Lab Manual 2017
Lab Manual 2017
Lab Manual 2017
FACULTY OF ENGINEERING
CHEMICAL ENGINEERING PROGRAMME
(HK03)
LAB MANUAL
Semester
Laboratory
WORKSHOP BLOCK E
MAKMAL SAINS HABA 2 BLOCK C
Lecturer
Dr. S.M. Anisuzzaman
Lab. Assistants
Mr. Razis
Mr. Muhd Ruslan
Mr. Saiyful
Table of Contents
2
1.0 Laboratory Safety in General
1.2Personal Protection
Laboratory coat, safety goggles and gloves (if needed) should be
worn all the time in the laboratory.
Always assure that you wash your hands before leaving the
laboratory.
Short skirts, shorts and open-toed shoes/sandals should not be
worn in the laboratory to avoid skin exposure.
3
1.3Fire Hazards and Hazardous Chemicals
Always store flammable liquids in appropriate safety cabinets/cans.
1.4Laboratory Housekeeping
All equipment should be inspected carefully before used.
4
Keep laboratory floor dry at all times. Any spills must be
immediately attended to.
1.6Emergency Procedures
All laboratory personnel/users must be familiar with the location
and uses of the safety devices in and around the laboratory, for
example:
Safety shower
Fume hood
Fire extinguisher
First aid kit
Eye wash station
Fire alarm
5
material is dry. Transfer mixture into plastic bag, tie up and label,
place in fume hood. Contact laboratory personnel for disposal.
6
2.0 Report Writing Guidelines
Your laboratory report should contain the followings:
Cover page
Name & Matric number of the student
Name of experiment
Date of experiment
Group number
2.0 Methodology
Equipment, apparatus and material
Procedure
Describe the process in chronological order explain all steps in
the order they actually happened, not as they were supposed to
happen
3.0 Result
Result
Clear/concise summary of the collected data
Reports of data and their analysis
Table & Figure
Should all be titled
Label clearly
Include some explanatory text describing what data appears in
the table
7
Observation
4.0 Discussion
Interpret the results of the experiment and discuss their meaning
Your discussion relates the results to the issues raised in the
introduction
Compare expected results with those obtained
Explain your results in terms of theoretical issues
Relate results to your experiment objective
Analyze any experimental error
5.0 Conclusion
Answer the problem stated in the title and introduction
Base your conclusion on your results
Reference
Laboratory manual
Any outside reading
Appendices
Raw data, calculation, graph, picture/figure, table that have not been
included in the report (make sure you refer to each appendices at least
once in your report)
8
FLUID MECHANICS LABORATORY EXPERIMENT 1
1.0 INTRODUCTION
D1 D2
P1 P2
9
Refer to Figure 1.2, from consideration of continuity between the
mouth of the venture at section 1 and the throat at section 2:
AV A V
Q 1 1 2 2 (1.1)
A2 V
2 1
A1 V2 (1.2)
Rearranging,
P1 P2 V 2 V12
H 2
g g (1.4)
(1.6)
AV A 2g H
Q 2 2 2
1 4 (1.7)
The actual discharge will be less than this due to losses causing
the velocity through the throat to be less than that predicted by
Bernoullis Theorem, therefore it is necessary to introduce an
10
experimentally determined coefficient of discharge C d. The actual
discharge will then be given by:
C A 2g H
Q d 2
1 4 (1.8)
where (1.9)
The coefficient of discharge varies with both the Reynolds
number and area ratio. Typically values for a machined venturi meter
are between 0.975 and 0.995.
The pressure loss across the venture meter is less than the
pressure difference measured between the mouth and the throat due
to the pressure recovery which occurs in the divergence as the kinetic
energy is reduced.
