Card Information

Names: Tin
Tin, syn
Formula: Sn
PDF Number: 4-673
Quality: star
Subfiles: inorganic mineral alloy NBS CP FOR EDU
Cell and Symmetry Information
System: tetragonal Space Group: I41/amd (no. 141)
a: 5.831 c: 3.182
Density (Dx): 7.286 Z: 4
Instrument Information
Radiation: CuKa1 Wavelength: 1.54056 Filter: Ni
Instrument(d): unknown
Instrument(I): diffractometer I type: unknown
I/Icor: 1.97
Comments and Additional Information
General: Space group given by Mark, Polanyi, Z. Phys., 18 75-96 (1925).
Source: Sample was furnished by Johnson Matthey Company, Ltd. and annealed 12
hours at 160 C.
Analysis: Analysis (wt.%): Pb 0.0012, Sb 0.001, Fe 0.00027, Cu 0.0002, As 0.0002, Bi
0.00012, S 0.0003, Sn 99.997 (by difference), other form alpha-Sn (cubic).
Temperature: Pattern taken at 26 C.
Melting Point: 231.8 degrees
Colour: Light gray metallic
General: Color from Dana's System of Mineralogy, 7th Ed., 485.
Pattern: See ICSD 40037 (PDF 86-2264).

Literature References
General: Swanson, Tatge. Natl. Bur. Stand. (U.S.), Circ. 539 I 24 (1953)

Peak Data

Intensity 4-673 (Tin)

100
Tin

80

60

40

20

0.50 1.00 1.50 2.00 2.50 3.00

d
 PeakList
h k l d I
2 0 0 2.9150 100
1 0 1 2.7930 90
2 2 0 2.0620 34
2 1 1 2.0170 74
3 0 1 1.6590 17
1 1 2 1.4840 23
4 0 0 1.4580 13
3 2 1 1.4420 20
4 2 0 1.3040 15
4 1 1 1.2920 15
3 1 2 1.2050 20
4 3 1 1.0950 13
1 0 3 1.0434 3
3 3 2 1.0401 5
4 4 0 1.0309 2
5 2 1 1.0252 5
2 1 3 0.9824 5
6 0 0 0.9718 2
3 0 3 0.9310 3
5 1 2 0.9286 13
6 2 0 0.9219 5
6 1 1 0.9178 5
3 2 3 0.8868 4
5 4 1 0.8755 2
4 1 3 0.8485 4
5 3 2 0.8466 10
6 3 1 0.8386 4
6 4 0 0.8086 6
7 0 1 0.8058 3

Card Information
Names: alpha-Tin
gray tin
Formula: Sn
PDF Number: 5-390
Quality: star
Subfiles: inorganic alloy NBS CP FOR EDU

Cell and Symmetry Information

System: cubic Space Group: Fd-3m (no. 227)
a: 6.489
Z: 8

Instrument Information
Radiation: CuKa1 Wavelength: 1.5405 Filter: Ni
Instrument(d): unknown
Instrument(I): diffractometer I type: unknown

Comments and Additional Information

Colour: Gray
Preparation: Sample was made from NBS Melting Point Standard 42D by seeding it with
small quantity of alpha-Sn.
Analysis: Spectroscopic analysis: <0.01% Cu, Fe, Pb.
 General: Sample was refrigerated at 10 C until just before use.
Temperature: Pattern taken at 25 C.
General: Merck Index , 8th Ed., p. 1053.
Pattern: See ICSD 70128 (PDF 87-794).

Literature References
General: Swanson, Fuyat. Natl. Bur. Stand. (U.S.), Circ. 539 II 12 (1953)

Peak Data
Intensity 5-390 (alpha-Tin)
100
PeakList
alpha-Tin h k l d I
1 1 1 3.7510 100
2 2 0 2.2940 83
80
3 1 1 1.9560 53
4 0 0 1.6220 12
3 3 1 1.4890 20
60 4 2 2 1.3250 21
5 1 1 1.2490 11
4 4 0 1.1470 6
5 3 1 1.0968 10
40
6 2 0 1.0260 9
5 3 3 0.9895 4
4 4 4 0.9365 3
20 5 5 1 0.9087 7
6 4 2 0.8671 13
7 3 1 0.8450 12
0

0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00

d

Card Information
Names: Tin
Formula: Sn
PDF Number: 18-1380
Quality: star
Subfiles: inorganic alloy

Cell and Symmetry Information

System: tetragonal Space Group: I4/mmm (no. 139)
a: 3.811 c: 3.483
Density (Dx): 7.790 Z: 2

Instrument Information
Radiation: CuKa Wavelength: 1.5418
Instrument(d): unknown
Instrument(I): unknown I type: unknown

Comments and Additional Information

Temperature: Pattern at 39 kbar, 308-320 C.

