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    Experiment 6 AlBr3

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    vc192677

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    Experiment 6 AlBr3

    Uploaded by

    vc192677
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    26 views2 pages

    Experiment 6 AlBr3

    Uploaded by

    vc192677

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    © All Rights Reserved
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    EXPERIMENT - 6

    Aim
    To analyse the given salt for one anion and one cation present in it.
    Material required
    Boiling tubes, test tubes, test tube holder, test tube stand, delivery tube, corks,
    filter papers, common lab reagents
    PROCEDURE
    S. Experiment Observation Inference
    No.
    PHYSICAL EXAMINATION OF THE SALT
    1 Noted the colour of the White Cu2+, Fe2+, Ni2+,
    given salt. Co2+ , Mn2+ are
    absent.
    2 Noted the smell of the No Smell of ammonia. Absence Of
    salt. CH3COO- and
    NH4+
    TEST FOR ACID RADICAL
    1 2 mL Salt solution + 1 mL No gas evolved Absence of
    dil.H2SO4 and warmed CO32-, S2-, SO32-,
    NO2-
    2 2 mL Salt solution + 1 mL Brown vapours evolved 𝐵𝑟 − May be
    conc. H2SO4 +heat. present.
    Confirmatory Test for Bromide(Br-) Radical
    3 AgNO3 Test: A pale yellow
    1 mL salt solution + dil. precipitate partially Presence of
    HNO3 + AgNO3 solution. soluble in ammonium 𝐵𝑟 − confirmed
    hydroxide solution is
    obtained.
    4 MnO2 Test: Brown vapours evolved Presence of
    1g of salt + a pinch 𝐵𝑟 − confirmed.
    ofMnO2 taken in a test
    tube. Add 3-4 drops
    conc.H2SO4and heat.
    TEST FOR BASIC RADICAL
    1 2mL salt solution+ 2 mL No gas evolved Absence of
    NaOH solution + Heated 𝑁𝐻4+
    2 Salt solution + dil. HCl No ppt Group I absent
    3 Above solution + H2S gas Np Black ppt Group II absent
    4 Salt solution + NH4Cl A gelatinous white Group III(Al3+)
    solid + heated + NH4OH precipitate may be present
    in excess added
    Dissolve the precipitate in dilute HCl and divide the solution into two
    parts.
    5 First part+ NaOH solution A white gelatinous ppt Presence of Al3+
    soluble in excess of confirmed
    NaOH solution formed
    6 Lake Test: A blue ppt floating in Presence of Al3+
    Second part+ 2-3 drops colourless solution is confirmed
    blue litmus solution + obtained
    ammonium hydroxide
    solution drop by drop.

    RESULT: The given inorganic salt contains 𝑨𝒍𝟑+ as basic radical 𝑩𝒓− and as
    acid radical. So, the salt is AlBr3

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