1.2 OBJECTIVES
11
Diameter of venturi mouth = ______ mm
Diameter of venturi throat = ______ mm
Manometer Manometer
Flowrat
Inlet (cm) Outlet (cm) Sampl Time
e
1 2 3 Averag 1 2 3 Averag e (L) (s)
(L/min)
e e
23
22
21
20
19
18
17
16
15
14
13
12
11
OBSERVATIONS:
12
Quantities of water
collected, Q (L)
Time to collect
water, t (s)
Volume flow rate,
Q (L/min)
Inlet head, H1 (m)
Outlet head, H2
(m)
Venturi differential
head, H (H1-H2)
(m)
Venturi differential
head, (H)1/2
Area of venturi
throat, A2 (m2)(10-
4
)
Velocity at venturi
throat, V2 (m/s)
Q, volumetric flow
rate (A2V2)
Actual discharge,
Cd
13
FLUID MECHANICS LABORATORY EXPERIMENT 2
2.0 INTRODUCTION
14
fluid
Reynolds was able to show that the character of the flow could
be described with the aid of a dimensionless parameter, which is now
known as Reynolds number,
VD
Re = (2.1)
hf 32 V (2.2)
i
L gD 2
hf 4 fV 2
i= (2.4)
L D2 g
V
(2.5)
y
15
The unit of viscosity is in the cgs system is the poise .
A measure of the fluidity of a substance is the kinematics
viscosity whch is defined as:-
(2.6)
i.e. =
(2.7)
P d2 / 4 (2.8)
P d2 / 4 = dL
(2.10)
P d (2.11)
L 4
16
P d
0
L 4 (2.12)
0
cons tan t
d D
(2.13)
From which it follows that the shear stress varies linearly from
zero at the centre to a maximum at the pipe wall.
The shear stress is related to velocity by Newtons law of
viscosity
V
r (2.14)
V P d
r L 4 (2.15)
Replacing d by 2r
rr P
V
2 L (2.16)
(2.18)
D 2 P
Vmean
32 L (2.19)
Rearranging,
17
32LV mean
P
D2 (2.20)
hf
The head loss per unit length of pipe which is known as the
L
hydraulic gradient, symbol i, is then given by
hf 32 Vmean
i
L gD 2
(2.22)
The forces acting on the cylinder of fluid are the pressure forces
producing the flow and the opposing shear forces caused by frictional
resistance at the wall.
LD PD 2 / 4
(2.23)
PD
(2.24)
L4
18
Now accepting that the shear stress is proportional to the square
of the mean velocity
V2 (2.25)
then, KV 2
(2.26)
where K is a constant.
P D
. KV 2
L 4
(2.27)
4 KLV 2
P (2.28)
D
4 KLV 2
hf =
gD
= 4 fL V
2
D 2g
(2.29)
where f = 2 K is the Darcy friction factor.
The alternative definition of friction factor is often shown as f (f
dash) and the head loss equation is then written as
2
hf = f ' L V
D 2g
(2.30)
19
2.1.6 Friction factors
The head loss due to friction for both laminar and turbulent flow
can be presicted by the Darcy Weisbatch equation
32 V
i
gD 2 (2.31)
(2.32)
4f V2 f 'V 2
i or i
D 2g D 2g (2.33)
16 16 64 64
where f or f '
VD Re VD Re (2.34)
20
Substituting for V into Poiseuilles equation for laminar flow
2
hf 4 fV 2 4 f 4Q hence i 1
i
L D 2 g D 2 g D 2 D4 (2.38)
2
hf4 fV 2 4 f 4Q hence i 1
i
L D2 g D 2 g D 2 D5 (2.39)
2.2 OBJECTIVES
Assembly Ensure the bell mouthed entry end of the P6220 test
section is at the left hand end and that is correctly
inserted into the inlet tank. Ensure that the P6221 7
mm bore test section is installed the correct way
round with the conical inlet at the left hand end.
1. Start the pump and establish a water flow through the test section.
Raise the swivel tube of the outlet tank so that it is close to the
vertical.
21
2. Adjust the bench regulating valve (or pump speed) to provide a
small overflow from the inlet tank and overflow pipe. Ensure that
any air bubbles are bled from the manometer tubes.