Literature References
General: Barnett et al. Science 141 1041 (1963)
Peak Data
Intensity 18-1380 (Tin) PeakList
100 h k l d I
Tin
1 1 0 2.6950 50
1 0 1 2.5710 100
80
2 0 0 1.9060 40
0 0 2 1.7410 10
2 1 1 1.5310 30
1 1 2 1.4630 5
60
2 2 0 1.3470 5

40

20

1.00 1.20 1.40 1.60 1.80 2.00 2.20 2.40 2.60 2.80
d
Card Information
Names: Lead
Lead, syn
Formula: Pb
PDF Number: 4-686
Quality: star
Subfiles: inorganic mineral alloy NBS CP FOR EDU

Cell and Symmetry Information

System: cubic Space Group: Fm-3m (no. 225)
a: 4.9506
Density (Dm): 11.365 Density (Dx): 11.341 Z: 4

Instrument Information
Radiation: CuKa1 Wavelength: 1.54056 Filter: Ni
Instrument(d): unknown
Instrument(I): diffractometer I type: unknown

Comments and Additional Information

Colour: Light gray metallic
Source: Sample obtained from American Smelting and Refining Company.
Preparation: It was annealed for 1 hour and 180 C in petrolatum.
Analysis: Spectrographic analysis shows faint traces of Bi and Mg.
General: Purity >99.999%.
Temperature: Pattern taken at 26 C.

Literature References
General: Swanson, Tatge. Natl. Bur. Stand. (U.S.), Circ. 539 I 34 (1953)

Peak Data
Intensity 4-686 (Lead) PeakList
100 h k l d I
Lead
1 1 1 2.8550 100
2 0 0 2.4750 50
80 2 2 0 1.7500 31
3 1 1 1.4930 32
2 2 2 1.4290 9
60 4 0 0 1.2380 2
3 3 1 1.1359 10
4 2 0 1.1069 7
40
4 2 2 1.0105 6
5 1 1 0.9526 5
4 4 0 0.8752 1
20
5 3 1 0.8369 9
6 0 0 0.8251 4
0

0.50 1.00 1.50 2.00 2.50 3.00

d
Card Information
Names: Zinc
Zinc, syn
Formula: Zn
PDF Number: 4-831
Quality: star
Subfiles: inorganic mineral alloy NBS CP FOR EDU PIG

Cell and Symmetry Information

System: hexagonal Space Group: P63/mmc (no. 194)
a: 2.665 c: 4.947
Density (Dm): 7.050 Density (Dx): 7.134 Z: 2

Instrument Information
Radiation: CuKa1 Wavelength: 1.5405 Filter: Ni
Instrument(d): unknown
Instrument(I): diffractometer I type: unknown
I/Icor: 3.80

Comments and Additional Information

Source: Sample from New Jersey Zinc Company, Sterling Hill, New Jersey, USA.
Temperature: Pattern taken at 26 C.
Melting Point: 420 degrees
Optical: B=2.58
Colour: Bluish white
Analysis: Spectroscopic analysis shows faint traces of Pb, Cu, Mg, Si.

Literature References
General: Swanson, Tatge. Natl. Bur. Stand. (U.S.), Circ. 539 I 16 (1953)
Optical: Winchell. Elements of Optical Mineralogy 1 (1927)

Peak Data
Intensity 4-831 (Zinc) PeakList
100
Zinc
h k l d I
0 0 2 2.4730 53
1 0 0 2.3080 40
1 0 1 2.0910 100
80

1 0 2 1.6870 28
60
1 0 3 1.3420 25
1 1 0 1.3320 21
0 0 4 1.2370 2
40 1 1 2 1.1729 23
2 0 0 1.1538 5
2 0 1 1.1236 17
20
1 0 4 1.0901 3
2 0 2 1.0456 5
0
2 0 3 0.9454 8
0.80 1.00 1.20 1.40 1.60 1.80 2.00 2.20 2.40 2.60 1 0 5 0.9093 6
d 1 1 4 0.9064 11
2 1 0 0.8722 5
2 1 1 0.8589 9
2 0 4 0.8437 2
0 0 6 0.8245 1
2 1 2 0.8225 9
Card Information
Names: Titanium
Formula: Ti
PDF Number: 44-1294
Quality: star
Subfiles: inorganic alloy CP FOR EXP

