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    Chemistry Record Work-Xii

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    PREJAN RAJA
    The document describes Experiment 1 from a chemistry lab manual on the preparation of Mohr's salt (ferrous ammonium sulfate). It provides the aim, theory, required materials, procedure, results, and an observation table. The procedure involves weighing ferrous sulfate and ammonium sulfate, dissolving them in water with dilute sulfuric acid, filtering and concentrating the solution through crystallization, and obtaining pure Mohr's salt crystals. The yield of ferrous ammonium sulfate crystals is then recorded.

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    Chemistry Record Work-Xii

    Uploaded by

    PREJAN RAJA
    240 views23 pages
    The document describes Experiment 1 from a chemistry lab manual on the preparation of Mohr's salt (ferrous ammonium sulfate). It provides the aim, theory, required materials, procedure, results, and an observation table. The procedure involves weighing ferrous sulfate and ammonium sulfate, dissolving them in water with dilute sulfuric acid, filtering and concentrating the solution through crystallization, and obtaining pure Mohr's salt crystals. The yield of ferrous ammonium sulfate crystals is then recorded.

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    CHEMISTRY RECORD WORK-XII

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    The document describes Experiment 1 from a chemistry lab manual on the preparation of Mohr's salt (ferrous ammonium sulfate). It provides the aim, theory, required materials, procedure, results, and an observation table. The procedure involves weighing ferrous sulfate and ammonium sulfate, dissolving them in water with dilute sulfuric acid, filtering and concentrating the solution through crystallization, and obtaining pure Mohr's salt crystals. The yield of ferrous ammonium sulfate crystals is then recorded.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    240 views23 pages

    Chemistry Record Work-Xii

    Uploaded by

    PREJAN RAJA
    The document describes Experiment 1 from a chemistry lab manual on the preparation of Mohr's salt (ferrous ammonium sulfate). It provides the aim, theory, required materials, procedure, results, and an observation table. The procedure involves weighing ferrous sulfate and ammonium sulfate, dissolving them in water with dilute sulfuric acid, filtering and concentrating the solution through crystallization, and obtaining pure Mohr's salt crystals. The yield of ferrous ammonium sulfate crystals is then recorded.

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    CHEMISTRY RECORD WORK (2020-21)

    REFERENCE: CHEMISTRY LAB MANUAL – FULL MARKS

    EXPERIMENT - 1
    PREPARATION OF MOHR’S SALT

    Aim
    To prepare a pure sample of Mohr’s salt (ferrous ammonium sulphate) FeSO4.(NH4)2SO4.6H2O.

    Theory
    The formula for ferrous ammonium sulphate is FeSO4.(NH4)2SO4.6H2O. It is prepared by
    dissolving equimolar mixture of hydrated ferrous sulphate and ammonium sulphate in water
    containing a little sulfuric acid. The solution is subjected to crystallization, ferrous ammonium
    sulphate separates out from the solution.
    The chemical reaction is given below.
    FeSO4 + (NH4)2SO4 + 6H2O → FeSO4.(NH4)2SO4.6H2O (Mohr’s salt)
    The addition of sulphuric acid in this experiment prevents the hydrolysis of this salt.

    Materials Required
    • Conical flask
    • Tripod stand
    • Burner
    • Funnel
    • Watch glass
    • Glass rod
    • Filter paper
    • Wire gauze
    • China dish
    • Ferrous sulphate
    • Ammonium sulphate
    • Dilute sulphuric acid

    Procedure
    • Weigh 7g of ferrous sulphate and 3.5g of ammonium sulphate separately.
    • Mix ferrous sulphate and ammonium sulfate in water in a beaker containing dilute
    sulphuric acid.
    • Gently warm the solution in order to get a clear solution.
    • Filter the solution in order to remove suspended impurities and concentrate the clear
    filtrate by heating it china dish over a sand bath till the crystallization point is reached.
    • Stir the solution occasionally during heating.
    • Keep the solution undisturbed for slow cooling. After some time crystal of ferrous
    ammonium sulphate will get separated from the solution.
    • Separate the crystals by decantation from the mother liquor and wash the crystals with
    cold water.
    • Dry the crystals and note down the yield of the product.
    Results:
    • The pure sample of Mohr’s salt is prepared.
    • The yield of Ferrous ammonium sulphate or Mohr’s salt is _______ gm.

    Observation Table:

    Colour of the crystal Light green

    Shape of the crystal Octahedral

    Solubility in water Soluble

    Action of blue litmus paper Blue litmus turns red

    Note : write this observation table in left side.


    EXPERIMENT – 2
    EXPERIMENT – 3
    EXPERIMENT – 4
    EXPERIMENT – 5
    EXPERIMENT – 6
    EXPERIMENT – 7
    EXPERIMENT – 8

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