Final Black Book
Final Black Book
Final Black Book
ASH IN CONCRETE
of
BACHELOR OF ENGINEERING
In
CIVIL ENGINEERING
Submitted By
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PUNE-411001
CERTIFICATE
This is to certify that the work contained in the project report/dissertation entitled,
I considered that the thesis has reached the standards and fulfilled the requirements of the
rules and regulations relating to the nature of the degree. The contents embodied in the thesis have
not been submitted for the award of any other degree or diploma in this or any other university.
Date: 20/05/2024
Place: Pune
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Head of Department External Examiner
AKNOWLEDGEMENT
It is always a pleasure to remind the fine people in the Engineering program for
in engineering.
that studying completion academically sound but also industry ready by including
such industrial training patterns. I express my immense pleasure and deep sense of
gratitude to PROF. UTTAM JADHAV (MENTOR) for his guidance and others who
Finally, I would like to thank all engineers who shared their precious knowledge with
us.
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Contents
CERTIFICATE...........................................................................................................................2
ACKNOWLEDGEMENT..........................................................................................................3
Index……………………………………………………………………………………………4
List of Figures.............................................................................................................................6
List of Tables..............................................................................................................................7
CHAPTER I................................................................................................................................8
INTRODUCTION.................................................................................................................8
CHAPTER II.............................................................................................................................12
CHAPTER III...........................................................................................................................16
CONSTRUCTION PROCESS............................................................................................16
CHAPTER IV...........................................................................................................................22
CONSTRUCTION MATERIALS.......................................................................................22
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4.1 BUILDING CONSTRUCTION MATERIALS.....................................................22
CHAPTER V............................................................................................................................26
SAFETY MEASURES........................................................................................................26
CHAPTER VI...........................................................................................................................27
PRACTICAL EXPERIENCE..............................................................................................27
CHAPTER VII..........................................................................................................................36
7.1 CONCLUSION....................................................................................................36
CHAPTER VIII........................................................................................................................38
REFRENCES................…………………………………………………..……..…….38
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List of Figures
6
List of Tables
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CHAPTER I
INTRODUCTION
The increasing population has resulted in a higher generation of domestic and industrial
wastewater sludge. The sludge ends up as a landfill in designated areas which makes the land
unusable. The search for lightweight materials for construction has led to the use of sludge as a
viable replacement for the basic composition of concrete due to its low density.
The dry sludge collected from PMC Wastewater Treatment Plant (WWTP) in Pune Province was
used as a partial replacement of cement in concrete. The sludge content in the sand varied from 5,
10, 15, 20 %. The outcomes of the analysis indicate that the partial replacement of cement with dry
The result showed that up to 7.5 % of cement could be replaced with dry sludge in concrete for
structural applications. The unit weight of the concrete decreased with increasing sludge content,
which was attributed to the lower density of the sludge. The SEM image revealed a porous nature
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1.2 INTRODUTION OF PROJECT
Concrete is a basic engineering material used in most civil engineering structures. Its popularity
as a basic building material in construction is linked to its strength, economic use, good durability,
and ability to be manufactured on-site. The ability to mold it into any shape and size because of its
plasticity in its fresh stage and its subsequent hardening to achieve strength is particularly useful. All
countries in the world have a high dependence on concrete for the construction of many different
infrastructures. However, the cost of concrete in developing countries has increased drastically in the
past two decades due to its high demand and production cost in the construction industry. This has
necessitated finding alternative materials for concrete composite production. These materials could
be used to partially replace cement, sand and/or coarse aggregate. One of the materials used as a
partial replacement in concrete is sewage sludge. The objective of sewage treatment is to produce
treated sewage water and sewage sludge suitable for safe discharge into the environment or reuse.
