robert azeradMétabolites omeprazole
OM, Omeprazole (M = 346)
5-hydroxyomeprazole (M = 362)
OMD, M= 346
H-1
7.10 (d)
7.09 (d)
7.00 (d)
H-3
6.98 (dd)
6.88 (dd)
6.84 (dd)
H-4
7.52 (d)
7.49 (d)
7.37 (d)
H-11
8.14 (s)
8.34 (s)
8.32 (s)
CH2-S
4.75 (AB)
? échangés avec MeOH-d4 ?
4.57 (s)
OCH3
3.85 (s)
3.70 (s)
3.83 (s)
3.72 (s)
3.82 (s)
CH3
2.23 (s)
2.16 (s)
2.14 (s)
2.28 (s)
CH2OH
-
4.65 (s)
4.66 (s)
C-1
99
C-1a
C-2
158
C-3
114
C-4
120
C-4a
C-5
C-6
61
C-7
152
C-8
C-9
162
C-10
128
C-11
149
C-12
16.5
C-13
15
OMe-2
55
OMe-9
60
N° C
d, ppm , J Hz
d, ppm
1
-
2
-
3
-
4
7.10, d, 2.4
5
-
6
6.98, dd, 2.4 & 8.9
115.0
7
7.52, d, 8.9
8
4.78-4.71 (AB system)
60.0
9
-
10
-
11
-
165
12
-
128
13
8.11, s
149.8
14
2.23*, s
11.4
15
2.16*, s
10.1
OCH3
3.85, s
54.85
OCH3
3.70, s
59.26
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