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    (CH3COO)2Pb

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    aditya chaudhary

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    © All Rights Reserved
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    (CH3COO)2Pb

    Uploaded by

    aditya chaudhary
    6 views1 page

    Copyright

    © © All Rights Reserved

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    Download as docx, pdf, or txt
    6 views1 page

    (CH3COO)2Pb

    Uploaded by

    aditya chaudhary

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    of 1

    EXPERIMENT

    AIM :- To analyse given salt for one cation and one anion.
    Experiment Observation Inference

    Physical examination-

    Note the colour of the given salt. White Fe2+, Cu2+, Ni2+,Co3+ are
    absent
    Note the smell of given salt
    Vinegar like smell CH3COO- may be present
    Test for anion:

    Dilute H2SO4 Test:

    To a pinch of salt add dil H2SO4 No gas evolved. CO32- , SO32- ,S2-, NO2- ions
    are absent.
    Conc. H2SO4 Test:

    Heat a pinch of salt with conc.H2SO4. Gas with vinegar like CH3COO- present.
    smell evolved.
    Confirmatory test for CH3COO- ion
    Neutral FeCl3 test:
    To aqueous solution of salt add
    Red ppt.
    neutral FeCl3 solution.
    Red colour disappears. CH3COO-confirmed..
    Filter the ppt. and add dil HCl to the
    filtrate.

    Test for cation:


    No smell of ammonia Zero group (NH4+ ) absent.
    Heat given salt with NaOH solution.

    Preparation of original solution (O.S.)


    Clear solution formed. Label it as O.S.
    Dissolve given salt in water.

    To O.S. add dil HCl. White ppt. I group(Pb2+) present


    Dissolve ppt in hot water. Divide it
    into two parts.
    Yellow ppt. Pb2+ confirmed.
    KI test- To first part add KI solution.
    K2CrO4 test- To second part add Pb2+ confirmed.
    Yellow ppt.
    K2CrO4 solution.

    Result: Given salt contains CH3COO- and Pb2+ ions.

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