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    Experiment 2 NH4 (PO4) 3

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    vc192677

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    Experiment 2 NH4 (PO4) 3

    Uploaded by

    vc192677
    12 views2 pages

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    Experiment 2 NH4(PO4)3

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    12 views2 pages

    Experiment 2 NH4 (PO4) 3

    Uploaded by

    vc192677

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    © All Rights Reserved
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    EXPERIMENT -
    Aim
    To analyse the given salt for one anion and one cation present in it.
    Material required
    Boiling tubes, test tubes, test tube holder, test tube stand, delivery tube, corks,
    filter papers, reagents
    PROCEDURE
    S. Experiment Observation Inference
    No.
    PHYSICAL EXAMINATION OF THE SALT
    1 Noted the colour of the White Cu2+, Fe2+, Ni2+, Co2+ ,
    given salt. Mn2+ are absent.
    2 Noted the smell of the Smell of NH4+ may be present
    salt. ammonia.
    TEST FOR ACID RADICAL
    1 2 mL solution of salt + 1 No gas evolved Absence of CO32-, S2-,
    mL dil.H2SO4 and SO32-, NO2-
    warmed
    2 2 mL solution of salt + 1 No gas evolved Absence of 𝐶𝑙 − ,
    mL conc. H2SO4 + heat 𝐵𝑟 − , 𝐼 − ,𝐶𝐻3 𝐶𝑂𝑂−
    𝐶2 𝑂4 2− , 𝑁𝑂32−
    3 2mL salt solution + dil. No ppt formed
    HCl + 2mL of BaCl2 Absence of 𝑆𝑂42−
    solution
    4 2mL salt solution + Conc. A canary yellow Presence of 𝑃𝑂43−
    HNO3+ ammonium precipitate is confirmed
    molybdate formed
    solution.Heated the
    mixture to boiling.
    TEST FOR BASIC RADICAL
    1 2mL salt solution + 2 mL Colourless gas Presence of 𝑁𝐻4+
    NaOH solution +Heat with ammoniacal
    smell evolved.

    2 Bring a glass rod dipped White fumes are Presence of 𝑁𝐻4+


    in Conc.HCl near the observed. confirmed
    mouth of the test tube.
    3 Add Nessler’s reagent to Brown ppt Presence of 𝑁𝐻4+
    the above solution formed confirmed

    RESULT: The given inorganic salt contains 𝑵𝑯+ 𝟑−


    𝟒 as basic radical and as𝑷𝑶𝟒
    acid radical. So, the salt is (𝑵𝑯𝟒 )3𝑷𝑶𝟒

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