Designation: C 1019 – 03

Standard Test Method for

Sampling and Testing Grout1
This standard is issued under the fixed designation C 1019; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.

This standard has been approved for use by agencies of the Department of Defense.

1. Scope* 3. Significance and Use

1.1 This test method covers procedures for both field and 3.1 Grout used in masonry is a fluid mixture of cementitious
laboratory sampling and compression testing of grout used in materials and aggregate with a high water content for ease of
masonry construction. Grout for masonry is specified under placement.
Specification C 476. 3.1.1 During construction, grout is placed within or between
NOTE 1—The testing agency performing this test method should be
absorptive masonry units. Excess water must be removed from
evaluated in accordance with Practice C 1093. grout specimens in order to provide compressive strength test
results more nearly indicative of the grout strength in the wall.
1.2 The values stated in inch-pound units are to be regarded In this test method, molds are made from masonry units having
as the standard. the same absorption and moisture content characteristics as
1.3 This standard does not purport to address all of the those being used in the construction.
safety problems, if any, associated with its use. It is the 3.2 This test method is used to either help select grout
responsibility of the user of this standard to establish appro- proportions by comparing test values or as a quality control test
priate safety and health practices and determine the applica- for uniformity of grout preparation during construction.
bility of regulatory limitations prior to use. 3.3 The physical exposure condition and curing of the grout
2. Referenced Documents are not exactly reproduced, but this test method does subject
the grout specimens to absorption conditions similar to those
2.1 ASTM Standards:
experienced by grout in the wall.
C 39/C 39M Test Method for Compressive Strength of Cy-
lindrical Concrete Specimens2 NOTE 2—Test results of grout specimens taken from a wall should not
C 143/C 143M Test Method for Slump of Hydraulic Ce- be compared to test results obtained with this test method.
ment Concrete2 4. Apparatus
C 476 Specification for Grout for Masonry3
C 511 Specification for Moist Cabinets, Moist Rooms, and 4.1 Maximum-Minimum Thermometer.
Water Storage Tanks Used in the Testing of Hydraulic 4.2 Straightedge, a steel straightedge not less than 6 in.
Cements and Concretes4 (152.4 mm) long and not less than 1⁄16 in. (1.6 mm) in
C 617 Practice for Capping Cylindrical Concrete Speci- thickness.
mens2 4.3 Tamping Rod, a nonabsorbent rod, either round or
C 1064/C 1064M Test Method for Temperature of Freshly square in cross section nominally 5⁄8 in. (15.9 mm) in dimen-
Mixed Portland Cement Concrete2 sion with ends rounded to hemispherical tips of the same
C 1093 Practice for Accreditation of Testing Agencies for diameter. The rod shall be a minimum length of 12 in. (304.8
Unit Masonry3 mm).
4.4 Nonabsorbent Blocks, nonabsorbent, rigid squares with
side dimensions equal to one half the desired grout specimen
1
This test method is under the jurisdiction of ASTM Committee C12 on Mortars height, within a tolerance of 5 %, and of sufficient quantity or
and Grouts for Unit Masonry and is the direct responsibility of Subcommittee thickness to yield the desired grout specimen height, as shown
C12.02 on Research and Methods of Test.
Current edition approved June 10, 2003. Published August 2003. Originally
in Fig. 1, Fig. 2, and Fig. 3.
approved in 1984. Last previous edition approved in 2002 as C 1019–02. NOTE 3—Nonabsorbent blocks may be of plastic, wood, or other
2
Annual Book of ASTM Standards, Vol 04.02.
3 nonabsorbent material. Certain species of wood contain sugars which
Annual Book of ASTM Standards, Vol 04.05.
4
Annual Book of ASTM Standards, Vol 04.01.

*A Summary of Changes section appears at the end of this standard.

Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.