Variable Head
Outlet Tank
Quantity of water
Collected, Q
(Litres)
Time to Collect
Water, t (sec)
Inlet Head,
H1 (mm)
Outlet Head
H2 (mm)
Variable Head
Outlet Tank
Quantity of water
Collected, Q
(Litres)
Time to Collect
Water, t (sec)
Inlet Head,
H1 (mm)
Outlet Head
H2 (mm)
22
OBSERVATIONS:
Quantity of Water
Collected, Q (litre)
Time to Collect
Water, t (sec)
Volume Flow Rate, Q
(litres/min)
Mean Velocity, V
(m/sec)
Loge V
Reynolds Number, Re
Loge Re
Inlet Head, H1 (mm)
Outlet Head, H2 (mm)
Friction Head Loss, hf
(mm) (H1-H2)
Loge hf
Friction Factor, f
Loge f
23
Density:.. kg/m2
Viscosity:.cP
Quantity of Water
Collected, Q (litre)
Time to Collect
Water, t (sec)
Volume Flow Rate, Q
(litres/min)
Mean Velocity, V
(m/sec)
Loge V
Reynolds Number, Re
Loge Re
Inlet Head, H1 (mm)
Outlet Head, H2 (mm)
Friction Head Loss, hf
(mm) (H1-H2)
Loge hf
Friction Factor, f
Loge f
24
APPENDIX
25
FLUID MECHANICS LABORATORY EXPERIMENT 3
3.0 INTRODUCTION
26
Cv (USA) US Gallons / min Pound / inch2
kv (Europe) Cubic meters / hour Kg / cm2
P
Q CV (3.1)
S
SQ 2
P (3.2)
C v2
SQ 2
hv (3.3)
gC v2
Q2 A 2V 2
hv (3.4)
gC v2 gC v2
V2
hv K v (3.5)
2g
Equating these two expressions for the valve head loss yields:
1
K v (3.6)
C v2
a) Linear in which Cv .
27
proportional increase in valve opening causes the same
proportional increase in flow providing the pressure across
the valve remains constant. For example, if a valve has a
Cv of 64 at 80% opening and an equal percentage
characteristic, then at 40% opening the C v will be 64 x
(40/80)2 = 16. If the valve opening is changed from 40%
to 41%, the Cv valve will increase from 16 to 16(41/40) 2 =
16.81, that is a 5.0625% increase. If the valve opening at
80% is increased to 82% the C v value will increase from 64
to 64(82/80)2 = 67.24, that is a 5.0625% increase in flow.
3.2 OBJECTIVE
28
3.3 EQUIPMENT PREPARATION
1. Before starting the pump, operate the valve through its full range of
movement and establish, using a protractor for the ball valve, a
datum position and means of measuring the degree of valve
opening.
2. Fully open the valve in the test section. Start the pump and
establish a water flow through the test section. Raise the swivel
tube of the outlet tank so that it is close the vertical.
Water Temperature . C
Density .kg/m2
Viscosity .. cP
Test Section Diameter mm
29
Quantity of water
Collected, Q
(litres)
Time to Collect
Water, t (sec)
Volume Flow Rate,
Q (litres/min)
Mean Velocity,
V (m/sec)
Velocity Head,
V 2 /2g (m)
Inlet Head,
h 1 (mm)
Outlet Head,
h 2 (mm)
Pipe Friction Loss,
h P (mm)
Valve Friction Loss,
h V (m)
Valve Pressure
Loss,
P (Pa)
Valve Flow
Coefficient,
C V (gpm/psi1/2)
Valve Opening,
degrees ()
Valve Opening, t
Percent (%)
OBSERVATION:
3. Calculate the velocity and hence the velocity head for each result.
30
experiment 2 then correct the results for any difference in the
diameter of the two test sections (P 1/D5).
5. Calculate the pressure loss across the valve and determine the
valve flow coefficient for each result, convert the flow coefficient to
a percentage of the flow coefficient for the fully open valve.
6. Plot a graph of flow coefficient against valve opening for ball valve.
31
FLUID MECHANICS LABORATORY EXPERIMENT 4
4.0 INTRODUCTION
Gauge pressure
Absolute
pressure
Vacuum
Atmospheric Pressure
Pressure)
( Barometer
Absolute zero
32
Zero atmospheric pressure is the pressure at which air is
removed creates at vacuum. This pressure is called ABSOLUTE ZERO.
