Ex. No.: Date: Identification of Copper Alloys

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Ex. No.

:
Date :

IDENTIFICATION OF COPPER ALLOYS

Aim:
To identity the given mounted specimen by metallographic examination.

Apparatus required:

Grinding machine, double disc polishing machine, emery papers, and


Triocular microscope.

Etchant used ……………………………………….

Procedure:

1. The properly prepared metal specimen is kept under the metallurgical


microscope on the specimen table.
2. The objective and eye-piece are chosen properly to get the required
magnification.
3. The source light is switched on.
4. The metal specimen is focused by adjusting draw tube using coarse and fine
adjustment screws.
5. The metal is identified by viewing through the microscope and is compared
with the available charts.
6. If the image is not clear choose the next objectives lens and repeat the entire
procedure from step 4, till we get correct image.

Pre Lab Questions:

1. How brass differs from bronze based on composition?

2. Mention few applications of copper alloys.

Page no.
PURE COPPER
METAL / ALLOYS ETCHANT USED OBSERVATION
100 ml Dist. Water
Fully α phase with
10 gms of Ammonium Persulphate
PURE COPPER different grains
10 ml HCL 32%
orientation
10 -15 Sec Etching time

BRASS
METAL / ALLOYS ETCHANT USED OBSERVATION
100 ml Dist. Water
10 gms of Ammonium Persulphate Presence of White
BRASS
10 ml HCL 32% structure
10 -15 Sec Etching time

BRONZE

METAL / ALLOYS ETCHANT USED OBSERVATION


100 ml Dist. Water Presence of α
10 gms of Ammonium Persulphate phase, β Phase of
BRONZE
10 ml HCL 32% brass with different
10 -15 Sec Etching time color
3. Mention few areas where bronze is used

4. Which is hard material- brass or bronze?

5. What etchant is used to observe the microstructure?

Post Lab Questions:

1. Based on microstructure how brass differs from bronze?

2. What are the different phases you observe in the bronze microstructure?

3. What are the different phases of brass you have observed?

Page no.
SRM UNIVERSITY, KATTANKULATHUR Expt. No.:
MATERIALS TECHNOLOGY LAB Date:
METALLOGRAPHIC SHEET

Magnification :

Etchant used :

Composition of :
Etchant

Time of Etching : OBSERVED ACTUAL

Material Details:

Metal Identified :

Metal Composition :

Polishing Procedure :

Heat Treatment (if any) :

Description of Micro :
Structure

Material Properties :

Application :

Page no.
SRM UNIVERSITY, KATTANKULATHUR Expt. No.:
MATERIALS TECHNOLOGY LAB Date:
METALLOGRAPHIC SHEET

Magnification :

Etchant used :

Composition of :
Etchant

Time of Etching : OBSERVED ACTUAL

Material Details:

Metal Identified :

Metal Composition :

Polishing Procedure :

Heat Treatment (if any) :

Description of Micro :
Structure

Material Properties :

Application :

Page no.
SRM UNIVERSITY, KATTANKULATHUR Expt. No.:
MATERIALS TECHNOLOGY LAB Date:
METALLOGRAPHIC SHEET

Magnification :

Etchant used :

Composition of :
Etchant

Time of Etching : OBSERVED ACTUAL

Material Details:

Metal Identified :

Metal Composition :

Polishing Procedure :

Heat Treatment (if any) :

Description of Micro :
Structure

Material Properties :

Application :

Page no.
4. How α and ß phase differ by structure?

5. Which phase is hard? α phase or β phase.

Result:

Page no.

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