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 C 1019 – 03
unit in contact with the grout specimen shall not have been
previously used to mold specimens. Place nonabsorbent
blocks, cut to proper size and of the proper thickness or
quantity, at the bottom of the space to achieve the necessary
height of specimen. Tolerance on space and specimen dimen-
sions shall be within 5 % of the specimen width. See Fig. 1,
Fig. 2, and Fig. 3and accompanying notes.
NOTE—Front masonry unit stack not shown to allow view of specimen.
NOTE 6—Other methods of obtaining grout specimens and specimens
FIG. 1 Grout Mold (Units 6 in. (152.4 mm) or Less in Height, 21⁄4
of different geometry have been employed in grout testing, but are not
in. (57.2 mm) High Brick Shown)
described in this test method. Other methods used to obtain grout
specimens include: drilling grout-filled cores of regular units; filling cores
of masonry units specifically manufactured to provide grout specimens;
filling compartments in slotted corrugated cardboard boxes specifically
manufactured to provide grout specimens; and forming specimens from
different sized masonry units of the same or similar material.
Since test results vary with methods of forming and specimen geometry,
comparative test results between the specimen described in this test
method and the proposed specimen should be required and confined to a
single specimen shape and method of forming.
6.4 Line the masonry surfaces that will be in contact with
NOTE—Front masonry unit not shown to allow view of specimen. the grout specimen with a thin, permeable material to prevent
FIG. 2 Grout Mold (Units Greater than 6 in. (152.4 mm) High, 8 in. bond to the masonry units.
(203.2 mm) High Concrete Masonry Unit Shown)
NOTE 7—The lining, such as paper towel, is used to aid in stripping the
grout specimen from the mold. Proper installation of the lining prevents
cause retardation of cement. In order to prevent this from occurring, new irregularly sized specimens and varying test results.
wooden blocks shall be soaked in limewater for 24 h, sealed with varnish
or wax, or covered with an impermeable material prior to use. 6.5 Brace units to prevent displacement during grouting and
curing.
4.5 Panels and plates, pieces of 3⁄4 in. (19 mm) plywood
with dimensions as needed to contain units and grout speci- 7. Sampling Grout
mens. Soak in limewater for 24 h, seal with varnish or wax, or
7.1 Size of Sample—Grout samples to be used for slump and
cover with an impermeable material prior to use. A nonabsor-
compressive strength tests shall be a minimum of 1⁄2 ft3 (0.014
bant material of equivalent stiffness to the plywood is permit-
m3).
ted.
7.2 Procedure—The procedures used in sampling shall
PROCEDURES include the use of precautions that will assist in obtaining
samples that are representative of the nature and condition of
5. Test Specimens the grout. After the final slump adjustment has been made,
5.1 Each grout specimen shall have a square cross-section, sample grout as the grout is being placed.
3 in. (76 mm) or larger on the sides and twice as high as its 7.2.1 Field Sampling—Collect two or more portions taken
width. Dimensional tolerances shall be within 5 % of the width at regularly spaced intervals during the discharge of the middle
selected. portion of the batch. The elapsed time between obtaining the
5.2 Test at least three specimens at each age specified. first and final portions of the sample shall be not more than 15
min.
NOTE 4—Frequency of sampling and age of test is to be determined by 7.2.2 Laboratory Sampling—The entire mixed batch of
the specifier of this test method and is usually found in the construction grout is the sample.
documents.
NOTE 8—The field technician sampling, making, and curing specimens
6. Mold Construction for acceptance testing should be certified (American Concrete Institute
6.1 Select a level location where the molds remain undis- Field Testing Technician—Grade I, National Concrete Masonry Associa-
tion Masonry Testing Technician, or equivalent). Equivalent certification
turbed for 48 h. programs should include both written and performance examinations.
NOTE 5—The location of specimen construction should be protected 7.3 Transport the grout sample to the mold location. Protect
and as free from perceptible vibration as possible.
the sample from the sun, wind, and other sources of rapid
6.2 The construction of the mold shall simulate the in-situ evaporation and from contamination. Remix the sample with a
construction. If the grout is placed between two different types shovel or trowel to ensure uniformity.
of masonry units, both types shall be used to construct the
mold. 8. Temperature and Slump Test
6.3 Form a space with a square cross-section, 3 in. (76 mm) 8.1 Measure and record the temperature of the grout sample
or larger on each side and twice as high as its width, by in accordance with Test Method C 1064/C 1064M.
stacking masonry units of the same type and moisture condi- 8.2 Begin filling the slump cone within 5 min of obtaining
tion as those being used in the construction. The surface of the the final portion of the sample.