Any pressure measured on these bases is called ABSOLUTE PRESSURE.
Thus one atmospheric pressure is equal to 101.325 kilo Newton per
square meter (kN/m2) or 14.7 pound per square inch. Since barometer
is used to measure atmospheric pressure, this pressure is often
referred to as Barometer pressure, Pb.
Generally pressure measuring device measure pressure
difference from that of atmospheric. The resulting pressure is called
Gauge pressure, Pg which can be positive or negative value. Thus,
33
4.1.1.3 Velocity Head, (Hv)
34
minimum head that pump must exert to the fluid before any flow
occurs.
When liquid flows from one point to the next suction side of the
pump to discharge side, there is a small head loss due to fricton-
between liquid and passage wall. This is called Friction Head.
The values of the above losses depend on the flow. The higher
the flow rate, the higher the loss. Therefore, during pump operation the
Actual Total Suction Head to Static Suction Lift plus Friction Head from
1 to 5. If the liquid level on the suction side is higher than centerline of
the pump Total Suction Head equal Static Suction Head minus Total
Friction on the suction side.
Similarly, on the discharge side, the sum of all friction losses
from 6 to 9 is the Total Friction Head on the discharge side. The Total
Discharge Head thus equal Static Head plus Friction Head on the
discharge side.
35
4.1.1.6 Total Head of Fluid,(HT)
Total head at any point of the liquid is the sum of all heads at
point.
HT = H p + H v + H s
= P/ + V2/2g + Z (4.6)
If friction is considered,
HTD = HT1 HT2 + Hf12
=( P2 P1)/ + (V22 V12)/2g + (Z2-Z1) + Hf12 (4.9)
Power is the amount of work done per unit time. This unit may
be in Watts (N-m/s). One Horse Power equal 745.7 Watts or 550ft-lb/s.
In pump operation, we consider 2 types of power.
This is power that pump delivers to the liquid and often referred
to has Hydraulic Power or Water Power. Hydraulic Power depend on the
rate of flow (Q) and head (HTD) or pressure (P).
Wo QP or QHTD (4.10)
If Wo is the liquid power in Watts
Q is the Flow rate in lt/min
P is the pressure in kg/cm 2
L 1 min 1m 3 kg f 10 4 cm 2 9.81N
W0 Q P
min 60 sec 1000 L cm 2 m2 1kg f
= 1.635 Q P (N- m)/sec
36
= 1.635 Q P Watts. (4.11)
Wi = Fr 2n (4.12)
4.2 OBJECTIVES
37
To determine the total head-discharge characteristics, hydraulic power
and efficiency of a centrifugal pump:
[Attn: Do not use the variable Speed Control Unit to adjust the
flowrate or to correct any changes in pump speed]
38
3. Start the test with the regulating valve fully closed. Record
the pump suction and delivery pressures and the pump
speed.
3. Start the test with the regulating valve fully closed and a
pump speed of 60 rev/sec. Record the pump suction and
delivery pressures and the pump speed.
39
7. Further readings are taken for pump heads at approximately
equal increments of pump discharge pressure until the beach
regulating valve is fully open.