The most common treatment options for sewage sludge include anaerobic digestion, aerobic
Snyman et al., reported that most of the wastewater treatment plants in South Africa dispose their
sewage sludge on dedicated land disposal (DLD) sites (also known as sacrificial lands) since this is
the quickest and cheapest way to dispose of the sewage sludge. Tantawy et al., stated that in the past
decades, sewage sludge was primarily disposed of on the land (landfill) and sea waters. Space
limitations for existing landfills and increasing environmental concerns such as groundwater
pollution from land leachate, odor emission and soil contamination have prompted an investigation
of alternative disposal routes. In trying to make good and practical use of this material, to reduce the
dangerous effect on the environment and reduce landfill, it was introduced into concrete as part of
the basic components. Yagua et al., reported that the performance of concrete containing dry sludge
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depends on sludge composition, organic material content and volume of incorporation. Sludge has
Sludge has a devastating effect on the environment and the health of people. The utilization of
sewage sludge ashes (SSA) for agricultural purposes was discontinued due to environmental and
health concerns regarding the heavy metals and toxic elements present in the sludge. Both share the
same sentiments that there is a need to research different options to improve sludge disposal while
ensuring that people’s health and the environment are compromised. No research has been done in
Pune to use wastewater dry sludge in concrete pavement bricks, neither has the SSA from this region
been evaluated for heavy metals’ leakage to the environment. Based on these reasons, concrete cubes
containing sludge can be made at an industrial scale to evaluate the impact of Pune based wastewater
sludge in concrete and on the environment. Hence, the need to further research on the optimal
design’s method for the incorporation of sludge in concrete and area of suitable application.
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1.3 OBJECTIVES OF PROJECT
contributes to significant carbon emissions. Using sewage byproducts or other sustainable materials
materials can provide a useful outlet for waste materials that might otherwise be disposed of in
Cost Savings: In some cases, using sewage byproducts or alternative materials may be more cost-
Improved Energy Efficiency: Some alternative construction materials, such as those made from
sewage byproducts, may offer better insulation properties, which can contribute to improved energy
efficiency in buildings.
However, it's important to note that using sewage byproducts in construction would require careful
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CHAPTER II
Yagüe, Valls, and Vàzquez studied the impact of utilizing dry sewage sludge on
different percentages (5, 10, 15, 20) % by weight of cement. The result showed a
decrease in mechanical strength when adding 10% sludge, as well as the longest initial
and final setting times. The strengths of the 2.5 and 5% mortars are relatively similar,
concluded that there was a reduction in the mechanical strength and density of the
mortar due to the addition of sludge to the increase in its porosity, also there was a
retard in the hydration process of the cement. Sewage sludge stabilized and the
quantity of leachable heavy ions was reduced in comparison with that of control
sample.
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Paper Title: 1 Using Sewage Sludge as additive.
Al-Nasrawi, 2003
Matar, 2008
Findings from the paper: - The reduction in strength was increased with the increase of sludge
- Dry and wet sludge can be feasibly utilized in concrete mixtures to 15%.
- No significant changes were made to the pore structure of the pastes when replacing cement with
- Utilizing SSA together with GC could produce acceptable mechanical, durability, and leaching
properties.
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Jamshidi et al., 2013
Findings from the paper: - Physical properties of the produced aggregate incorporated with sewage
sludge are similar or better than that of the commercial type especially for water absorption.
- Reduction in concrete strength due to using artificial aggregate in comparison with granite
aggregate.
- Workability of concrete decreased with the addition of waste dry sludge as a partial replacement
Findings from the paper: - Utilizing a mixture of 50% of sludge, 25% of SF, and 25% of RHA at the
temperature used in the brick kiln was the optimum percentages for brick production.
- Increase in water absorption and thermal insulation with a reduction in the compressive
- The quality of produced bricks at 5% of sludge replacement is preferable to that of only clay
incorporated bricks.
