturer Supplier Type Order No.
Schurter Schurter G-fuse insert SPT No. 0001.2516
T16A 5x20mm
Wickmann Wickmann G-fuse insert No. 19195
T1.25A 5x20 mm
64
Ultra-Low Refrigerated Circulators
8. Safety recommendations
Follow the safety recommendations to prevent damage to persons or property. Further,
the valid safety instructions for working places must be followed.
• Some parts of the bath cover and the pump connections may become extremely
warm during continuous operation. Therefore, exercise particular caution when
touching these parts.
Notice:
Check the safety installations at least twice a year!
• Excess temperature protection according to IEC 61010-2-010
With a screwdriver turn back the adjustable excess temperature protection until the
shut-down point (actual temperature).
• Low level protection according to IEC 61010-2-010
To check the function of the float, it can be manually lowered with a screwdriver
for example.
65
Electrical connections
9. Electrical connections
Notice:
Use shielded cables only.
The shield of the connecting cable is electrically connected to the plug housing.
The unit ensures safe operation if connecting cables with a maximum length of 3 m are
used. The use of longer cables does not affect proper performance of the unit, however
external interferences may have a negative impact on safe operation.
66
Ultra-Low Refrigerated Circulators
RS232 interface cable 9-pin / 9-pin, 2.5 m - Order No.: 8 980 073
/ Control output
The T connector may be used for control of JULABO refrigerated
circulators or as output for alarm messages.
Alarm output
(for external alarm signal)
This potential-free change-over contact is activated in case of an alarm
when pins 2 and 3 are connected.
67
Electrical connections
STAND-BY input
(for external emergency switch-off)
STAND-BY
Pin Signal
1 Voltage output Channel 1 0 ... 10 V
2 Voltage output Channel 2 0 ... 10 V
REG+E-PROG 3 GND for outputs 0V
4 Programmer input EPROG 0 to 10 V / 0 to 20 mA
5 Current output Channel 3 0 to 20 mA / 4 to 20 mA
6 GND for Progammer 0V
68
Ultra-Low Refrigerated Circulators
F
Like all parameters which can be entered through the keypad, interface
parameters are stored in memory even after the circulator is turned off.
In remote control mode: After a power interruption the order to start and all
F values which have to be adjusted must be resent from the personal computer
via the interface.
AUTOSTART is not possible.
69
Remote control
Â
To ensure a safe data transfer, the time gap between two commands should be
at least 250 ms.
The circulator automatically responds to an in command with a data string
followed by a LF (Line Feed). The next command should only be sent after
10 ms.
F
The out commands are valid only in remote control mode.
Examples:
When the RS485 interface is used, the three-digit instrument address stands in
front of each command.
(example: address Ad32 = A032 )
Notice: out-commands
Temperature values can be displayed on the circulator in the unit °C or °F.
According to this setting the instructions via the interface also have to be made in the
set unit.
70
Ultra-Low Refrigerated Circulators
71
Remote control
72
Ultra-Low Refrigerated Circulators
73
Remote control
74
Ultra-Low Refrigerated Circulators
75
JULABO Service – Online remote diagnosis
ç see example
76
Ultra-Low Refrigerated Circulators
77
Cleaning the unit
Repairs
Before asking for a service technician or returning a JULABO instrument for
repair, please contact an authorized JULABO service station.
JULABO reserves the right to carry out technical modifications with repairs for
providing improved performance of a unit.
78