Ex. No.: Date: Identification of Light Metal Alloys

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Ex. No.

:
Date :

IDENTIFICATION OF LIGHT METAL ALLOYS


Aim:

To identity the given mounted specimen by metallographic examination.

Apparatus required:

Grinding machine, double disc polishing machine, emery papers, and


Trinocular microscope.

Etchant used ……………………………………….

Procedure:

1. The properly prepared metal specimen is kept under the metallurgical


microscope on the specimen table.
2. The objective and eye-piece are choosen properly to get the required
magnification.
3. The source light is switched on.
4. The metal specimen is focused by adjusting draw tube using coarse and fine
adjustment screws.
5. The metal is identified by viewing through the microscope and is compared
with the available charts.
6. If the image is not clear choose the next objectives lens and repeat the entire
procedure from step 4, till we get correct image.

Pre Lab Questions:

1. Which etchant is used to identify the structure?

2. Mention few applications of Titanium alloy?

Page no.
ALUMINIUM – SILICON ALLOY

METAL / ALLOYS ETCHANT USED OBSERVATION


96 ml of dist. Water
Shining Si particles
ALUMINIUM – SILICON 6 ml of HNO3 65%
distributed in Al
ALLOY 2 ml of HF 40%
matrix
10 -15 Sec Etching time

TITANIUM ALLOY

METAL / ALLOYS ETCHANT USED OBSERVATION


96 ml of dist. Water Presence of α phase,
6 ml of HNO3 65%
Ti-6Al-4V ALLOY β Phase duplex
2 ml of HF 40%
10 -15 Sec Etching time microstructure

MAGNESIUM ALLOY

METAL / ALLOYS ETCHANT USED OBSERVATION


96 ml of dist. Water
AZ91 MAGNESIUM 6 ml of HNO3 65% Presence of α phase,
ALLOY 2 ml of HF 40% β Phase
10 -15 Sec Etching time
3. Mention few applications of magnesium alloy?

4. What is the difference between wrought alloy and cast alloy?

5. What is the composition of etchant used for Light Metal Alloys?

Post Lab Questions:

1. What is the difference between the Nital and Al based alloy etchant?

2. At which magnification the Al-Si Alloy can be obtained neatly?

3. Mention few applications of Al- Si based alloy

Page no.
SRM UNIVERSITY, KATTANKULATHUR Expt. No.:
MATERIALS TECHNOLOGY LAB Date:
METALLOGRAPHIC SHEET

Magnification :

Etchant used :

Composition of :
Etchant

Time of Etching : OBSERVED ACTUAL

Material Details:

Metal Identified :

Metal Composition :

Polishing Procedure :

Heat Treatment (if any) :

Description of Micro :
Structure

Material Properties :

Application :

Page no.
SRM UNIVERSITY, KATTANKULATHUR Expt. No.:
MATERIALS TECHNOLOGY LAB Date:
METALLOGRAPHIC SHEET

Magnification :

Etchant used :

Composition of :
Etchant

Time of Etching : OBSERVED ACTUAL

Material Details:

Metal Identified :

Metal Composition :

Polishing Procedure :

Heat Treatment (if any) :

Description of Micro :
Structure

Material Properties :

Application :

Page no.
SRM UNIVERSITY, KATTANKULATHUR Expt. No.:
MATERIALS TECHNOLOGY LAB Date:
METALLOGRAPHIC SHEET

Magnification :

Etchant used :

Composition of :
Etchant

Time of Etching : OBSERVED ACTUAL

Material Details:

Metal Identified :

Metal Composition :

Polishing Procedure :

Heat Treatment (if any) :

Description of Micro :
Structure

Material Properties :

Application :

Page no.
4. Write the procedure for the preparation of the etchant.

5. State the need of etchant.

Result:

Page no.

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