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- The ash generated from sludge incineration, which contains high amounts of Fe, Al, Ca and Si can
- The consumed firing energy decreased by up to 48.6% for bricks incorporating 25% of SS due to
Findings from the paper: Using SSA as an additive in concrete block production resulted from density
and strength similar to that of the control sample (without SSA) at 28 days of curing with a
significant
- Sludge and/or waste produced from water, sewage treatment, and power plants can be feasibly
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CHAPTER III
CONSTRUCTION PROCESS
1.Calculating values of fine aggregate, coarse aggregate, and cement for concrete mix:
When developing a mix design for concrete, there is always a Target Design Strength (TDS) in
mind. This TDS help to categorise which range the concrete falls into, which could be a low
strength (≤20 MPa), medium strength (20–25 MPa) or high strength (>25 MPa). This strength will
inform the ratio of the cement, sand, stone, and water level. Concrete containing other components
other than the general natural aggregates tend to show low strength. Concrete with a compressive
strength greater than 25 MPa after 28 days, are applicable for structural applications. Due to the
lower density of the sludge, the concrete will be lightweight concrete. For this research work, the
design strength was 25 MPa, making it applicable for the lightweight high-strength structural
TDS = CS + 1.64(SD)
Where TDS is the target design strength, CS is the characteristic strength, and SD is the standard
deviation.
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2.Calculating water cement ratio:
The water cement ratio (w/c) of 0.65 was adopted based on the trial mix that was conducted. The
concrete was hand mixed in line with SANS 5861-1:2006. Based on the mix design in Table 2, a
trial mix was conducted, and the optimal mix was adopted. The partial sand replacement with dry
sludge ranging between 2.5, 5, 7.5, 10 and 12.5 %, represented by C1, C2, C3, C4 and C5
respectively done. Concrete cube compacting done using vibrating table method. The cast cubes
were allowed to set on a non-vibrating floor and covered with polyethylene bags to prevent rapid
evaporation. The cubes were cure in wastewater and potable water and were crushed after 7, 14
and 28 days. The temperature of the water bath where the concrete cubes cured were maintained
2.Making concrete mix by replacing cement with 0, 5, 10, 15, 20% of sludge ash.
6.Tensile member test for checking the strength of the concrete mix.
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Fig. 3.1 Mixing of concrete
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Fig. 3.2 Casting of beam
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Fig. 3.3 Initial setting of beams
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Fig. 3.4 Curing of beams.
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CHAPTER IV
CONSTRUCTION MATERIALS
The basic construction materials used for the beam structure are –
1. Cement
2. Sand
3. Aggregate
4. Sludge ash
1.Cement
Company: - ULTRATECH
Ordinary Portland Cement (OPC) the most widely and commonly used cement in the world.
This type of cement is manufactured as a powder by mixing limestone and other raw materials
which consist of argillaceous, calcareous and gypsum. It is preferred in places where there is a
need for fast construction and setting time. This cement is available in the market in three grades
namely OPC 33, OPC 43 and OPC 53. These grades imply the maximum strength of the particular
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Grade attains 27 Mpa in 7days compared to 23 Mpa by 43-grade cement and achieves a final
compression strength of 53 Megapascals in 28 days. Where OPC is used- OPC is widely used for
the construction of high-rise buildings, roads, dams, bridges, flyovers where high strength and fast
setting is required.
2.Sand
It is a fine quality white-grey sand used in concrete and masonry work. It can also be used for
plastering, brickworks, RCC etc. This sand has a better grain shape with a smooth texture and
demands less moisture since water is already trapped within its particles. It consists of 5-20% of
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Fig. 4.2 Sand
3.Aggregate
Both types of aggregates i.e., Fine and Coarse Aggregates are used for the preparation of concrete.
The Natural Aggregates are in rough shape, and it can get stuck in the concrete pipe while
4.Sludge Ash
The dry sludge used for this research was collected from PMC Wastewater Treatment Plant
(WWTP) of Pune Province, Maharashtra. The environmental friendliness of the dry sludge was also
considered to promote its use in lightweight concrete. The sludge was air dried and was crushed until
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Fig. 4.5 Sludge Ash
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CHAPTER V
SAFETY MEASURES
Safety is the most important factor when it comes to working on a construction site. Especially the
workers working at high-rise structures are most prone to accidents. Hence the safety of workers
and employees should be taken care of. Safety measures on the site were taken as follows:
1.Due to the hazardous nature of wastewater sludge, proper handling was ensured to prevent direct
3.For proper handling of the material, some basic precautions were followed throughout the
experiment, this include but not limited to the use of gloves, glasses, dust mask, safety shoes and
protective clothing.