Cell and Symmetry Information

System: hexagonal Space Group: P63/mmc (no. 194)
a: 2.9505 c: 4.6826
Density (Dx): 4.504 Z: 2

Instrument Information
Radiation: CuKa1 Wavelength: 1.54056 Filter: Graph
Instrument(d): diffractometer Cut Off: 15.0 Standard: Si
Instrument(I): diffractometer I type: peak heights
I/Icor: 0.9

Comments and Additional Information

Colour: Gray
Source: Sample was obtained from A.D. Mackay Inc.
General: Average relative standard deviation in intensity of the ten strongest
reflections for three specimen mounts = 6.7%.
Pattern: Validated by calculated pattern.
Pattern: To replace 5-682.
General: Component of pyrotechnic boom powders.

Literature References
General: Sailer, R., McCarthy, G., North DakotaState University, Fargo, North
Dakota, USA. ICDD Grant-in-Aid (1993)

Peak Data
Intensity 44-1294 (Titanium)
PeakList
100
h k l d I
Titanium 1 0 0 2.5550 25
0 0 2 2.3410 30
1 0 1 2.2430 100
80
1 0 2 1.7262 13
1 1 0 1.4753 11
1 0 3 1.3320 11
60 2 0 0 1.2776 1
1 1 2 1.2481 9
2 0 1 1.2324 6
0 0 4 1.1707 1
40
2 0 2 1.1215 1
1 0 4 1.0643 1
2 0 3 0.9887 2
20 2 1 0 0.9658 1
2 1 1 0.9459 4
1 1 4 0.9170 3
0
2 1 2 0.8928 1
0.80 1.00 1.20 1.40 1.60 1.80 2.00 2.20 2.40 2.60
d
Card Information
Names: Molybdenum
Formula: Mo
PDF Number: 42-1120
Quality: star
Subfiles: inorganic alloy CP FOR EDU

Cell and Symmetry Information

System: cubic Space Group: Im-3m (no. 229)
a: 3.1472
Z: 2

Instrument Information
Radiation: CuKa1 Wavelength: 1.5405988 Filter: Graph
Instrument(d): diffractometer Cut Off: 3.0 Standard: Al2O3
Instrument(I): diffractometer I type: unknown
I/Icor: 7.38

Comments and Additional Information

Source: Sample from Johnson Matthey, AESAR 10030, Lot G11A06.
Colour: Black
Pattern: To replace 4-809.

Literature References
General: Schreiner, W., Intelligent Controls Inc.,Amawalk, NY, USA. ICDD Grant-in-
Aid (1991)
Unit Cell: Swanson, Tatge. Natl. Bur. Stand. (U.S.), Circ. 539 1 20 (1953)

Peak Data
Intensity 42-1120 (Molybdenum)
PeakList
100
h k l d I
Molybdenum 1 1 0 2.2247 100
2 0 0 1.5738 16
2 1 1 1.2847 31
80 2 2 0 1.1129 9
3 1 0 0.9953 14
2 2 2 0.9085 3
60
3 2 1 0.8411 24

40

20

0.80 1.00 1.20 1.40 1.60 1.80 2.00 2.20 2.40

d
Card Information
Names: Magnesium
Formula: Mg
PDF Number: 35-821
Quality: star
Subfiles: inorganic alloy NBS CP FOR EDU EXP
Cell and Symmetry Information
System: hexagonal Space Group: P63/mmc (no. 194)
a: 3.20936 c: 5.2112
Z: 2
Instrument Information
Radiation: CuKa1 Wavelength: 1.5405981 Filter: Graph
Instrument(d): diffractometer Cut Off: 17.7 Standard: W
Instrument(I): diffractometer I type: peak heights
Comments and Additional Information
Source: The sample was obtained from Fisher Scientific Company, Fair Lawn, New
Jersey, USA. It contained a small amount of Mg ( O H )2.
Colour: Dark gray
Temperature: The temperature of data collection was approximately 25.0 C.
Pattern: To replace 4-770.
General: Pyrotechnic.
Literature References
General: Natl. Bur. Stand. (U.S.) Monogr. 25 21 82 (1984)
Structure: Jevins, A. et al. Z. Phys. Chem. (B) 40 347 (1938)

