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    Experiment 8 (NH4) 2 CO3

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    vc192677

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    Experiment 8 (NH4) 2 CO3

    Uploaded by

    vc192677
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    Original Title

    Experiment 8 (NH4)2 CO3 (1)

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    3 views2 pages

    Experiment 8 (NH4) 2 CO3

    Uploaded by

    vc192677

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
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    EXPERIMENT - 8

    Aim
    To analyse the given salt for one anion and one cation present in it.
    Material required
    Boiling tubes, test tubes, test tube holder, test tube stand, delivery tube, corks,
    filter papers, reagents
    PROCEDURE
    S. Experiment Observation Inference
    No.
    PHYSICAL EXAMINATION OF THE SALT
    1 Noted the colour of the White Cu2+, Fe2+, Ni2+, Co2+ ,
    given salt. Mn2+ are absent.
    2 Noted the smell of the Smell of NH4+ may be present
    salt. ammonia.
    TEST FOR ACID RADICAL
    1 0.1 g of salt + 1 mL Gas with brisk Presence of of CO32-
    dil.H2SO4 and warmed effervescence
    evolved which
    turns lime water
    milky.
    2 2mL Salt solution + Gas with brisk Presence of CO32-
    dil.HCl effervescence
    evolved which
    turns lime water
    milky.
    3 2mL Salt solution + White ppt Presence of CO32-
    MgSO4 solution confirmed
    TEST FOR BASIC RADICAL
    1 Heated 0.1 g of salt + 2 Colourless gas Presence of 𝑁𝐻4+
    mL NaOH solution with ammoniacal
    smell evolved.
    2 Bring a glass rod dipped White fumes are Presence of 𝑁𝐻4+
    in Conc.HCl near the observed. confirmed
    mouth of the test tube.
    3 Add Nessler’s reagent to Brown ppt Presence of 𝑁𝐻4+
    the above solution formed confirmed

    RESULT: The given inorganic salt contains NH4+as basic radical and as CO32-
    acid radical. So, the salt is (𝑵𝑯𝟒 )2CO3

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