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CHAPTER VI
PRACTICAL
EXPERIENCE
In this chapter, experiments and tests were carried out in order to examine the achievement of
sewage sludge ash as a filler in concrete. The procedure of preparing the sewage sludge, the
materials used for the experiment and the type of testing such as Workability test,
compressive test, and flexural are being discussed. The methodology and setup of the
The concrete mix design is calculated by using a trial mix design method. The trial mix
design method is used to acquire a perspective on the constituents of the concrete based on
specific requirements. The proportion of the cement, water, coarse aggregate, and fine
aggregate was calculated based on the specified values by Indian standard. The concrete
of 10% due to freshness and lack of experience in casting concrete and the slump is specified
Preparation of SSA:
To ensure the consistency of samples, the sewage sludge is acquired from the same treatment
plant. The sewage sludge is collected after 7 consecutive non-raining days for best quality
control purposes and to ensure the sewage sludge is in dry condition. When collecting the
sludge, impurities such as grass, roots and trash is filtered and removed. Only the top layer of
sewage sludge is being collected to prevent over deep excavation which may cause the
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bottom sand layer of the drying beds to be mixed with the sewage sludge. Before the oven
drying and incineration process of sewage sludge, the sewage sludge was kept in a container
to prevent the sewage sludge from contact with other impurities. The sewage sludge is
oven dried at the temperature of 100°C for a period of 24 hours to ensure that the samples are
The sewage sludge is incinerated in a closed-lid method to make sure that all the sewage
sludge.
ash is fully trapped inside the cup. The sewage sludge is incinerated from room temperature to
the maximum temperature of 600°C for a duration of 3 hours. Time taken to incinerate from
room temperature to 600°C is approximately 15 minutes and cooling down duration from
600°C to 200°C is approximately 5 hours. The sewage sludge ash is removed from the
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Yield of SSA:
The average yielding percentage results obtained from 10 times of incineration at the temperature
of 600 °C for the duration of 3 hours of sewage sludge ash is 47.45 %. This shows that the
waste has been reduced by more than half and the leftover residue, which is the sewage
sludge ash, isa potential cement replacement material. the reduction in the volume due to
during the incineration process, the organic compounds and microorganisms been removed
Casting of cubes:
1.Grade of concrete - M 25
2.Proportion - 1: 1: 2
3.No of beams - 5
(gm.)
00 0 1870 gm.
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Table 6.2 Weights of aggregate
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Fig. 6.2 Weight of containers with sludge ash
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6.2 Test to be performed on the concrete:
1.Workability Test:
Slump cone test is to determine the workability or consistency of concrete mix prepared at the
laboratory or the construction site during the progress of the work. A concrete slump test is
carried out from batch to batch to check the uniform quality of concrete during construction. The
slump test is the simplest workability test for concrete, involves low cost and provides
immediate results. Due to this fact, it has been widely used for workability tests since 1922.
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2.Water absorption Test:
The water absorption test of concrete measures the amount of water that a concrete sample can
absorb. This test is important for determining the durability and resistance to water of the
concrete and helps to ensure that the concrete will perform as expected in its intended
environment.
3.Compression Test:
The compressive strength of the concrete cube test provides an idea about all the
characteristics of concrete. By this single test one judge that whether Concreting has been
done properly or not. Compressive strength of concrete depends on many factors such as
water-cement ratio, cement strength, quality of concrete material, and quality control during
4.Flexural Test:
Flexural strength of Concrete, also known as Modulus of rupture, is an indirect measure of the
tensile strength of unreinforced concrete. Modulus of rupture can also be defined as the
measure of the extreme fiber stresses when a member is subjected to bending. Apart from
external loading, tensile stresses can also be caused by warping, corrosion of steel, drying
shrinkage and temperature gradient. Concrete is strong in compression but weak in tension
because of which the flexural strength accounts for only 10% to 20% of the compressive
strength.
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5.Appearance Test:
Appearance test shows us that with the increasing Sewage Sludge Ash how the Appearance.
6.Workability Test:
measured.
The beams were cast for this test having dimensions (150mmX150mmX1000mm). The
specimen was placed in a machine for uniform loading. The load was applied to uppermost
part of mound along with two loading points. Applying loads two steel rollers were used in
the assembly. The load continuously applied 180kg/min until failure occurs. The Flexural
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strength test at 28 days (N/mm2) when the sludge is added in increasing order then test reading
of the tensile reading get deceasing gradually for the M30 grade concrete.
