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    Fi011822 - Alcan RM 10

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    harry mahfuzan
    This document provides a certificate of analysis for a certified reference material called RM-10, which is a red mud sample from Vaudreuil, Canada collected on August 2, 2001. It was certified according to Alcan standard methods and includes assigned values for 20 chemical parameters determined using various test methods, such as loss on ignition, elemental composition by XRF, and phases by DSC. The certificate also provides guidance on sample usage and traceability of the certification.

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    Fi011822 - Alcan RM 10

    Uploaded by

    harry mahfuzan
    23 views2 pages
    This document provides a certificate of analysis for a certified reference material called RM-10, which is a red mud sample from Vaudreuil, Canada collected on August 2, 2001. It was certified according to Alcan standard methods and includes assigned values for 20 chemical parameters determined using various test methods, such as loss on ignition, elemental composition by XRF, and phases by DSC. The certificate also provides guidance on sample usage and traceability of the certification.

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    FI011822_ALCAN-RM-10

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    This document provides a certificate of analysis for a certified reference material called RM-10, which is a red mud sample from Vaudreuil, Canada collected on August 2, 2001. It was certified according to Alcan standard methods and includes assigned values for 20 chemical parameters determined using various test methods, such as loss on ignition, elemental composition by XRF, and phases by DSC. The certificate also provides guidance on sample usage and traceability of the certification.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    23 views2 pages

    Fi011822 - Alcan RM 10

    Uploaded by

    harry mahfuzan
    This document provides a certificate of analysis for a certified reference material called RM-10, which is a red mud sample from Vaudreuil, Canada collected on August 2, 2001. It was certified according to Alcan standard methods and includes assigned values for 20 chemical parameters determined using various test methods, such as loss on ignition, elemental composition by XRF, and phases by DSC. The certificate also provides guidance on sample usage and traceability of the certification.

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    © All Rights Reserved
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    ALCAN

    Arvida Research and Development Centre


    1955 Mellon Blvd. Mailing Address: Tel.: (418) 699-6585
    Jonquière, Québec G7S 4K8 P.O. Box 1250 Fax: (418) 699-2919
    Canada Jonquière, Québec G7S 4K8 www.alcan.com
    Canada

    ALCAN CONFIDENTIAL

    Alcan Certified Reference Material Program


    Certificate of Analysis

    RED MUD FROM Canada (Vaudreuil, august 2 2001)- RM-10

    Certification:

    This reference material has been certified according to Alcan standard methods for which
    ARDC is accredited ISO 17025. 20 bottles randomly selected were analyzed for this preliminary
    certification. The measurement of uncertainty, which is represented by one standard deviation,
    includes the inter-bottled heterogeneity and the method precision. Results are updated by
    benchmark analysis in 2007.

    Usage:

    This certified reference sample is intended both for instrument calibration and method control.
    Before sampling, the bottle should be vigorously shaken. An extra amount of sample should
    then be dried at 105°C for two hours. Finally, the exact portion is extracted. Do not return the
    unused sample in the bottle.

    Traceability:

    This material is traceable to previous Alcan standards for wet chemical analyses and phase
    analyses (TEA, TOC, g.Al2O3). For elemental composition, this material is traceable to NIST
    pure compounds and to previous Alcan standards.

    RM-10 Page 1 of 2 june 2007


    Arvida Research and Development Centre

    -2-

    ALCAN CONFIDENTIAL

    Assigned values:

    Assigned Standard
    Parameter Value Deviation Test Method
    (%) (%)
    Loss of Mass, 110-1000°C as H 2O and C 9.6 0.1 LECO or TGA
    Aluminum as Al2O3 20.1 0.2 Alcan SM 1359-99, XRF, glass beads/ICP
    Iron as Fe2O3 44.2 0.5 Alcan SM 1359-99, XRF, glass beads/ICP
    Silicon as SiO2 10.3 0.1 Alcan SM 1359-99, XRF, glass beads/ICP
    Titanium as TiO2 6.99 0.05 Alcan SM 1359-99, XRF, glass beads/ICP
    Chromium as Cr2O3 0.181 0.003 Alcan SM 1359-99, XRF, glass beads/ICP
    Calcium as CaO 1.15 0.02 Alcan SM 1359-99, XRF, glass beads/ICP
    Phosphorus as P2O5 0.198 0.005 Alcan SM 1359-99, XRF, glass beads/ICP
    Zirconium as ZrO2 0.213 0.006 Alcan SM 1359-99, XRF, glass beads/ICP
    Zinc as ZnO 0.007 0.002 Alcan SM 1359-99, XRF, glass beads/ICP
    Manganese as MnO 0.019 0.004 Alcan SM 1359-99, XRF, glass beads/ICP
    Vanadium as V2O5 0.210 0.004 Alcan SM 1359-99, XRF, glass beads/ICP
    Potassium as K2O 0.032 0.004 Alcan SM 1359-99, XRF, glass beads/ICP
    Magnesium as MgO 0.049 0.008 Alcan SM 1359-99, XRF, glass beads/ICP
    Sodium as Na2O 6.1 0.1 Alcan SM 1359-99, XRF, glass beads/ICP
    Sulfur as % SO3 0.44 0.02
    g-Al2O3 as Al2O3 1.4 0.2 DSC Alcan SM 1029-00
    Alcan SM 1177-04 , high temperature
    Total Extratable Alumina as Al2O3 9.8 0.1 1
    digestion
    Total Organic Carbon as C 0.23 0.03 Wet Oxidation
    o
    1 Conditions: 5.0 N NaOH, 225 C, 30 min

    Dr. Stéphane Paré reviewed by Patrick Dubé


    June 18, 2007

    RM-10 Page 2 of 2 june 2007

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