Quantity of water
collected, Q (litres)
Time to collect water,
t (sec)
Pump 1 Inlet
pressure, P1 (bar)
Pump 1 Outlet
pressure, P2 (bar)
Pump 1 Speed,
(Rev/sec)
Pump 1 Electrical
Input Power, Wi
(Watts)
Constant Speed
Quantity of water
collected, Q (litres)
Time to collect water,
t (sec)
Pump 1 Inlet
pressure, P1 (bar)
Pump 1 Outlet
pressure, P2 (bar)
Pump 1 Electrical
Input Power, Wi
(Watts)
Quantity of water
collected, Q (litres)
Time to collect water,
40
t (sec)
Pump 1 Inlet
pressure, P1 (bar)
Pump 1 Outlet
pressure, P2 (bar)
Pump 1 Electrical
Input Power, Wi
(Watts)
OBSERVATION:
Hm = (P2-P1)/g
Wh = g HmQ
0 = Wh/Wi
Quantity of water
collected, Q (litres)
Time to collect water,
41
t (sec)
Volume Flow Rate
Q (litres/min)
Pump 1 Inlet
pressure, P1 (bar)
Pump 1 Outlet
pressure, P2 (bar)
Pump 1 Speed,
(Rev/sec)
Pump 1 Electrical
Input Power, Wi
(Watts)
Pump 1 Manometric
Head, Hm (meter)
Pump 1 Hydraulic
Power, Wh (Watts)
Pump 1 Overall
Efficiency, 0 (%)
Constant Speed
Quantity of water
collected, Q (litres)
Time to collect water,
t (sec)
Volume Flow Rate
Q (litres/min)
Pump 1 Inlet
pressure, P1 (bar)
Pump 1 Outlet
pressure, P2 (bar)
Pump 1 Speed,
(Rev/sec)
Pump 1 Electrical
Input Power, Wi
(Watts)
Pump 1 Manometric
Head, Hm (meter)
Pump 1 Hydraulic
Power, Wh (Watts)
Pump 1 Overall
Efficiency, 0 (%)
Quantity of water
collected, Q (litres)
42
Time to collect water,
t (sec)
Volume Flow Rate
Q (litres/min)
Pump 1 Inlet
pressure, P1 (bar)
Pump 1 Outlet
pressure, P2 (bar)
Pump 1 Speed,
(Rev/sec)
Pump 1 Electrical
Input Power, Wi
(Watts)
Pump 1 Manometric
Head, Hm (meter)
Pump 1 Hydraulic
Power, Wh (Watts)
Pump 1 Overall
Efficiency, 0 (%)
43
FLUID MECHANICS LABORATORY EXPERIMENT 5
5.0 INTRODUCTION
Coefficient of velocity
44
At a level H above the orifice, velocity of water discharge
through the orifice is V = 2gH. This velocity consists of horizontal and
vertical components. As air resistance is negligible, velocity V can be
considered as constant.
At the same time, the jet path is dropping due to gravity starting
from zero velocity at the orifice.
For this experiment, we assume the jet path touch the probes at
point 1, 2 ,3 8 respectively.
Y1, Y2 can be measured from the graph (tips of probe 1 and 2).
45
Water is directed to the bench measuring tank or a measuring
cup. Thus flow rate can be determined by timing.
5.2 OBJECTIVE
To study the flow through orifice i.e. velocity coefficient and discharge
coefficient and actual jet profile may be compared with that of theory.
An over flow pipe can adjust water level in the tank to as high as 42
cm from the center of the orifice. Water from overflow should be
directed to the storage tank.
The sharp edged orifice is attached to and flushing with the side of
the tank. Two orifices are provided 3 mm and 6 mm diameter.
46
measurement of flow rate.
3. Open the water supply valve to obtain a steady flow with minimum
overflow.
4. Wait until water level in the tank and jet profile is stable before
adjusting the probes tips to be in line with the center of the jet and
record the probe tips profile (upper tips) as well as y=0 mark.
5. Record the flow volume by using a stop watch and the bench
measuring tank or a measuring cup.
Experiment No.
1 2 3 4 5 6 7
Water level H (mm)
Volume (lit)
Time (sec)
Flow rate (lit/min)
Distance from graph
(mm)
X1 = 50, Y1 =
X2 = 100, Y2 =
X3 = 150, Y3 =
X4 = 200, Y4 =
X5 = 250, Y5 =
X6 = 300, Y6 =
X7 = 350, Y7 =
X8 = 400, Y8 =
Coefficient of Velocity
CV1
CV2
CV3
CV4
CV5
CV6
CV7
47
CV8
Coefficient of
Discharge
Cd
OBSERVATIONS:
48
5.6 RESULTS AND ANALYSIS
Diameter of Orifice d = 8 mm
Water level H = 410 mm
Volume = 2 L
Time = 21.26 s
Flow rate = 0.094 L/s
X5 = 250 mm
Y5 = 43 mm
Coefficient of velocity, CV
CV = X/2YH
CV5 = 250/243x410
CV5 = 250/2x132.78 =0.94
49