1 0 4.52
2 5 4.06
3 10 3.89
4 15 3.05
5 20 2.89
8.Appearance Change:
The first change in concrete after using SSA appeared in the appearance of the specimens.
Fig. 10 shows six concrete specimens in which the content of sludge ash was increased
from left to right. In this figure, the con- troll specimen, with no SSA, is shown on the
left, while the specimen in which 30% of cement was replaced with SSA is shown on the
right. As can be seen, the color of specimens has become darker as the content of SSA has
increased, such that the specimen containing 30% SSA is entirely dark.
The 100mm Dia x 50 mm height cylinder after casting were immersed in water for 90 days
curing. These specimens were then oven dried for 24 hours at the temperature 110°C until the
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mass became constant and again weighed. This weight was noted as the dry weight (W1) of
the cylinder. After that the specimen was kept in hot water at 85°c for 3.5 hours.
Then this weight was noted as the wet weight (W2) of the cylinder.
Where,
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Fig. 6.5 Flexural Failure
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CHAPTER VII
CONCLUSION
1.5% replacement of cement by wastepaper sludge ash showed 10% increase in compressive
3.With increase in wastepaper sludge ash content, percentage water absorption increases.
4.With increase in wastepaper sludge ash content, average weight decreases by 4.58% for mixture
with 20% wastepaper sludge ash content thus making wastepaper sludge ash concrete light weight.
5.The workability of concrete mix decreases with increase in wastepaper sludge ash content.
6.Splitting tensile strength decreases with increase in wastepaper sludge ash content and is more
7.Use of wastepaper sludge ash in concrete can prove to be economical as it is non useful waste
8.Use of wastepaper sludge ash in concrete will eradicate the disposal problem of wastepaper
sludge ash, reduce emission of harmful pollutants by cement manufacture industry into our
environment and thus prove to be environment friendly, paving way for greener concrete.
9.Use of wastepaper sludge ash in concrete will preserve natural resources that are used for cement
manufacture and thus make concrete construction industry sustainable and wastepaper sludge can
be used as fuel before using its ash in concrete for partial cement replacement and also the
disposal problem for paper industries for this waste material is fully solved.
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FUTURE SCOPE
We have studied in the work that the wastepaper sludge has the cementations properties, during
the entire course of we have got some clues where further work can be done:
The study may be further extended to check the ability of concrete to pumping purpose, because
The wastepaper sludge is a constructional element, and it is mandatory to check such concrete
under flexure, shear, torsion, and compression provide a framework for ensuring quality and
safety in construction practices. Finally, initiatives to raise public awareness and promote
acceptance of sludge-based construction materials are necessary for fostering widespread adoption
and overcoming potential barriers to implementation. There will be several aspects that can be
sludge
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CHAPTER VIII
REFRENCES
Alqedra, M.Arafa & M.Mattar Influence of low and high organic wastewater sludg on physical
and mechanical properties of concrete mixes” Journal of Environmental sciences and Technology
Ghada Mortada Rabie (2016) “Using of Wastewater Dry and Wet Sludge in Concrete Mix”.
Khalil Ahmed, “Hybrid composites prepared from Industrial waste: Mechanical and swelling
R. F. Reis and J. S. Cordeiro (2013) “Sustainable uses and method for water treatment plant
Roccaro, “Use of sludge from water and wastewater treatment plants in the production of
concrete,” 2015.
Baeza, F., Payá, J., Galao, O., Saval, J. M. and Garcés, P. (2014). Blending of Industrial Waste
from Different Sources as Partial Substitution of Portland cement in Pastes and Mortars. Journal
Benhelal, E., Zahedi, G., Shamsaei, E. and Bahadori, A. 2013. Global Strategies and Potentials to
Curb CO2 Emissions in Cement Industry. Journal of Cleaner Production, 51, 142–16.
against Carbonation and Chloride Migration. Journal of Materials and Structures, 37(273), 591.
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