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 C 1019 – 03

NOTE—
FIG. 3 Grout Mold with Brick and Concrete Masonry Units

8.3 Measure and record the slump in accordance with the 10. Transportation, Curing, and Testing of the Specimens
requirements of Test Method C 143/C 143M. 10.1 Remove the molds between 24 and 48 h after making
the specimens.
9. Compressive Test Specimen 10.2 Within 30 min after removing the molds, place speci-
9.1 If grout from the slump test is used for the compressive mens in a protective container and keep specimens damp.
test specimens, remix the sample. Begin filling the compressive 10.3 Transport field specimens to the laboratory within 8 h
strength molds within 15 min of obtaining the final portion of after mold removal.
the sample. 10.4 Within 8 h after mold removal, place in a moist room,
9.2 Fill the mold with grout in two layers of approximately moist cabinet, or water storage tank conforming to Specifica-
equal depth. Rod each layer 15 times with the tamping rod. tion C 511. Store there until day of testing.
Rod the bottom layer through its depth. Slightly overfill the 10.5 Store there until day of testing. Keep specimen damp
mold. Rod the second layer with the tamping rod penetrating 1⁄2 until tested.
in. (12.7 mm) into the lower layer. Distribute the strokes 10.6 Cap the specimens in accordance with the applicable
uniformly over the cross section of the mold. requirements of Practice C 617.
9.3 Strike off the top surface of the specimen with a
NOTE 9—Practice C 617 refers to capping cylindrical specimens; there-
straightedge to produce a flat surface that is even with the top fore, the alignment devices may need to be modified to ensure proper use
edge of the mold and that has no depressions or projections with the rectangular prism specimens of this method. All other sections of
larger than 1⁄8 in. (3.2 mm). Cover immediately with a damp Practice C 617 are applicable.
absorbent material such as cloth or paper towel. Keep the top 10.7 Measure and record the width of each face at mid-
surface of the specimens damp by wetting the absorbent height. Measure and record the height of each face at mid-
material and covering with a nonabsorbent, nonreactive mate- width. Measure and record the amount out of plumb at
rial to retain the moisture. Do not disturb the specimens. mid-width of each face.
9.4 Within 30 min after filling the mold, add sufficient grout 10.8 Test the specimens in a damp condition in accordance
without rodding to fill the depression caused by initial water with the applicable requirements of Test Method C 39/C 39M.
loss. Strike off the top surface of the specimen with a
straightedge to produce a flat surface that is even with the top 11. Calculations
edge of the mold. Cover immediately with a damp absorbent 11.1 Determine the average cross-sectional area by measur-
material such as cloth or paper towel. Keep the top surface of ing the width of each face at its mid-height, calculating the
the specimen damp by wetting the absorbent material and average width of opposite faces, and multiplying the averages.
covering with a nonabsorbent, nonreactive material. Do not 11.2 Calculate the compressive strength by dividing the
disturb the specimen until the molds are removed. maximum load by the average cross-sectional area and express
9.5 Protect the specimens from freezing and variations in the result to the nearest 10 psi (69 kPa).
temperature. Store an indicating maximum-minimum ther-
mometer with the specimens and record the maximum and 12. Report
minimum temperatures experienced prior to the time the 12.1 The report shall include the following:
specimens are placed in the final curing environment. 12.1.1 Mix design,

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 C 1019 – 03
12.1.2 Slump of the grout, TABLE 2 Statistics of Field-Prepared Specimens
12.1.3 Type and number of units used to form mold for Number of
Mean, psi (MPa)
Standard Deviation, Coefficient of
specimens, Specimens psi (MPa) Variation, %

12.1.4 Description of the specimens—dimensions, amount 3 3583 (24.7) 118 (0.81) 3.3
6 5455 (37.6) 324 (2.23) 5.9
out of plumb in percent, 6 3992 (27.5) 228 (1.57) 5.7
12.1.5 Curing history, including initial temperature, maxi-
mum and minimum temperatures, and age of specimens when
transported to laboratory and when tested,
12.1.6 Maximum load and compressive strength of each 13.1.2 The standard deviation from field specimens of grout
specimen and average compressive strength of the specimens, will be higher than that for laboratory specimens. There is less
and control of grout ingredients, conditions of units for mold
12.1.7 Description of failure. construction, and initial curing environment in field-prepared
specimens.
13. Precision and Bias 13.2 Limited test data are available for analysis at this time.
13.1 General: A more detailed statement will be provided later. The following
13.1.1 The masonry units used to form the mold have summary of available data is provided for review.
different absorption rates and will remove slightly different 13.2.1 Laboratory Specimens—The coefficients of variation
amounts of water from each specimen. Thus the standard for a series of three laboratory prepared specimens ranged from
deviation for this test method is higher than that using a 5.8 % with a mean value of 6452 psi (44.45 MPa) to 24.6 %
nonabsorbent mold. with a mean value of 1373 psi (9.47 MPa) averaging 14.4 %.
The standard deviation ranged from 211 psi (1.46 MPa) to 505
TABLE 1 Statistics of Laboratory-Prepared Specimens psi (3.48 MPa). Tests with a larger number of specimens had
Number of Standard Deviation, Coefficient of the characteristics found in Table 1.
Mean, psi (MPa)
Specimens psi (MPa) Variation, %
13.2.2 Field Specimens—Test reports from one project
5 3784 (26.1) 306 (2.11) 8.1
5 2494 (17.2) 220 (1.52) 8.8
show the characteristics found in Table 2.
5 3178 (21.9) 634 (4.37) 20.0
6 5480 (37.8) 899 (6.2) 16.4 14. Keywords
10 5350 (36.9) 826 (5.7) 15.4
12 3872 (26.7) 333 (2.30) 8.6 14.1 cementitious; compressive strength; grout; masonry
units

SUMMARY OF CHANGES

Committee C12 has identified the location of selected changes to this standard since C 1019–02 that may
impact the use of this standard.

(1) Section 10.5 was added to address specimen curing and (3) Sections 4.5 and Fig 3 were added and Section 4.4 and 6.2
handling. were revised to include grout specimens for double wythe
(2) Section 10.4 was changed to permit curing in a moist walls.
cabinet

Committee C12 has identified the location of selected changes to this standard since C 1019–00be1 that may impact the use of
this standard.

(1) Section 10 was revised to modify and add specific time (3) Reference for grout to conform to Specification C 476 was
requirements for handling and curing grout specimens. added.
(2) Paragraph 10.4 was changed to permit curing in a water
tank.

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 C 1019 – 03

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