Peak Data
Intensity 35-821 (Magnesium) PeakList
100 h k l d I
Magnesium
1 0 0 2.7782 25
0 0 2 2.6050 36
80 1 0 1 2.4520 100
1 0 2 1.9002 15
1 1 0 1.6047 12
60 1 0 3 1.4730 16
2 0 0 1.3899 2
1 1 2 1.3664 13
40 2 0 1 1.3430 8
0 0 4 1.3028 2
2 0 2 1.2264 2
20 1 0 4 1.1797 2
2 0 3 1.0854 3
2 1 0 1.0506 1
0 2 1 1 1.0299 4
0.50 1.00 1.50 2.00 2.50 3.00
1 1 4 1.0116 3
d
1 0 5 0.9760 2
2 1 2 0.9742 2
2 0 4 0.9505 1
3 0 0 0.9266 1
2 1 3 0.8988 2
3 0 2 0.8729 1
2 0 5 0.8338 1
1 0 6 0.8289 1
2 1 4 0.8178 1
3 0 3 0.8174 1
2 2 0 0.8023 1
Card Information
Names: Silicon
Silicon, syn
Formula: Si
PDF Number: 27-1402
Quality: star
Subfiles: inorganic mineral alloy CP FOR EDU

Cell and Symmetry Information

System: cubic Space Group: Fd-3m (no. 227)
a: 5.43088
Density (Dx): 2.329 Z: 8

Instrument Information
Radiation: CuKa1 Wavelength: 1.5405981
Instrument(d): diffractometer Standard: W
Instrument(I): diffractometer I type: unknown
I/Icor: 4.70

Comments and Additional Information

Temperature: Pattern taken at 25(1) C.
Source: This sample is NBS Standard Reference Material No. 640.
General: Reflections calculated from precision measurement of a#0.
General: a#0 uncorrected for refraction.
Pattern: To replace 5-565 and 26-1481.
Colour: Gray

Literature References
General: Natl. Bur. Stand. (U.S.) Monogr. 25 13 35 (1976)

Peak Data

Intensity 27-1402 (Silicon) PeakList

100 h k l d I
Silicon
1 1 1 3.1355 100
2 2 0 1.9201 55
80 3 1 1 1.6375 30
4 0 0 1.3577 6
3 3 1 1.2459 11
60
4 2 2 1.1086 12
5 1 1 1.0452 6
4 4 0 0.9600 3
40
5 3 1 0.9180 7
6 2 0 0.8587 8
5 3 3 0.8282 3
20

0.50 1.00 1.50 2.00 2.50 3.00 3.50

d
Card Information
Names: Copper
Copper, syn
Formula: Cu
PDF Number: 4-836
Quality: star
Subfiles: inorganic mineral alloy NBS CP FOR EDU

Cell and Symmetry Information

System: cubic Space Group: Fm-3m (no. 225)
a: 3.6150
Density (Dm): 8.950 Density (Dx): 8.936 Z: 4

Instrument Information
Radiation: CuKa1 Wavelength: 1.5405 Filter: Ni
Instrument(d): unknown
Instrument(I): diffractometer I type: unknown

Comments and Additional Information

Melting Point: 1083 degrees
Preparation: It had been heated in an H2 atmosphere at 300 C.
Source: Sample from metallurgical laboratory of NBS, Gaithersburg, Maryland, USA.
General: Impurities from 0.001-0.01%, Ag, Al, Bi, Fe, Si, Zn.
RL Opaque mineral optical data on specimen from unspecified locality,
R#3R%=60.65, Disp.=Std.
VH VHN#1#0#0=96-104,
General: Measured density and color from Dana's System of Mineralogy, 7th Ed., I
99.
Colour: Red
Pattern: See ICSD 64699 (PDF 85-1326).
Temperature: Pattern taken at 26 C.

Literature References
General: Swanson, Tatge. Natl. Bur. Stand. (U.S.), Circ. 539 I 15 (1953)
RL IMA Commission on Ore Microscopy QDF ( )

Peak Data
Intensity 4-836 (Copper) PeakList
100
Copper
h k l d I
1 1 1 2.0880 100
2 0 0 1.8080 46
80
2 2 0 1.2780 20
3 1 1 1.0900 17
60
2 2 2 1.0436 5
4 0 0 0.9038 3
3 3 1 0.8293 9
40 4 2 0 0.8083 8

20

0.80 1.00 1.20 1.40 1.60 1.80 2.00 2.20

d